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Title: Natural circulation loop using liquid nitrogen for cryo-detection system

The natural circulation loop is designed for the cryogenic insert in a Fourier transform ion cyclotron resonance (FTICR) mass spectrometer. Sensitivity is the key parameter of a FTICR mass spectrometer and the cryo-cooling of the pre-amplifier can reduce the thermal noise level and thereby improve the signal-to-noise ratio. The pre-amplifier consisted of non-magnetic materials is thermally connected to the cooling loop which is passing through the flange maintaining ultra-high vacuum in the ion cell. The liquid nitrogen passes through inside of the loop to cool the pre-amplifier indirectly. At the end, a cryocooler is located to re-condense nitrogen vapor generated due to the heat from the pre-amplifier. The circulating fluid removes heat from the pre-amplifier and transports it to the cryocooler or heat sink. In this paper the natural circulation loop for cryogenic pre-amplifier is introduced for improving the sensitivity of cryo-detector. In addition, the initial cool-down of the system by a cryocooler is presented and the temperature of the radiation shield is discussed with respect to the thickness of shield and the thermal radiation load.
Authors:
 [1]
  1. Korea Basic Science Institute, 169-148 Gwahak-ro, Yuseong-gu, Daejeon, 305-806 (Korea, Republic of)
Publication Date:
OSTI Identifier:
22263992
Resource Type:
Journal Article
Resource Relation:
Journal Name: AIP Conference Proceedings; Journal Volume: 1573; Journal Issue: 1; Conference: International cryogenic materials conference, Anchorage, AK (United States), 17-21 Jun 2013; Other Information: (c) 2014 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; 71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS; AMPLIFIERS; COOLING; DETECTION; FOURIER TRANSFORMATION; ION CYCLOTRON-RESONANCE; LIQUIDS; MAGNETIC MATERIALS; MASS SPECTROMETERS; NATURAL CONVECTION; NITROGEN; SENSITIVITY; SIGNAL-TO-NOISE RATIO; THERMAL RADIATION; VAPORS