Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time

Zhang, Qingteng; Dufresne, Eric M.; Grybos, Pawel; Kmon, Piotr; Maj, Piotr; Narayanan, Suresh; Deptuch, Grzegorz W.; Szczygiel, Robert; Sandy, Alec

doi:10.1107/S1600577516005166

Title: Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time

Journal Article · Tue Apr 19 00:00:00 EDT 2016 · Journal of Synchrotron Radiation (Online)

DOI:https://doi.org/10.1107/S1600577516005166· OSTI ID:1326216

Zhang, Qingteng ^[1]; Dufresne, Eric M. ^[1]; Grybos, Pawel ^[2]; Kmon, Piotr ^[2]; Maj, Piotr ^[2]; Narayanan, Suresh ^[1]; Deptuch, Grzegorz W. ^[3]; Szczygiel, Robert ^[2]; Sandy, Alec ^[1]

Argonne National Lab. (ANL), Lemont, IL (United States)
AGH Univ. of Science and Technology, Krakow (Poland)
Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)

Small-angle scattering X-ray photon correlation spectroscopy (XPCS) studies were performed using a novel photon-counting pixel array detector with dual counters for each pixel. Each counter can be read out independently from the other to ensure there is no readout dead-time between the neighboring frames. A maximum frame rate of 11.8 kHz was achieved. Results on test samples show good agreement with simple diffusion. As a result, the potential of extending the time resolution of XPCS beyond the limit set by the detector frame rate using dual counters is also discussed.

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States); Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), High Energy Physics (HEP)

Grant/Contract Number:: AC02-06CH11357; AC02-07CH11359

OSTI ID:: 1326216

Alternate ID(s):: OSTI ID: 1333142

Report Number(s):: FERMILAB-PUB-16-530-PPD; JSYRES; 128033

Journal Information:: Journal of Synchrotron Radiation (Online), Vol. 23, Issue 3; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 21 works

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Dynamic Scaling of Colloidal Gel Formation at Intermediate Concentrations Zhang, Qingteng; Bahadur, Divya; Dufresne, Eric M. Physical Review Letters, Vol. 119, Issue 17 https://doi.org/10.1103/physrevlett.119.178006	journal	October 2017
Ultra-small-angle X-ray photon correlation spectroscopy using the Eiger detector Zinn, T.; Homs, A.; Sharpnack, L. Journal of Synchrotron Radiation, Vol. 25, Issue 6 https://doi.org/10.1107/s1600577518013899	journal	October 2018
Evolution of structure and dynamics of thermo-reversible nanoparticle gels—A combined XPCS and rheology study Bahadur, Divya; Zhang, Qingteng; Dufresne, Eric M. The Journal of Chemical Physics, Vol. 151, Issue 10 https://doi.org/10.1063/1.5111521	journal	September 2019
Sub-microsecond-resolved multi-speckle X-ray photon correlation spectroscopy with a pixel array detector Zhang, Qingteng; Dufresne, Eric M.; Narayanan, Suresh Journal of Synchrotron Radiation, Vol. 25, Issue 5 https://doi.org/10.1107/s1600577518009074	journal	August 2018

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Title: Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time

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