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Title: Microwave-assisted synthesis of transition metal phosphide

A method of synthesizing transition metal phosphide. In one embodiment, the method has the steps of preparing a transition metal lignosulfonate, mixing the transition metal lignosulfonate with phosphoric acid to form a mixture, and subjecting the mixture to a microwave radiation for a duration of time effective to obtain a transition metal phosphide.
Authors:
Publication Date:
OSTI Identifier:
1166767
Report Number(s):
8,920,688
12/754,336
DOE Contract Number:
FC-3606G086072
Resource Type:
Patent
Research Org:
Board of Trustees of the University of Arkansas, Little Rock, AR (United States)
Sponsoring Org:
USDOE
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY