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Title: Recovery of very dilute acetic acid using ion exchange

Journal Article · · Industrial and Engineering Chemistry Research
;  [1]
  1. Univ. of Stellenbosch (South Africa). Dept. of Chemical Engineering

Acetic and related acids occur in many industrial wastewaters, often mixed with several other classes of organic compounds. Acetic acid can be recovered from 1% solutions using weakly basic ion exchange resins. The acid is adsorbed by the free-base form of the resin, which can then be eluted using a slurry of lime to give a solution of calcium acetate. This solution could either be evaporated to crystallize calcium acetate or reacted with sulfuric acid to form acetic acid and gypsum. Laboratory tests of the proposed process gave product solutions of 15--20% acetic acid using pure 1% acetic acid as feed. Some measurements using a typical industrial effluent gave similar recoveries and showed that there was no initial fouling of the resins.

Sponsoring Organization:
USDOE
OSTI ID:
178402
Journal Information:
Industrial and Engineering Chemistry Research, Vol. 34, Issue 7; Other Information: PBD: Jul 1995
Country of Publication:
United States
Language:
English