Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography

Meirer, F.; Kalirai, S.; Weker, J. Nelson; Liu, Y.; Andrews, J. C.; Weckhuysen, B. M.

doi:10.1039/C5CC00401B

Title: Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography

Journal Article · Tue Apr 14 00:00:00 EDT 2015 · ChemComm

DOI:https://doi.org/10.1039/C5CC00401B· OSTI ID:1215407

Meirer, F. ^[1]; Kalirai, S. ^[1]; Weker, J. Nelson ^[2]; Liu, Y. ^[2]; Andrews, J. C. ^[2]; Weckhuysen, B. M. ^[1]

Utrecht Univ., Utrecht (The Netherlands)
SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States)

Metal accumulation at the catalyst particle surface plays a role in particle agglutination during fluid catalytic cracking.

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Research Organization:: SLAC National Accelerator Lab., Menlo Park, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC)

Grant/Contract Number:: 321140

OSTI ID:: 1215407

Journal Information:: ChemComm, Vol. 51, Issue 38; ISSN 1359-7345

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 35 works

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References (26)

Designing FCC catalysts with high-silica Y zeolites Scherzer, Julius Applied Catalysis, Vol. 75, Issue 1 https://doi.org/10.1016/S0166-9834(00)83119-X	journal	August 1991
Heterogeneities of individual catalyst particles in space and time as monitored by spectroscopy Buurmans, Inge L. C.; Weckhuysen, Bert M. Nature Chemistry, Vol. 4, Issue 11 https://doi.org/10.1038/nchem.1478	journal	October 2012
Hard and soft X-ray microscopy and tomography in catalysis: bridging the different time and length scales Grunwaldt, Jan-Dierk; Schroer, Christian G. Chemical Society Reviews, Vol. 39, Issue 12 https://doi.org/10.1039/c0cs00036a	journal	January 2010
Imaging Catalysts at Work: A Hierarchical Approach from the Macro- to the Meso- and Nano-scale Grunwaldt, Jan-Dierk; Wagner, Jakob B.; Dunin-Borkowski, Rafal E. ChemCatChem, Vol. 5, Issue 1 https://doi.org/10.1002/cctc.201200356	journal	November 2012
On the interaction of vanadium and nickel compounds with cracking catalyst Pompea, Robert; Järóasb, Sven; Vannerbergb, Nils-Gösta Applied Catalysis, Vol. 13, Issue 1 https://doi.org/10.1016/S0166-9834(00)83335-7	journal	December 1984
Vanadium passivation of cracking catalysts by imaging secondary ion mass spectrometry Chao, Kuei-Jung; Lin, Long-Hui; Ling, Yong-Chien Applied Catalysis A: General, Vol. 121, Issue 2 https://doi.org/10.1016/0926-860X(94)00217-7	journal	January 1995
Nickel and vanadium on equilibrium cracking catalysts by imaging secondary ion mass spectrometry Kugler, E. Journal of Catalysis, Vol. 109, Issue 2 https://doi.org/10.1016/0021-9517(88)90221-7	journal	February 1988
Mapping Metals Incorporation of a Whole Single Catalyst Particle Using Element Specific X-ray Nanotomography Meirer, Florian; Morris, Darius T.; Kalirai, Sam Journal of the American Chemical Society, Vol. 137, Issue 1 https://doi.org/10.1021/ja511503d	journal	January 2015
Life and death of a single catalytic cracking particle Meirer, Florian; Kalirai, Sam; Morris, Darius Science Advances, Vol. 1, Issue 3 https://doi.org/10.1126/sciadv.1400199	journal	April 2015
Assessment of the 3 D Pore Structure and Individual Components of Preshaped Catalyst Bodies by X-Ray Imaging da Silva, Julio C.; Mader, Kevin; Holler, Mirko ChemCatChem, Vol. 7, Issue 3 https://doi.org/10.1002/cctc.201402925	journal	December 2014
Back Cover: Characterization of a Fluidized Catalytic Cracking Catalyst on Ensemble and Individual Particle Level by X-ray Micro- and Nanotomography, Micro-X-ray Fluorescence, and Micro-X-ray Diffraction (ChemCatChem 5/2014) Bare, Simon R.; Charochak, Meghan E.; Kelly, Shelly D. ChemCatChem, Vol. 6, Issue 5 https://doi.org/10.1002/cctc.201490033	journal	May 2014
Chemical imaging of catalytic solids with synchrotron radiation Beale, Andrew M.; Jacques, Simon D. M.; Weckhuysen, Bert M. Chemical Society Reviews, Vol. 39, Issue 12 https://doi.org/10.1039/c0cs00089b	journal	January 2010
Phase retrieval using polychromatic illumination for transmission X-ray microscopy Liu, Yijin; Andrews, Joy C.; Wang, Junyue Optics Express, Vol. 19, Issue 2 https://doi.org/10.1364/OE.19.000540	journal	January 2011
Hard X-ray Spectroscopic Nano-Imaging of Hierarchical Functional Materials at Work Andrews, Joy C.; Weckhuysen, Bert M. ChemPhysChem, Vol. 14, Issue 16 https://doi.org/10.1002/cphc.201300529	journal	September 2013
TXM-Wizard : a program for advanced data collection and evaluation in full-field transmission X-ray microscopy Liu, Yijin; Meirer, Florian; Williams, Phillip A. Journal of Synchrotron Radiation, Vol. 19, Issue 2 https://doi.org/10.1107/S0909049511049144	journal	January 2012
X-ray ptychographic computed tomography at 16 nm isotropic 3D resolution Holler, M.; Diaz, A.; Guizar-Sicairos, M. Scientific Reports, Vol. 4, Issue 1 https://doi.org/10.1038/srep03857	journal	January 2014
Fourier ring correlation as a resolution criterion for super-resolution microscopy Banterle, Niccolò; Bui, Khanh Huy; Lemke, Edward A. Journal of Structural Biology, Vol. 183, Issue 3 https://doi.org/10.1016/j.jsb.2013.05.004	journal	September 2013
3D elemental sensitive imaging using transmission X-ray microscopy Liu, Yijin; Meirer, Florian; Wang, Junyue Analytical and Bioanalytical Chemistry, Vol. 404, Issue 5 https://doi.org/10.1007/s00216-012-5818-9	journal	February 2012
Nanoscale elemental sensitivity study of Nd ₂ Fe ₁₄ B using absorption correlation tomography : Nanoscale Elemental Sensitivity Study of N Kao, Thomas L.; Shi, Crystal Y.; Wang, Junyue Microscopy Research and Technique, Vol. 76, Issue 11 https://doi.org/10.1002/jemt.22273	journal	August 2013
Study of the accessibility effect on the irreversible deactivation of FCC catalysts from contaminant feed metals Psarras, A. C.; Iliopoulou, E. F.; Nalbandian, L. Catalysis Today, Vol. 127, Issue 1-4 https://doi.org/10.1016/j.cattod.2007.05.021	journal	September 2007
Visualization of the Equilibrium FCC Catalyst Surface by AFM and SEM–EDS Bayraktar, Oguz; Kugler, Edwin L. Catalysis Letters, Vol. 90, Issue 3/4 https://doi.org/10.1023/B:CATL.0000004110.98820.d9	journal	October 2003
Nanoscale Morphological and Chemical Changes of High Voltage Lithium–Manganese Rich NMC Composite Cathodes with Cycling Yang, Feifei; Liu, Yijin; Martha, Surendra K. Nano Letters, Vol. 14, Issue 8 https://doi.org/10.1021/nl502090z	journal	July 2014
Hydrodynamics of a gas–solid fluidized bed with thermally induced interparticle forces Shabanian, Jaber; Chaouki, Jamal Chemical Engineering Journal, Vol. 259 https://doi.org/10.1016/j.cej.2014.07.117	journal	January 2015
High-speed tracking of rupture and clustering in freely falling granular streams Royer, John R.; Evans, Daniel J.; Oyarte, Loreto Nature, Vol. 459, Issue 7250 https://doi.org/10.1038/nature08115	journal	June 2009
Particle cluster dynamics during fluidization McMillan, Jennifer; Shaffer, Frank; Gopalan, Balaji Chemical Engineering Science, Vol. 100 https://doi.org/10.1016/j.ces.2013.02.047	journal	August 2013
The influence of interparticle forces on the fluidization behaviour of some industrial materials at high temperature Lettieri, P.; Yates, J. G.; Newton, D. Powder Technology, Vol. 110, Issue 1-2 https://doi.org/10.1016/S0032-5910(99)00274-0	journal	May 2000

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Magnetophoretic Sorting of Single Catalyst Particles Solsona, Miguel; Nieuwelink, Anne‐Eva; Meirer, Florian Angewandte Chemie International Edition, Vol. 57, Issue 33 https://doi.org/10.1002/anie.201804942	journal	August 2018
Nickel Poisoning of a Cracking Catalyst Unravelled by Single‐Particle X‐ray Fluorescence‐Diffraction‐Absorption Tomography Gambino, Marianna; Veselý, Martin; Filez, Matthias Angewandte Chemie International Edition, Vol. 59, Issue 10 https://doi.org/10.1002/anie.201914950	journal	January 2020
Accurate 3D Characterization of Catalytic Bodies Surface by Scanning Electron Microscopy Gontard, Lionel C.; Cauqui, Miguel Ángel; Yeste, María Pilar ChemCatChem, Vol. 11, Issue 14 https://doi.org/10.1002/cctc.201900659	journal	June 2019
Spatial and temporal exploration of heterogeneous catalysts with synchrotron radiation Meirer, Florian; Weckhuysen, Bert M. Nature Reviews Materials, Vol. 3, Issue 9 https://doi.org/10.1038/s41578-018-0044-5	journal	August 2018
Transformations of FCC catalysts and carbonaceous deposits during repeated reaction-regeneration cycles Almas, Qandeel; Naeem, Muhammad Awais; Baldanza, Maria Auxiliadora S. Catalysis Science & Technology, Vol. 9, Issue 24 https://doi.org/10.1039/c9cy01680e	journal	January 2019
Microfluidics and catalyst particles Solsona, M.; Vollenbroek, J. C.; Tregouet, C. B. M. Lab on a Chip, Vol. 19, Issue 21 https://doi.org/10.1039/c9lc00318e	journal	January 2019
Fluid catalytic cracking technology: current status and recent discoveries on catalyst contamination Bai, Peng; Etim, Ubong Jerome; Yan, Zifeng Catalysis Reviews, Vol. 61, Issue 3 https://doi.org/10.1080/01614940.2018.1549011	journal	December 2018
Chemical imaging of Fischer-Tropsch catalysts under operating conditions Price, Stephen W. T.; Martin, David J.; Parsons, Aaron D. Science Advances, Vol. 3, Issue 3 https://doi.org/10.1126/sciadv.1602838	journal	March 2017
Magnetophoretic Sorting of Single Catalyst Particles Solsona, Miguel; Nieuwelink, Anne‐Eva; Meirer, Florian Angewandte Chemie, Vol. 130, Issue 33 https://doi.org/10.1002/ange.201804942	journal	August 2018

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