Discrimination and quantification of Fe and Ni abundances in Genesis solar wind implanted collectors using X-ray standing wave fluorescence yield depth profiling with internal referencing

Choi, Y.; Eng, P.; Stubbs, J.; Sutton, S. R.; Schmeling, M.; Veryovkin, I. V.; Burnett, D.

doi:10.1016/j.chemgeo.2016.08.025

Title: Discrimination and quantification of Fe and Ni abundances in Genesis solar wind implanted collectors using X-ray standing wave fluorescence yield depth profiling with internal referencing

Journal Article · Sun Aug 21 00:00:00 EDT 2016 · Chemical Geology

DOI:https://doi.org/10.1016/j.chemgeo.2016.08.025· OSTI ID:1340292

Choi, Y. ^[1]; Eng, P. ^[2]; Stubbs, J. ^[3];

^[2]; Schmeling, M. ^[4]; Veryovkin, I. V. ^[5]; Burnett, D. ^[6]

Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Univ. of Chicago, Argonne, IL (United States); Univ. of Chicago, Chicago, IL (United States)
Univ. of Chicago, Chicago, IL (United States)
Loyola Univ., Chicago, IL (United States)
Univ. of Illinois, Chicago, IL (United States)
California Inst. of Technology (CalTech), Pasadena, CA (United States)

In this paper, X-ray standing wave fluorescence yield depth profiling was used to determine the solar wind implanted Fe and Ni fluences in a silicon-on-sapphire (SoS) Genesis collector (60326). An internal reference standardization method was developed based on fluorescence from Si and Al in the collector materials. Measured Fe fluence agreed well with that measured previously by us on a sapphire collector (50722) as well as SIMS results by Jurewicz et al. Measured Ni fluence was higher than expected by a factor of two; neither instrumental errors nor solar wind fractionation effects are considered significant perturbations to this value. Impurity Ni within the epitaxial Si layer, if present, could explain the high Ni fluences and therefore needs further investigation. As they stand, these results are consistent with minor temporally-variable Fe and Ni fractionation on the timescale of a year.

View Accepted Manuscript (DOE)

View Accepted Manuscript (Publisher)

Cite

Export

Save

Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES); National Aeronautics and Space Administration (NASA)

Grant/Contract Number:: AC02-06CH11357; FG02-94ER14466

OSTI ID:: 1340292

Alternate ID(s):: OSTI ID: 1398680

Journal Information:: Chemical Geology, Vol. 441, Issue C; ISSN 0009-2541

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 2 works

Citation information provided by
Web of Science

References (21)

X-Ray Evanescent-Wave Absorption and Emission Becker, R. S.; Golovchenko, J. A.; Patel, J. R. Physical Review Letters, Vol. 50, Issue 3 https://doi.org/10.1103/PhysRevLett.50.153	journal	January 1983
X-ray standing waves: a molecular yardstick for biological membranes Bedzyk, M.; Bilderback, D.; Bommarito, G. Science, Vol. 241, Issue 4874 https://doi.org/10.1126/science.3175619	journal	September 1988
X-ray standing waves at a reflecting mirror surface Bedzyk, M. J.; Bommarito, G. M.; Schildkraut, J. S. Physical Review Letters, Vol. 62, Issue 12 https://doi.org/10.1103/PhysRevLett.62.1376	journal	March 1989
Concentration Profile of a Dissolved Polymer near the Air-Liquid Interface: X-Ray Fluorescence Study Bloch, J. M.; Sansone, M.; Rondelez, F. Physical Review Letters, Vol. 54, Issue 10 https://doi.org/10.1103/PhysRevLett.54.1039	journal	March 1985
Solar composition from the Genesis Discovery Mission Burnett, D. S.; Team, G. S. Proceedings of the National Academy of Sciences, Vol. 108, Issue 48 https://doi.org/10.1073/pnas.1014877108	journal	May 2011
The Genesis solar wind sample return mission: Past, present, and future Burnett, D. S. Meteoritics & Planetary Science, Vol. 48, Issue 12 https://doi.org/10.1111/maps.12241	journal	December 2013
Ion Implants as Matrix-Appropriate Calibrators for Geochemical Ion Probe Analyses Burnett, Donald S.; Jurewicz, Amy J. G.; Woolum, Dorothy S. Geostandards and Geoanalytical Research, Vol. 39, Issue 3 https://doi.org/10.1111/j.1751-908X.2014.00318.x	journal	January 2015
Theoretical Form Factor, Attenuation, and Scattering Tabulation for Z =1–92 from E =1–10 eV to E =0.4–1.0 MeV Chantler, C. T. Journal of Physical and Chemical Reference Data, Vol. 24, Issue 1 https://doi.org/10.1063/1.555974	journal	January 1995
Detailed Tabulation of Atomic Form Factors, Photoelectric Absorption and Scattering Cross Section, and Mass Attenuation Coefficients in the Vicinity of Absorption Edges in the Soft X-Ray (Z=30–36, Z=60–89, E=0.1 keV–10 keV), Addressing Convergence Issues of Earlier Work Chantler, C. T. Journal of Physical and Chemical Reference Data, Vol. 29, Issue 4 https://doi.org/10.1063/1.1321055	journal	July 2000
Glancing-incidence x-ray fluorescence of layered materials de Boer, D. K. G. Physical Review B, Vol. 44, Issue 2 https://doi.org/10.1103/PhysRevB.44.498	journal	July 1991
Resonance enhancement of x rays in layered materials: Application to surface enrichment in polymer blends Dev, B. N.; Das, Amal K.; Dev, S. Physical Review B, Vol. 61, Issue 12 https://doi.org/10.1103/PhysRevB.61.8462	journal	March 2000
Accurate analysis of shallowly implanted solar wind ions by SIMS backside depth profiling Heber, Veronika S.; McKeegan, Kevin D.; Burnett, Donald S. Chemical Geology, Vol. 390 https://doi.org/10.1016/j.chemgeo.2014.10.003	journal	December 2014
Nickel Isotopic Composition and Nickel/Iron Ratio in the Solar Wind: Results from SOHO/CELIAS/MTOF Karrer, R.; Bochsler, P.; Giammanco, C. Space Science Reviews, Vol. 130, Issue 1-4 https://doi.org/10.1007/s11214-007-9220-4	journal	July 2007
Atomic radiative and radiationless yields for K and L shells Krause, M. O. Journal of Physical and Chemical Reference Data, Vol. 8, Issue 2 https://doi.org/10.1063/1.555594	journal	April 1979
Surface Studies of Solids by Total Reflection of X-Rays Parratt, L. G. Physical Review, Vol. 95, Issue 2 https://doi.org/10.1103/PhysRev.95.359	journal	July 1954
Elemental Abundances of the Bulk Solar Wind: Analyses from Genesis and ACE Reisenfeld, D. B.; Burnett, D. S.; Becker, R. H. Space Science Reviews, Vol. 130, Issue 1-4 https://doi.org/10.1007/s11214-007-9215-1	journal	July 2007
Distortion of depth profiles during sputtering Sigmund, P.; Gras-Marti, A. Nuclear Instruments and Methods, Vol. 168, Issue 1-3 https://doi.org/10.1016/0029-554X(80)91281-1	journal	January 1980
Pb(II) distributions at biofilm-metal oxide interfaces Templeton, A. S.; Trainor, T. P.; Traina, S. J. Proceedings of the National Academy of Sciences, Vol. 98, Issue 21 https://doi.org/10.1073/pnas.201150998	journal	September 2001
Structure and reactivity of environmental interfaces: Application of grazing angle X-ray spectroscopy and long-period X-ray standing waves Trainor, Thomas P.; Templeton, Alexis S.; Eng, Peter J. Journal of Electron Spectroscopy and Related Phenomena, Vol. 150, Issue 2-3 https://doi.org/10.1016/j.elspec.2005.04.011	journal	February 2006
RIMS analysis of Ca and Cr in Genesis solar wind collectors Veryovkin, I. V.; Tripa, C. E.; Zinovev, A. V. Surface and Interface Analysis, Vol. 43, Issue 1-2 https://doi.org/10.1002/sia.3523	journal	June 2010
Resonance-enhanced x-rays in thin films: a structure probe for membranes and surface layers Wang, J.; Bedzyk, M.; Caffrey, M. Science, Vol. 258, Issue 5083 https://doi.org/10.1126/science.1439784	journal	October 1992

Cited By (1)

The future of Genesis science Burnett, D. S.; Jurewicz, A. J. G.; Woolum, D. S. Meteoritics & Planetary Science, Vol. 54, Issue 5 https://doi.org/10.1111/maps.13266	journal	February 2019

Similar Records

Discrimination and quantification of contamination and implanted solar wind in Genesis collector shards using grazing incidence synchrotron x-ray techniqies: Initial results

Conference · Wed Dec 13 00:00:00 EST 2006 · OSTI ID:1340292

Kitts, K; Sutton, S; Eng, P; +2 more

X-ray standing wave based internal reference method for quantification of implanted Fe in Genesis samples

Conference · Thu Mar 19 00:00:00 EDT 2009 · OSTI ID:1340292

Kitts, K; Choi, Y; Eng, P; +1 more

Discrimination and quantification of implanted solar wind in Genesis collector shards using grazing incidence synchrotron x-ray techniques: New detector initial results

Conference · Tue Apr 29 00:00:00 EDT 2008 · OSTI ID:1340292

Kitts, K; Choi, Y; Sutton, S R; +3 more

Related Subjects

36 MATERIALS SCIENCE
depth profile modeling
Genesis mission
implant quantification
solar wind fluence
X-ray standing wave analysis

Title: Discrimination and quantification of Fe and Ni abundances in Genesis solar wind implanted collectors using X-ray standing wave fluorescence yield depth profiling with internal referencing

Citation Formats

References (21)

Cited By (1)

Similar Records

Related Subjects