The stopped-drop method: a novel setup for containment-free and time-resolved measurements
Journal Article
·
· Journal of Synchrotron Radiation
A novel setup for containment-free time-resolved experiments at a free-hanging drop is reported. Within a dead-time of 100 ms a drop of mixed reactant solutions is formed and the time evolution of a reaction can be followed from thereon by various techniques. As an example, a small-angle X-ray scattering study on the formation mechanism of EDTA-stabilized CdS both at a synchrotron and a laboratory X-ray source is presented here. While the evolution can be followed with one drop only at a synchrotron source, a stroboscopic mode with many drops is preferable for the laboratory source.
- Research Organization:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Organization:
- USDOE Office of Science - Office of Basic Energy Sciences - Scientific User Facilities Division; Argonne National Laboratory - Advanced Photon Source; German Research Foundation (DFG)
- DOE Contract Number:
- AC02-06CH11357
- OSTI ID:
- 1254859
- Journal Information:
- Journal of Synchrotron Radiation, Vol. 23, Issue 2; ISSN 0909-0495
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
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