Chopped sample heating for quantitative profile analysis of low energy electron diffraction spots at high temperatures
- Institut fuer Laser- und Plasmaphysik, Universitaet Duisburg-Essen, D-45117 Essen (Germany)
Spot profile analysis low energy electron diffraction (SPA-LEED) is one of the most versatile and powerful methods for the determination of the structure and morphology of surfaces even at elevated temperatures. In setups where the sample is heated directly by an electric current, the resolution of the diffraction images at higher temperatures can be heavily degraded due to the inhomogeneous electric and magnetic fields around the sample. Here we present an easily applicable modification of the common data acquisition hardware of the SPA-LEED, which enables the system to work in a pulsed heating mode: Instead of heating the sample with a constant current, a square wave is used and electron counting is only performed when the current through the sample vanishes. Thus, undistorted diffration images can be acquired at high temperatures.
- OSTI ID:
- 20644018
- Journal Information:
- Review of Scientific Instruments, Vol. 75, Issue 11; Other Information: DOI: 10.1063/1.1807003; (c) 2004 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
- Country of Publication:
- United States
- Language:
- English
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