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Title: Synthesis and X-ray crystal structure determination of N-p-methylphenyl-4-benzoyl-3,4-diphenyl-2-azetidinone

The title compound, C{sub 29}H{sub 23}NO{sub 2}, has been characterized by single-crystal X-ray diffraction at two different temperatures (303 K and 120 K) and wavelengths (MoK{sub {alpha}} and CuK{sub {alpha}}). The non-centrosymmetric hexagonal crystal structure contains four-membered planar {beta}-lactam ring with an unusually long C-C bond. The {beta}-lactam ring is almost planar.
Authors:
 [1] ;  [2] ;  [1] ;  [2] ;  [3] ; ;  [4]
  1. University of Ankara, Department of Engineering Physics, Faculty of Engineering (Turkey)
  2. Hacettepe University, Faculty of Sciences, Department of Chemistry (Turkey)
  3. Darmstadt University of Technology, Institute of Material Science (Germany)
  4. Institute of Physics (Czech Republic)
Publication Date:
OSTI Identifier:
22054040
Resource Type:
Journal Article
Resource Relation:
Journal Name: Crystallography Reports; Journal Volume: 55; Journal Issue: 7; Other Information: Copyright (c) 2010 Pleiades Publishing, Ltd.; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; CRYSTAL STRUCTURE; MONOCRYSTALS; ORGANIC NITROGEN COMPOUNDS; SYNTHESIS; TEMPERATURE RANGE 0065-0273 K; TEMPERATURE RANGE 0273-0400 K; X RADIATION; X-RAY DIFFRACTION