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Title: Preparation and characterization of solar exfoliated graphene

Abstract

Hummer's method was used for the chemical synthesis of graphite oxide from graphite flakes. Simultaneous exfoliation and reduction of graphite oxide to Graphene was achieved through focused solar light irradiation using a convex lens. The morphological characteristics were studied using SEM and TEM. Layered morphology of Graphene was observed through TEM. Raman spectra and FTIR were used for the structural characterization of Graphene. EDAX analysis showed the drop in oxygen content during exfoliation. The method offered a faster, easier and environmental friendly method to produce Graphene for potential applications.

Authors:
Publication Date:
OSTI Identifier:
22308038
Resource Type:
Journal Article
Journal Name:
AIP Conference Proceedings
Additional Journal Information:
Journal Volume: 1620; Journal Issue: 1; Conference: Optics 14: International conference on optics: Light and its interactions with matter, Calicut, Kerala (India), 19-21 Mar 2014; Other Information: (c) 2014 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 0094-243X
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; CARBON OXIDES; FOURIER TRANSFORMATION; GRAPHENE; GRAPHITE; INFRARED SPECTRA; IRRADIATION; MORPHOLOGY; MULTI-ELEMENT ANALYSIS; RAMAN SPECTRA; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; TRANSMISSION ELECTRON MICROSCOPY; VISIBLE RADIATION

Citation Formats

M, Sreejesh, S, Nagaraja H., E-mail: hosakoppa@gmail.com, and K, Udaya Bhat, E-mail: udayabhatk@gmail.com. Preparation and characterization of solar exfoliated graphene. United States: N. p., 2014. Web. doi:10.1063/1.4898293.
M, Sreejesh, S, Nagaraja H., E-mail: hosakoppa@gmail.com, & K, Udaya Bhat, E-mail: udayabhatk@gmail.com. Preparation and characterization of solar exfoliated graphene. United States. https://doi.org/10.1063/1.4898293
M, Sreejesh, S, Nagaraja H., E-mail: hosakoppa@gmail.com, and K, Udaya Bhat, E-mail: udayabhatk@gmail.com. 2014. "Preparation and characterization of solar exfoliated graphene". United States. https://doi.org/10.1063/1.4898293.
@article{osti_22308038,
title = {Preparation and characterization of solar exfoliated graphene},
author = {M, Sreejesh and S, Nagaraja H., E-mail: hosakoppa@gmail.com and K, Udaya Bhat, E-mail: udayabhatk@gmail.com},
abstractNote = {Hummer's method was used for the chemical synthesis of graphite oxide from graphite flakes. Simultaneous exfoliation and reduction of graphite oxide to Graphene was achieved through focused solar light irradiation using a convex lens. The morphological characteristics were studied using SEM and TEM. Layered morphology of Graphene was observed through TEM. Raman spectra and FTIR were used for the structural characterization of Graphene. EDAX analysis showed the drop in oxygen content during exfoliation. The method offered a faster, easier and environmental friendly method to produce Graphene for potential applications.},
doi = {10.1063/1.4898293},
url = {https://www.osti.gov/biblio/22308038}, journal = {AIP Conference Proceedings},
issn = {0094-243X},
number = 1,
volume = 1620,
place = {United States},
year = {Wed Oct 15 00:00:00 EDT 2014},
month = {Wed Oct 15 00:00:00 EDT 2014}
}