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Title: Recent advances in small-scale mechanical property measurement by nanoindentation

Journal Article · · Current Opinion in Solid State and Materials Science
 [1]
  1. Univ. of Tennessee, Knoxville, TN (United States); Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Since its initial development in the early 1980’s [1], nanoindentation has matured into one of the premier testing techniques for measuring mechanical properties at the micrometer and sub-micrometer scales and has emerged as a critical tool that has helped to shape the nanotechnology revolution. At the heart of the technique are testing systems with simple but precise force actuators and displacement measuring devices that record the force–displacement record as a diamond indenter, usually the form of a pyramid or a sphere, is pressed into and withdrawn from a small region in the surface of a material of interest. The nano-scale force–displacement data, which can be obtained with a spatial resolution as small as a few nanometers, contains a wealth of information about the local mechanical properties [2], [3] and [4]. This enables the mechanical characterization of very thin films, like those used in the semiconductor, magnetic storage, and hard coatings industries, as well as very small precipitates, particles and second phases, many of which may not exist in bulk form and cannot be characterized by traditional mechanical testing methods. Here, computer automation of nanoindentation testing systems now routinely provides for complete two-dimensional mapping of properties over regions stretching from sub-micron to millimeters in scale.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Science (SC)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1242671
Alternate ID(s):
OSTI ID: 1251244
Journal Information:
Current Opinion in Solid State and Materials Science, Vol. 19, Issue 6; ISSN 1359-0286
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 6 works
Citation information provided by
Web of Science

References (9)

Hardness measurement at penetration depths as small as 20 nm journal April 1983
A method for interpreting the data from depth-sensing indentation instruments journal August 1986
An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments journal June 1992
Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology journal January 2004
High temperature nanoindentation: The state of the art and future challenges journal December 2015
Dynamic nanoindentation testing for studying thermally activated processes from single to nanocrystalline metals journal December 2015
Nanoindentation of viscoelastic solids: A critical assessment of experimental methods journal December 2015
Nanoindentation of hydrated materials and tissues journal December 2015
Measurement of fracture toughness by nanoindentation methods: Recent advances and future challenges journal December 2015

Cited By (1)


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