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Title: Preparation and characterization of hollow glass microspheres coated by CoFe{sub 2}O{sub 4} nanoparticles using urea as precipitator via coprecipitation method

Journal Article · · Materials Research Bulletin
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  1. National Laboratory of Superhard Materials, Jilin University, Changchun 130012 (China)
  2. Institute of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo 454003 (China)

The composite of hollow glass microspheres coated by CoFe{sub 2}O{sub 4} nanoparticles has been successfully prepared using urea as precipitator via coprecipitation method. The resultant composites were characterized by X-ray diffraction, field emission scanning electron microscope and vibrating sample magnetometer. The results showed that the slow decomposition of urea could be beneficial to form uniform and entire cobalt ferrite coating layer on the surface of hollow glass microspheres. The smoothest morphology was obtained for the sample prepared from 0.7 M urea, while the sample prepared from 1.0 M urea had the thickest shell. This indicated that there was a competition between the morphology and thickness of the coated microspheres. A possible formation mechanism of hollow glass microspheres coated with cobalt ferrite was proposed. The magnetic properties of the samples were also investigated.

OSTI ID:
21199674
Journal Information:
Materials Research Bulletin, Vol. 44, Issue 2; Other Information: DOI: 10.1016/j.materresbull.2008.05.009; PII: S0025-5408(08)00168-2; Copyright (c) 2008 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA); ISSN 0025-5408
Country of Publication:
United States
Language:
English