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Title: Effect of roll hot press temperature on crystallite size of PVDF film

Fabrication PVDF films have been made using Hot Roll Press. Preparation of samples carried out for nine different temperatures. This condition is carried out to see the effect of Roll Hot Press temperature on the size of the crystallite of PVDF films. To obtain the diffraction pattern of sample characterization is performed using X-Ray Diffraction. Furthermore, from the diffraction pattern is obtained, the calculation to determine the crystallite size of the sample by using the Scherrer equation. From the experimental results and the calculation of crystallite sizes obtained for the samples with temperature 130 °C up to 170 °C respectively increased from 7.2 nm up to 20.54 nm. These results show that increasing temperatures will also increase the size of the crystallite of the sample. This happens because with the increasing temperature causes the higher the degree of crystallization of PVDF film sample is formed, so that the crystallite size also increases. This condition indicates that the specific volume or size of the crystals depends on the magnitude of the temperature as it has been studied by Nakagawa.
Authors:
;  [1] ; ; ;  [2] ;  [3]
  1. Departement of Physics Faculty of Science and Technology, Islamic State University Syarif Hidayatullah , Jl. Juanda 95 Ciputat Jakarta (Indonesia)
  2. Theoretical High Energy Physics and Instrumentation Group Research, Faculty Mathematics and Natural Sciences, Institut Teknologi Bandung, Jl. Ganesa 10 Bandung (Indonesia)
  3. Departement of Physics, Faculty of Mathematics and Natural Sciences, Universitas Negeri Padang, Jl.Prof. Hamka, Padang 25131 (Indonesia)
Publication Date:
OSTI Identifier:
22265966
Resource Type:
Journal Article
Resource Relation:
Journal Name: AIP Conference Proceedings; Journal Volume: 1589; Journal Issue: 1; Conference: ICMNS 2012: 4. international conference on mathematics and natural sciences: Science for health, food and sustainable energy, Bandung (Indonesia), 8-9 Nov 2012; Other Information: (c) 2014 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; CHEMICAL PREPARATION; CRYSTALLIZATION; CRYSTALS; DENSITY; FILMS; ORGANIC FLUORINE COMPOUNDS; POLYVINYLS; PRESSES; X-RAY DIFFRACTION