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Title: Ion dynamics in nanocrystalline LiMnPO{sub 4} synthesised by novel template free hydrothermal approach

A dense core rectangular shaped nanocrystalline LiMnPO{sub 4} material was synthesized by template free sucrose assisted hydrothermal synthesis. The material possess orthorhombic crystal structure with Pnma, space group having four formula units. The structural characterization was accomplished through X-ray diffraction, thermo gravimetry/differential thermal analysis. Morphology was identified by the SEM, VSM was used to verify the magnetic behavior of the material and electrical characterization was done through impedance spectroscopy and the results were reported.
Authors:
 [1] ; ;  [2]
  1. St. Aloysius' College, Edathua, Alappuzha-689 573, Kerala (India)
  2. Department of Physics, School of Physical, Chemical and Applied Sciences, Pondicherry University, R.V. Nagar, Kalapet, Pondicherry -605 014 (India)
Publication Date:
OSTI Identifier:
22269487
Resource Type:
Journal Article
Resource Relation:
Journal Name: AIP Conference Proceedings; Journal Volume: 1591; Journal Issue: 1; Conference: 58. DAE solid state physics symposium 2013, Patiala, Punjab (India), 17-21 Dec 2013; Other Information: (c) 2014 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
77 NANOSCIENCE AND NANOTECHNOLOGY; ALUMINIUM COMPOUNDS; CRYSTALS; DIFFERENTIAL THERMAL ANALYSIS; HYDROTHERMAL SYNTHESIS; IMPEDANCE; MANGANESE PHOSPHATES; MORPHOLOGY; NANOSTRUCTURES; ORTHORHOMBIC LATTICES; SCANNING ELECTRON MICROSCOPY; SPECTROSCOPY; THERMAL GRAVIMETRIC ANALYSIS; VIBRATING SAMPLE MAGNETOMETERS; X-RAY DIFFRACTION