Shape Evolution and Single Particle Luminescence of Organometal Halide Perovskite Nanocrystals

Zhu, Feng; Men, Long; Guo, Yijun; Zhu, Qiaochu; Bhattacharjee, Ujjal; Goodwin, Peter M.; Petrich, Jacob W.; Smith, Emily A.; Vela, Javier

doi:10.1021/nn507020s

Title: Shape Evolution and Single Particle Luminescence of Organometal Halide Perovskite Nanocrystals

Journal Article · Mon Feb 09 00:00:00 EST 2015 · ACS Nano

DOI:https://doi.org/10.1021/nn507020s· OSTI ID:1226916

Zhu, Feng ^[1]; Men, Long ^[2]; Guo, Yijun ^[1]; Zhu, Qiaochu ^[1]; Bhattacharjee, Ujjal ^[2]; Goodwin, Peter M. ^[3]; Petrich, Jacob W. ^[2]; Smith, Emily A. ^[2]; Vela, Javier ^[2]

Iowa State Univ., Ames, IA (United States)
Iowa State Univ., Ames, IA (United States); Ames Lab., Ames, IA (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)

Organometallic halide perovskites CH₃NH₃PbX₃ (X = I, Br, Cl) have quickly become one of the most promising semiconductors for solar cells, with photovoltaics made of these materials reaching power conversion efficiencies of near 20%. Improving our ability to harness the full potential of organometal halide perovskites will require more controllable syntheses that permit a detailed understanding of their fundamental chemistry and photophysics. In our manuscript, we systematically synthesize CH₃NH₃PbX₃ (X = I, Br) nanocrystals with different morphologies (dots, rods, plates or sheets) by using different solvents and capping ligands. CH₃NH₃PbX₃ nanowires and nanorods capped with octylammonium halides show relatively higher photoluminescence (PL) quantum yields and long PL lifetimes. CH₃NH₃PbI₃ nanowires monitored at the single particle level show shape-correlated PL emission across whole particles, with little photobleaching observed and very few off periods. Our work highlights the potential of low-dimensional organometal halide perovskite semiconductors in constructing new porous and nanostructured solar cell architectures, as well as in applying these materials to other fields such as light-emitting devices and single particle imaging and tracking.

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Research Organization:: Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-07CH11358

OSTI ID:: 1226916

Report Number(s):: IS-J 8570

Journal Information:: ACS Nano, Vol. 9, Issue 3; ISSN 1936-0851

Publisher:: American Chemical SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 223 works

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Perovskite Thin Film Consisting with One-Dimensional Nanowires Li, Xinli; Chen, Yongchao; Li, Lihua Materials, Vol. 11, Issue 9 https://doi.org/10.3390/ma11091759	journal	September 2018
Top-Down Approaches Towards Single Crystal Perovskite Solar Cells Schlipf, Johannes; Askar, Abdelrahman M.; Pantle, Florian Scientific Reports, Vol. 8, Issue 1 https://doi.org/10.1038/s41598-018-23211-x	journal	March 2018
Ligand-free all-inorganic metal halide nanocubes for fast, ultra-sensitive and self-powered ozone sensors Brintakis, K.; Gagaoudakis, E.; Kostopoulou, A. Nanoscale Advances, Vol. 1, Issue 7 https://doi.org/10.1039/c9na00219g	journal	January 2019
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Swelling‐Deswelling Microencapsulation‐Enabled Ultrastable Perovskite−Polymer Composites for Photonic Applications He, Ziqian; He, Juan; Zhang, Caicai The Chemical Record, Vol. 20, Issue 7 https://doi.org/10.1002/tcr.201900074	journal	December 2019
An ultra-broadband perovskite-PbS quantum dot sensitized carbon nanotube photodetector Ka, Ibrahima; Gerlein, Luis F.; Asuo, Ivy M. Nanoscale, Vol. 10, Issue 19 https://doi.org/10.1039/c7nr08608c	journal	January 2018
Evolution of Photoluminescence, Raman, and Structure of CH3NH3PbI3 Perovskite Microwires Under Humidity Exposure Segovia, Rubén; Qu, Geyang; Peng, Miao Nanoscale Research Letters, Vol. 13, Issue 1 https://doi.org/10.1186/s11671-018-2470-0	journal	March 2018
High-quality CsPbBr ₃ perovskite nanocrystals for quantum dot light-emitting diodes Du, Xiafang; Wu, Guan; Cheng, Jian RSC Advances, Vol. 7, Issue 17 https://doi.org/10.1039/c6ra27665b	journal	January 2017
Luminescent perovskites: recent advances in theory and experiments Song, Zhen; Zhao, Jing; Liu, Quanlin Inorganic Chemistry Frontiers, Vol. 6, Issue 11 https://doi.org/10.1039/c9qi00777f	journal	January 2019
CsPbBr_3 perovskite quantum dots: saturable absorption properties and passively Q-switched visible lasers Li, Jingzhou; Dong, Hongxing; Xu, Bin Photonics Research, Vol. 5, Issue 5 https://doi.org/10.1364/prj.5.000457	journal	January 2017
Unveiling the Photo‐ and Thermal‐Stability of Cesium Lead Halide Perovskite Nanocrystals Boote, Brett W.; Andaraarachchi, Himashi P.; Rosales, Bryan A. ChemPhysChem, Vol. 20, Issue 20 https://doi.org/10.1002/cphc.201900432	journal	October 2019
The Luminescence of CH ₃ NH ₃ PbBr ₃ Perovskite Nanoparticles Crests the Summit and Their Photostability under Wet Conditions is Enhanced Gonzalez-Carrero, Soranyel; Francés-Soriano, Laura; González-Béjar, María Small, Vol. 12, Issue 38 https://doi.org/10.1002/smll.201600209	journal	August 2016
Revealing the Formation Mechanism of CsPbBr ₃ Perovskite Nanocrystals Produced via a Slowed-Down Microwave-Assisted Synthesis Li, Yanxiu; Huang, He; Xiong, Yuan Angewandte Chemie, Vol. 130, Issue 20 https://doi.org/10.1002/ange.201713332	journal	April 2018
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Enhancement in lifespan of halide perovskite solar cells Wang, Qiong; Phung, Nga; Di Girolamo, Diego Energy & Environmental Science, Vol. 12, Issue 3 https://doi.org/10.1039/c8ee02852d	journal	January 2019
Quantum confinement effect and exciton binding energy of layered perovskite nanoplatelets Wang, Qiang; Liu, Xiao-Dan; Qiu, Yun-Hang AIP Advances, Vol. 8, Issue 2 https://doi.org/10.1063/1.5020836	journal	February 2018
Ultrafast terahertz snapshots of excitonic Rydberg states and electronic coherence in an organometal halide perovskite Luo, Liang; Men, Long; Liu, Zhaoyu Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/ncomms15565	journal	June 2017
Direct TEM observation of the “acanthite α-Ag ₂ S–argentite β-Ag ₂ S” phase transition in a silver sulfide nanoparticle Sadovnikov, S. I.; Gerasimov, E. Yu. Nanoscale Advances, Vol. 1, Issue 4 https://doi.org/10.1039/c8na00347e	journal	January 2019
ZnO nanocrystals incorporating PEIE and a fluorene-based polyelectrolyte as electron transport layers for pure cesium-containing perovskite light-emitting devices Chang, Chun-Jung; Yang, Sheng-Hsiung Materials Research Express, Vol. 6, Issue 10 https://doi.org/10.1088/2053-1591/ab34d0	journal	August 2019
Light diffusing, down-converting perovskite-on-polymer microspheres Zhang, Caicai; He, Ziqian; Chen, Hao Journal of Materials Chemistry C, Vol. 7, Issue 22 https://doi.org/10.1039/c9tc01130g	journal	January 2019
Aligned Single-Crystalline Perovskite Microwire Arrays for High-Performance Flexible Image Sensors with Long-Term Stability Deng, Wei; Zhang, Xiujuan; Huang, Liming Advanced Materials, Vol. 28, Issue 11 https://doi.org/10.1002/adma.201505126	journal	January 2016
Perovskite nanocrystals: across-dimensional attachment, film-scale assembly on a flexible substrate and their fluorescence properties Huang, Wenyi; Liu, Jiajia; Bai, Bing Nanotechnology, Vol. 29, Issue 12 https://doi.org/10.1088/1361-6528/aaa806	journal	February 2018
Lead‐Free Semiconductors: Soft Chemistry, Dimensionality Control, and Manganese‐Doping of Germanium Halide Perovskites Men, Long; Rosales, Bryan A.; Gentry, Noreen E. ChemNanoMat, Vol. 5, Issue 3 https://doi.org/10.1002/cnma.201800497	journal	January 2019
A Microscale Perovskite as Single Component Broadband Phosphor for Downconversion White-Light-Emitting Devices Yuan, Zhao; Zhou, Chenkun; Messier, Joshua Advanced Optical Materials, Vol. 4, Issue 12 https://doi.org/10.1002/adom.201600667	journal	September 2016
1D Organic-Inorganic Hybrid Perovskite Micro/Nanocrystals: Fabrication, Assembly, and Optoelectronic Applications Xu, Xiuzhen; Zhang, Xiujuan; Deng, Wei Small Methods, Vol. 2, Issue 7 https://doi.org/10.1002/smtd.201700340	journal	April 2018
Imaging Heterogeneously Distributed Photo‐Active Traps in Perovskite Single Crystals Yuan, Haifeng; Debroye, Elke; Bladt, Eva Advanced Materials, Vol. 30, Issue 13 https://doi.org/10.1002/adma.201705494	journal	February 2018
Recent advances in controlling the crystallization of two-dimensional perovskites for optoelectronic device Luo, Shi-Qiang; Wang, Ji-Fei; Yang, Bin Frontiers of Physics, Vol. 14, Issue 5 https://doi.org/10.1007/s11467-019-0901-8	journal	May 2019
In situ inclusion of thiocyanate for highly luminescent and stable CH ₃ NH ₃ PbBr ₃ perovskite nanocrystals Cai, Tao; Li, Fan; Jiang, Yihua Nanoscale, Vol. 11, Issue 3 https://doi.org/10.1039/c8nr07987k	journal	January 2019
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Decorating Perovskite Quantum Dots in TiO ₂ Nanotubes Array for Broadband Response Photodetector Zheng, Zhi; Zhuge, Fuwei; Wang, Yaguang Advanced Functional Materials, Vol. 27, Issue 43 https://doi.org/10.1002/adfm.201703115	journal	September 2017
Compositional and Dimensional Control of 2D and Quasi‐2D Lead Halide Perovskites in Water Jana, Atanu; Ba, Qiankai; Kim, Kwang S. Advanced Functional Materials, Vol. 29, Issue 28 https://doi.org/10.1002/adfm.201900966	journal	May 2019
Tuning the Optical Properties of Perovskite Nanoplatelets through Composition and Thickness by Ligand-Assisted Exfoliation Hintermayr, Verena A.; Richter, Alexander F.; Ehrat, Florian Advanced Materials, Vol. 28, Issue 43 https://doi.org/10.1002/adma.201602897	journal	September 2016
Luminescent perovskite quantum dots: synthesis, microstructures, optical properties and applications Chen, Daqin; Chen, Xiao Journal of Materials Chemistry C, Vol. 7, Issue 6 https://doi.org/10.1039/c8tc05545a	journal	January 2019
Progress of Surface Science Studies on ABX ₃ ‐Based Metal Halide Perovskite Solar Cells Qiu, Longbin; He, Sisi; Ono, Luis K. Advanced Energy Materials, Vol. 10, Issue 13 https://doi.org/10.1002/aenm.201902726	journal	April 2020
Unconventional solution-phase epitaxial growth of organic-inorganic hybrid perovskite nanocrystals on metal sulfide nanosheets Zhang, Zhipeng; Sun, Fangfang; Zhu, Zhaohua Science China Materials, Vol. 62, Issue 1 https://doi.org/10.1007/s40843-018-9274-y	journal	May 2018
Tuning Charge Carrier Dynamics and Surface Passivation in Organolead Halide Perovskites with Capping Ligands and Metal Oxide Interfaces Godin, Robert; Ma, Xuerui; González-Carrero, Soranyel Advanced Optical Materials, Vol. 6, Issue 5 https://doi.org/10.1002/adom.201701203	journal	January 2018
Confining metal-halide perovskites in nanoporous thin films Demchyshyn, Stepan; Roemer, Janina Melanie; Groiß, Heiko Science Advances, Vol. 3, Issue 8 https://doi.org/10.1126/sciadv.1700738	journal	August 2017
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Perovskite Nanoparticles: Synthesis, Properties, and Novel Applications in Photovoltaics and LEDs Kulkarni, Sneha A.; Mhaisalkar, Subodh G.; Mathews, Nripan Small Methods, Vol. 3, Issue 1 https://doi.org/10.1002/smtd.201800231	journal	October 2018
Solvent Engineering Boosts the Efficiency of Paintable Carbon-Based Perovskite Solar Cells to Beyond 14% Chen, Haining; Wei, Zhanhua; He, Hexiang Advanced Energy Materials, Vol. 6, Issue 8 https://doi.org/10.1002/aenm.201502087	journal	January 2016
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Facile Synthesis of Methylammonium Lead Iodide Perovskite with Controllable Morphologies with Enhanced Luminescence Performance Wang, Tao; Zhang, Huafang; Hou, Sumin Nanomaterials, Vol. 9, Issue 12 https://doi.org/10.3390/nano9121660	journal	November 2019
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Quantifying the Thermodynamics of Ligand Binding to CsPbBr ₃ Quantum Dots Smock, Sara R.; Williams, Travis J.; Brutchey, Richard L. Angewandte Chemie, Vol. 130, Issue 36 https://doi.org/10.1002/ange.201806916	journal	August 2018
Organometal halide perovskite nanocrystals embedded in silicone resins with bright luminescence and ultrastability Wang, Hai; Lin, Hechun; Piao, Xianqing Journal of Materials Chemistry C, Vol. 5, Issue 46 https://doi.org/10.1039/c7tc04055e	journal	January 2017
Fabrication of Semiconducting Methylammonium Lead Halide Perovskite Particles by Spray Technology Ahmadian-Yazdi, Mohammad-Reza; Eslamian, Morteza Nanoscale Research Letters, Vol. 13, Issue 1 https://doi.org/10.1186/s11671-017-2430-0	journal	January 2018
Highly Luminescent Cesium Lead Halide Perovskite Nanocrystals with Tunable Composition and Thickness by Ultrasonication Tong, Yu; Bladt, Eva; Aygüler, Meltem F. Angewandte Chemie International Edition, Vol. 55, Issue 44 https://doi.org/10.1002/anie.201605909	journal	September 2016
Recent advances in one-dimensional halide perovskites for optoelectronic applications Qiu, Ting; Hu, Yanqiang; Xu, Feng Nanoscale, Vol. 10, Issue 45 https://doi.org/10.1039/c8nr05862h	journal	January 2018
Performance-Enhancing Broadband and Flexible Photodetectors Based on Perovskite/ZnO-Nanowire Hybrid Structures Gao, Ting; Zhang, Qi; Chen, Junnian Advanced Optical Materials, Vol. 5, Issue 12 https://doi.org/10.1002/adom.201700206	journal	May 2017
Synthesis of Lead‐free CsGeI ₃ Perovskite Colloidal Nanocrystals and Electron Beam‐induced Transformations Wu, Xiaotong; Song, Weidong; Li, Qian Chemistry – An Asian Journal, Vol. 13, Issue 13 https://doi.org/10.1002/asia.201800573	journal	May 2018
Crystal Structure Formation of CH3NH3PbI3-xClx Perovskite Luo, Shiqiang; Daoud, Walid Materials, Vol. 9, Issue 3 https://doi.org/10.3390/ma9030123	journal	February 2016
Verringerung schädlicher Defekte für leistungsstarke Metallhalogenid‐Perowskit‐Solarzellen Ono, Luis K.; Liu, Shengzhong (Frank); Qi, Yabing Angewandte Chemie, Vol. 132, Issue 17 https://doi.org/10.1002/ange.201905521	journal	April 2020
Analysing the effect of crystal size and structure in highly efficient CH ₃ NH ₃ PbI ₃ perovskite solar cells by spatially resolved photo- and electroluminescence imaging Mastroianni, S.; Heinz, F. D.; Im, J. -H. Nanoscale, Vol. 7, Issue 46 https://doi.org/10.1039/c5nr05308k	journal	January 2015
Confining metal-halide perovskites in nanoporous thin films Demchyshyn, Stepan; Roemer, Janina Melanie; Groiß, Heiko Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2017-10105	text	January 2017
Top-Down Approaches Towards Single Crystal Perovskite Solar Cells Müller-Buschbaum, Johannes Schlipf, Abdelrahman M. Askar, Florian Pantle, Benjamin D. Wiltshire, Anton Sura, Peter Schneider, Linus Huber, Karthik Shankar, Peter University of Alberta Libraries https://doi.org/10.7939/r3-rqba-ff33	text	January 2018
In Situ Transmission Electron Microscopy Study of Electron Beam-Induced Transformations in Colloidal Cesium Lead Halide Perovskite Nanocrystals Dang, Zhiya; Shamsi, Javad; Palazon, Francisco ACS Nano, Vol. 11, Issue 2 https://doi.org/10.1021/acsnano.6b08324	journal	February 2017
Exploration of Near-Infrared-Emissive Colloidal Multinary Lead Halide Perovskite Nanocrystals Using an Automated Microfluidic Platform Lignos, Ioannis; Morad, Viktoriia; Shynkarenko, Yevhen ACS Nano, Vol. 12, Issue 6 https://doi.org/10.1021/acsnano.8b01122	journal	May 2018
Photoluminescence Blinking of Single-Crystal Methylammonium Lead Iodide Perovskite Nanorods Induced by Surface Traps Yuan, Haifeng; Debroye, Elke; Caliandro, Giorgio ACS Omega, Vol. 1, Issue 1 https://doi.org/10.1021/acsomega.6b00107	journal	July 2016
Solution Synthesis Approach to Colloidal Cesium Lead Halide Perovskite Nanoplatelets with Monolayer-Level Thickness Control Akkerman, Quinten A.; Motti, Silvia Genaro; Srimath Kandada, Ajay Ram Journal of the American Chemical Society, Vol. 138, Issue 3 https://doi.org/10.1021/jacs.5b12124	journal	January 2016
Defect-induced local variation of crystal phase transition temperature in metal-halide perovskites Dobrovolsky, Alexander; Merdasa, Aboma; Unger, Eva L. Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/s41467-017-00058-w	journal	June 2017
Atomic scale insights into structure instability and decomposition pathway of methylammonium lead iodide perovskite Chen, Shulin; Zhang, Xiaowei; Zhao, Jinjin Nature Communications, Vol. 9, Issue 1 https://doi.org/10.1038/s41467-018-07177-y	journal	November 2018

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