Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit

Dufresne, Eric M.; Narayanan, Suresh; Sandy, Alec R.; Kline, David M.; Zhang, Qingteng; Landahl, Eric C.; Ross, Steve

doi:10.1364/OE.24.000355

Title: Pushing x-ray photon correlation spectroscopy beyond the continuous frame rate limit

Journal Article · Wed Jan 06 00:00:00 EST 2016 · Optics Express

DOI:https://doi.org/10.1364/OE.24.000355· OSTI ID:1251156

Dufresne, Eric M. ^[1]; Narayanan, Suresh ^[1]; Sandy, Alec R. ^[1]; Kline, David M. ^[1]; Zhang, Qingteng ^[1]; Landahl, Eric C. ^[2]; Ross, Steve ^[3]

Argonne National Lab. (ANL), Argonne, IL (United States)
DePaul Univ., Chicago, IL (United States). Dept. of Physics
Northern Illinois Univ., DeKalb, IL (United States). Dept. of Electrical Engineering

We demonstrate delayed-frame X-ray Photon Correlation Spectroscopy with 120 microsecond time resolution, limited only by sample scattering rates, with a prototype Pixel-array detector capable of taking two image frames separated by 153 ns or less. Although the overall frame rate is currently limited to about 4 frame pairs per second, we easily measured millisecond correlation functions. In conclusion, this technology, coupled to the use of brighter synchrotrons such as Petra III or the NSLS-II should enable X-ray Photon Correlation Spectroscopy on microsecond time scales on a wider variety of materials.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division; USDOE Office of Science - Small Business Innovation Research (SBIR) and Small Business Technology Transfer (STTR) - Small Business Innovative Research Grant Program

Grant/Contract Number:: AC02-06CH11357; SC0004235

OSTI ID:: 1251156

Journal Information:: Optics Express, Vol. 24, Issue 1; ISSN 1094-4087

Publisher:: Optical Society of America (OSA)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 4 works

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Cited By (3)

Spatial and temporal pre-alignment of an X-ray split-and-delay unit by laser light interferometry Roseker, W.; Lee, S.; Walther, M. Review of Scientific Instruments, Vol. 90, Issue 4 https://doi.org/10.1063/1.5089496	journal	April 2019
Submillisecond X-ray photon correlation spectroscopy from a pixel array detector with fast dual gating and no readout dead-time Zhang, Qingteng; Dufresne, Eric M.; Grybos, Pawel Journal of Synchrotron Radiation, Vol. 23, Issue 3 https://doi.org/10.1107/s1600577516005166	journal	April 2016
Spatial and temporal pre-alignment of an X-ray split-and-delay unit by laser light interferometry Roseker, Wojciech; Lee, S.; Walther, Michael Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2019-01681	text	January 2019

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