Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition

Sunny, Steffi; Vogel, Nicolas; Howell, Caitlin; Vu, Thy L.; Aizenberg, Joanna

doi:10.1002/adfm.201401289

Title: Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition

Abstract

Omniphobic coatings are designed to repel a wide range of liquids without leaving stains on the surface. A practical coating should exhibit stable repellency, show no interference with color or transparency of the underlying substrate and, ideally, be deposited in a simple process on arbitrarily shaped surfaces. We use layer-by-layer (LbL) deposition of negatively charged silica nanoparticles and positively charged polyelectrolytes to create nanoscale surface structures that are further surface-functionalized with fluorinated silanes and infiltrated with fluorinated oil, forming a smooth, highly repellent coating on surfaces of different materials and shapes. We show that four or more LbL cycles introduce sufficient surface roughness to effectively immobilize the lubricant into the nanoporous coating and provide a stable liquid interface that repels water, low-surface-tension liquids and complex fluids. The absence of hierarchical structures and the small size of the silica nanoparticles enables complete transparency of the coating, with light transmittance exceeding that of normal glass. The coating is mechanically robust, maintains its repellency after exposure to continuous flow for several days and prevents adsorption of streptavidin as a model protein. As a result, the LbL process is conceptually simple, of low cost, environmentally benign, scalable, automatable and therefore may present an efficientmore »« less

Authors:

Sunny, Steffi ^[1]; Vogel, Nicolas ^[1]; Howell, Caitlin ^[1]; Vu, Thy L. ^[1]; Aizenberg, Joanna ^[1]

Harvard Univ., Cambridge MA (United States)

Publication Date:: Mon Sep 01 00:00:00 EDT 2014

Research Org.:: Harvard Univ., Cambridge, MA (United States)

Sponsoring Org.:: USDOE Advanced Research Projects Agency - Energy (ARPA-E)

OSTI Identifier:: 1163858

Report Number(s):: DOE-HARVARD-AR0000326-7
Journal ID: ISSN 1616-301X; DOE-HARVARD-AR0000326-7

Grant/Contract Number:: AR0000326

Resource Type:: Journal Article: Accepted Manuscript

Journal Name:: Advanced Functional Materials

Additional Journal Information:: Journal Volume: 24; Journal Issue: 42; Journal ID: ISSN 1616-301X

Publisher:: Wiley

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; colloids; layer-by-layer; nanostructures; wetting; omniphobicity

Citation Formats


                    Sunny, Steffi, Vogel, Nicolas, Howell, Caitlin, Vu, Thy L., and Aizenberg, Joanna. Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition.  United States: N. p., 2014. 
        Web.  doi:10.1002/adfm.201401289.

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                    Sunny, Steffi, Vogel, Nicolas, Howell, Caitlin, Vu, Thy L., & Aizenberg, Joanna. Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition.  United States.  https://doi.org/10.1002/adfm.201401289

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                    Sunny, Steffi, Vogel, Nicolas, Howell, Caitlin, Vu, Thy L., and Aizenberg, Joanna. 2014.  
        "Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition".  United States.  https://doi.org/10.1002/adfm.201401289.  https://www.osti.gov/servlets/purl/1163858.

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@article{osti_1163858,

  title        = {Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition},

  author       = {Sunny, Steffi and Vogel, Nicolas and Howell, Caitlin and Vu, Thy L. and Aizenberg, Joanna},

  abstractNote = {Omniphobic coatings are designed to repel a wide range of liquids without leaving stains on the surface. A practical coating should exhibit stable repellency, show no interference with color or transparency of the underlying substrate and, ideally, be deposited in a simple process on arbitrarily shaped surfaces. We use layer-by-layer (LbL) deposition of negatively charged silica nanoparticles and positively charged polyelectrolytes to create nanoscale surface structures that are further surface-functionalized with fluorinated silanes and infiltrated with fluorinated oil, forming a smooth, highly repellent coating on surfaces of different materials and shapes. We show that four or more LbL cycles introduce sufficient surface roughness to effectively immobilize the lubricant into the nanoporous coating and provide a stable liquid interface that repels water, low-surface-tension liquids and complex fluids. The absence of hierarchical structures and the small size of the silica nanoparticles enables complete transparency of the coating, with light transmittance exceeding that of normal glass. The coating is mechanically robust, maintains its repellency after exposure to continuous flow for several days and prevents adsorption of streptavidin as a model protein. As a result, the LbL process is conceptually simple, of low cost, environmentally benign, scalable, automatable and therefore may present an efficient synthetic route to non-fouling materials.},

  doi          = {10.1002/adfm.201401289},

  url          = {https://www.osti.gov/biblio/1163858},
  journal      = {Advanced Functional Materials},

  issn         = {1616-301X},

  number       = 42,

  volume       = 24,

  place        = {United States},

  year         = {Mon Sep 01 00:00:00 EDT 2014},

  month        = {Mon Sep 01 00:00:00 EDT 2014}

}

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https://doi.org/10.1177/1535370216640942

Drop impact dynamics on slippery liquid-infused porous surfaces: influence of oil thickness
text, January 2018

Muschi, M.; Brudieu, B.; Teisseire, J.
arXiv
https://doi.org/10.48550/arxiv.1801.05200

Double-sided slippery liquid-infused porous materials using conformable mesh
journal, September 2019

Geraldi, Nicasio R.; Guan, Jian H.; Dodd, Linzi E.
Scientific Reports, Vol. 9, Issue 1
https://doi.org/10.1038/s41598-019-49887-3

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Title: Lubricant-infused nanoparticulate coatings assembled by layer-by-layer deposition

Abstract

Citation Formats

Designing Superoleophobic Surfaces journal, December 2007

Robust omniphobic surfaces journal, November 2008

Effect of Surface Wettability on the Adsorption of Proteins and Detergents journal, April 1998

Device‐Associated Infections: A Macroproblem that Starts with Microadherence journal, November 2001

Bacterial flagella explore microscale hummocks and hollows to increase adhesion journal, March 2013

Purity of the sacred lotus, or escape from contamination in biological surfaces journal, April 1997

Super-Hydrophobic Surfaces: From Natural to Artificial journal, December 2002

Non-sticking drops journal, September 2005

Design and Creation of Superwetting/Antiwetting Surfaces journal, December 2006

Natural and biomimetic artificial surfaces for superhydrophobicity, self-cleaning, low adhesion, and drag reduction journal, January 2011

Candle Soot as a Template for a Transparent Robust Superamphiphobic Coating journal, December 2011

Metastable Underwater Superhydrophobicity journal, October 2010

Superhydrophobic Tracks for Low-Friction, Guided Transport of Water Droplets journal, April 2011

Switchable Static and Dynamic Self-Assembly of Magnetic Droplets on Superhydrophobic Surfaces journal, July 2013

Transparent Superhydrophobic Films Based on Silica Nanoparticles journal, June 2007

Stable Superhydrophobic Coatings from Polyelectrolyte Multilayers journal, July 2004

All-Nanoparticle Thin-Film Coatings journal, October 2006

Fuzzy Nanoassemblies: Toward Layered Polymeric Multicomposites journal, August 1997

Buildup of ultrathin multilayer films by a self-assembly process: III. Consecutively alternating adsorption of anionic and cationic polyelectrolytes on charged surfaces journal, April 1992

Nanoengineering of Particle Surfaces journal, January 2001

Form and Function in Multilayer Assembly: New Applications at the Nanoscale journal, August 2004

Biomedical Applications of Layer-by-Layer Assembly: From Biomimetics to Tissue Engineering journal, December 2006

Layer-by-layer assembly as a versatile bottom-up nanofabrication technique for exploratory research and realistic application journal, January 2007

Layer-by-Layer Assembly of Nanowires for Three-Dimensional, Multifunctional Electronics journal, March 2007

Template Synthesis of Nanostructured Materials via Layer-by-Layer Assembly † journal, February 2008

Building biomedical materials layer-by-layer journal, May 2012

The architecture and biological performance of drug-loaded LbL nanoparticles journal, July 2013

Spray-Layer-by-Layer Carbon Nanotube/Electrospun Fiber Electrodes for Flexible Chemiresistive Sensor Applications journal, September 2013

Bioinspired self-repairing slippery surfaces with pressure-stable omniphobicity journal, September 2011

Liquid-infused structured surfaces with exceptional anti-biofouling performance journal, July 2012

Hydrophobic Liquid-Infused Porous Polymer Surfaces for Antibacterial Applications journal, July 2013

Liquid-Infused Nanostructured Surfaces with Extreme Anti-Ice and Anti-Frost Performance journal, June 2012

Mechanism of Frost Formation on Lubricant-Impregnated Surfaces journal, April 2013

Robust Prototypical Anti-icing Coatings with a Self-lubricating Liquid Water Layer between Ice and Substrate journal, May 2013

Adaptive fluid-infused porous films with tunable transparency and wettability journal, April 2013

Nanochromatography Driven by the Coffee Ring Effect journal, March 2011

Lubricant-infused micro/nano-structured surfaces with tunable dynamic omniphobicity at high temperatures journal, June 2013

Enhanced Condensation on Lubricant-Impregnated Nanotextured Surfaces journal, October 2012

Immersion Condensation on Oil-Infused Heterogeneous Surfaces for Enhanced Heat Transfer journal, June 2013

Slippery Liquid-Infused Porous Surfaces Showing Marine Antibiofouling Properties journal, October 2013

Hierarchical or Not? Effect of the Length Scale and Hierarchy of the Surface Roughness on Omniphobicity of Lubricant-Infused Substrates journal, March 2013

Perfluoropolyether-infused nano-texture: a versatile approach to omniphobic coatings with low hysteresis and high transparency journal, January 2013

Gold peroxide complexes and the conversion of hydroperoxides into gold hydrides by successive oxygen-transfer reactions journal, July 2013

Resistance Of Solid Surfaces To Wetting By Water journal, August 1936

Wettability of porous surfaces journal, January 1944

Omniphobic Slippery Coatings Based on Lubricant-Infused Porous Polyelectrolyte Multilayers journal, August 2013

Nanoprotective Layer-by-Layer Coatings with Epoxy Components for Enhancing Abrasion Resistance: Toward Robust Multimaterial Nanoscale Films journal, September 2013

Alternately Assembled Ultrathin Film of Silica Nanoparticles and Linear Polycations journal, February 1997

Hydrothermal Treatment of Nanoparticle Thin Films for Enhanced Mechanical Durability journal, March 2008

Verwendung von Schwingquarzen zur W�gung d�nner Schichten und zur Mikrow�gung journal, April 1959

Layer-by-Layer-Assembled High-Performance Broadband Antireflection Coatings journal, February 2010

Facile Method to Fabricate Raspberry-like Particulate Films for Superhydrophobic Surfaces journal, December 2007

Corrosion-Resistant Superhydrophobic Coatings on Mg Alloy Surfaces Inspired by Lotus Seedpod journal, January 2017

Oil-Impregnated Nanoporous Oxide Layer for Corrosion Protection with Self-Healing journal, February 2017

Lubricant-Infused Anisotropic Porous Surface Design of Reduced Graphene Oxide Toward Electrically Driven Smart Control of Conductive Droplets' Motion journal, April 2017

Bioinspired Superwettability Micro/Nanoarchitectures: Fabrications and Applications journal, January 2019

External Stimuli Responsive Liquid‐Infused Surfaces Switching between Slippery and Nonslippery States: Fabrications and Applications journal, January 2020

Designing Liquid‐Infused Surfaces for Medical Applications: A Review journal, August 2018

Bio-Inspired Superhydrophobic and Omniphobic Wood Surfaces journal, November 2016

Conductive Electrochemically Active Lubricant-Infused Nanostructured Surfaces Attenuate Coagulation and Enable Friction-Less Droplet Manipulation journal, July 2018

Self‐Supplying Liquidity Oil‐Adsorbed Slippery Smooth Surface for Both Liquid and Solid Repellency journal, December 2019

Slippery Surface Based on Photoelectric Responsive Nanoporous Composites with Optimal Wettability Region for Droplets' Multifunctional Manipulation journal, November 2018

Emerging Applications of Bioinspired Slippery Surfaces in Biomedical Fields journal, July 2018

Biomimetic Self‐Cleaning Anisotropic Solid Slippery Surface with Excellent Stability and Restoration journal, March 2019

Recent Development of Durable and Self-Healing Surfaces with Special Wettability journal, February 2016

Facile preparation of superhydrophobic and oleophobic surfaces via the combination of Cu(0)-mediated reversible-deactivation radical polymerization and click chemistry journal, June 2018

Effect of the texture geometry on the slippery behavior of liquid-infused nanoporous surfaces journal, October 2018

Design of anti-icing surfaces: smooth, textured or slippery? journal, January 2016

Oil-Impregnated Hydrocarbon-Based Polymer Films journal, August 2018

A New Method for Intense Cavitation Bubble Generation on Layer-by-Layer Assembled SLIPS journal, August 2019

Double-sided slippery liquid-infused porous materials using conformable mesh journal, September 2019

A colloidoscope of colloid-based porous materials and their uses journal, January 2016

Slippery liquid-infused substrates: a versatile preparation, unique anti-wetting and drag-reduction effect on water journal, January 2016

Bio-inspired photonic crystals with superwettability journal, January 2016

Drop impact dynamics on slippery liquid-infused porous surfaces: influence of oil thickness journal, January 2018

Recent advances of bioinspired functional materials with specific wettability: from nature and beyond nature journal, January 2019

Biomimetic self-slippery and transferable transparent lubricant-infused functional surfaces journal, January 2018

Designing Superoleophobic Surfaces
journal, December 2007

Robust omniphobic surfaces
journal, November 2008

Effect of Surface Wettability on the Adsorption of Proteins and Detergents
journal, April 1998

Device‐Associated Infections: A Macroproblem that Starts with Microadherence
journal, November 2001

Bacterial flagella explore microscale hummocks and hollows to increase adhesion
journal, March 2013

Purity of the sacred lotus, or escape from contamination in biological surfaces
journal, April 1997

Super-Hydrophobic Surfaces: From Natural to Artificial
journal, December 2002

Non-sticking drops
journal, September 2005

Design and Creation of Superwetting/Antiwetting Surfaces
journal, December 2006

Natural and biomimetic artificial surfaces for superhydrophobicity, self-cleaning, low adhesion, and drag reduction
journal, January 2011

Candle Soot as a Template for a Transparent Robust Superamphiphobic Coating
journal, December 2011

Metastable Underwater Superhydrophobicity
journal, October 2010

Superhydrophobic Tracks for Low-Friction, Guided Transport of Water Droplets
journal, April 2011

Switchable Static and Dynamic Self-Assembly of Magnetic Droplets on Superhydrophobic Surfaces
journal, July 2013

Transparent Superhydrophobic Films Based on Silica Nanoparticles
journal, June 2007

Stable Superhydrophobic Coatings from Polyelectrolyte Multilayers
journal, July 2004

All-Nanoparticle Thin-Film Coatings
journal, October 2006

Fuzzy Nanoassemblies: Toward Layered Polymeric Multicomposites
journal, August 1997

Buildup of ultrathin multilayer films by a self-assembly process: III. Consecutively alternating adsorption of anionic and cationic polyelectrolytes on charged surfaces
journal, April 1992

Nanoengineering of Particle Surfaces
journal, January 2001

Form and Function in Multilayer Assembly: New Applications at the Nanoscale
journal, August 2004

Biomedical Applications of Layer-by-Layer Assembly: From Biomimetics to Tissue Engineering
journal, December 2006

Layer-by-layer assembly as a versatile bottom-up nanofabrication technique for exploratory research and realistic application
journal, January 2007

Layer-by-Layer Assembly of Nanowires for Three-Dimensional, Multifunctional Electronics
journal, March 2007

Template Synthesis of Nanostructured Materials via Layer-by-Layer Assembly ^†
journal, February 2008

Building biomedical materials layer-by-layer
journal, May 2012

The architecture and biological performance of drug-loaded LbL nanoparticles
journal, July 2013

Spray-Layer-by-Layer Carbon Nanotube/Electrospun Fiber Electrodes for Flexible Chemiresistive Sensor Applications
journal, September 2013

Bioinspired self-repairing slippery surfaces with pressure-stable omniphobicity
journal, September 2011

Liquid-infused structured surfaces with exceptional anti-biofouling performance
journal, July 2012

Hydrophobic Liquid-Infused Porous Polymer Surfaces for Antibacterial Applications
journal, July 2013

Liquid-Infused Nanostructured Surfaces with Extreme Anti-Ice and Anti-Frost Performance
journal, June 2012

Mechanism of Frost Formation on Lubricant-Impregnated Surfaces
journal, April 2013

Robust Prototypical Anti-icing Coatings with a Self-lubricating Liquid Water Layer between Ice and Substrate
journal, May 2013

Adaptive fluid-infused porous films with tunable transparency and wettability
journal, April 2013

Nanochromatography Driven by the Coffee Ring Effect
journal, March 2011

Lubricant-infused micro/nano-structured surfaces with tunable dynamic omniphobicity at high temperatures
journal, June 2013

Enhanced Condensation on Lubricant-Impregnated Nanotextured Surfaces
journal, October 2012

Immersion Condensation on Oil-Infused Heterogeneous Surfaces for Enhanced Heat Transfer
journal, June 2013

Slippery Liquid-Infused Porous Surfaces Showing Marine Antibiofouling Properties
journal, October 2013

Hierarchical or Not? Effect of the Length Scale and Hierarchy of the Surface Roughness on Omniphobicity of Lubricant-Infused Substrates
journal, March 2013

Perfluoropolyether-infused nano-texture: a versatile approach to omniphobic coatings with low hysteresis and high transparency
journal, January 2013

Gold peroxide complexes and the conversion of hydroperoxides into gold hydrides by successive oxygen-transfer reactions
journal, July 2013

Resistance Of Solid Surfaces To Wetting By Water
journal, August 1936

Wettability of porous surfaces
journal, January 1944

Omniphobic Slippery Coatings Based on Lubricant-Infused Porous Polyelectrolyte Multilayers
journal, August 2013

Nanoprotective Layer-by-Layer Coatings with Epoxy Components for Enhancing Abrasion Resistance: Toward Robust Multimaterial Nanoscale Films
journal, September 2013

Alternately Assembled Ultrathin Film of Silica Nanoparticles and Linear Polycations
journal, February 1997

Hydrothermal Treatment of Nanoparticle Thin Films for Enhanced Mechanical Durability
journal, March 2008

Verwendung von Schwingquarzen zur W�gung d�nner Schichten und zur Mikrow�gung
journal, April 1959

Layer-by-Layer-Assembled High-Performance Broadband Antireflection Coatings
journal, February 2010

Facile Method to Fabricate Raspberry-like Particulate Films for Superhydrophobic Surfaces
journal, December 2007

Corrosion-Resistant Superhydrophobic Coatings on Mg Alloy Surfaces Inspired by Lotus Seedpod
journal, January 2017

Oil-Impregnated Nanoporous Oxide Layer for Corrosion Protection with Self-Healing
journal, February 2017

Lubricant-Infused Anisotropic Porous Surface Design of Reduced Graphene Oxide Toward Electrically Driven Smart Control of Conductive Droplets' Motion
journal, April 2017

Bioinspired Superwettability Micro/Nanoarchitectures: Fabrications and Applications
journal, January 2019

External Stimuli Responsive Liquid‐Infused Surfaces Switching between Slippery and Nonslippery States: Fabrications and Applications
journal, January 2020

Designing Liquid‐Infused Surfaces for Medical Applications: A Review
journal, August 2018

Bio-Inspired Superhydrophobic and Omniphobic Wood Surfaces
journal, November 2016

Conductive Electrochemically Active Lubricant-Infused Nanostructured Surfaces Attenuate Coagulation and Enable Friction-Less Droplet Manipulation
journal, July 2018

Self‐Supplying Liquidity Oil‐Adsorbed Slippery Smooth Surface for Both Liquid and Solid Repellency
journal, December 2019

Slippery Surface Based on Photoelectric Responsive Nanoporous Composites with Optimal Wettability Region for Droplets' Multifunctional Manipulation
journal, November 2018

Emerging Applications of Bioinspired Slippery Surfaces in Biomedical Fields
journal, July 2018

Biomimetic Self‐Cleaning Anisotropic Solid Slippery Surface with Excellent Stability and Restoration
journal, March 2019

Recent Development of Durable and Self-Healing Surfaces with Special Wettability
journal, February 2016

Facile preparation of superhydrophobic and oleophobic surfaces via the combination of Cu(0)-mediated reversible-deactivation radical polymerization and click chemistry
journal, June 2018

Effect of the texture geometry on the slippery behavior of liquid-infused nanoporous surfaces
journal, October 2018

Design of anti-icing surfaces: smooth, textured or slippery?
journal, January 2016

Oil-Impregnated Hydrocarbon-Based Polymer Films
journal, August 2018

A New Method for Intense Cavitation Bubble Generation on Layer-by-Layer Assembled SLIPS
journal, August 2019

Double-sided slippery liquid-infused porous materials using conformable mesh
journal, September 2019

A colloidoscope of colloid-based porous materials and their uses
journal, January 2016

Slippery liquid-infused substrates: a versatile preparation, unique anti-wetting and drag-reduction effect on water
journal, January 2016

Bio-inspired photonic crystals with superwettability
journal, January 2016

Drop impact dynamics on slippery liquid-infused porous surfaces: influence of oil thickness
journal, January 2018

Recent advances of bioinspired functional materials with specific wettability: from nature and beyond nature
journal, January 2019

Biomimetic self-slippery and transferable transparent lubricant-infused functional surfaces
journal, January 2018

A stable solid slippery surface with thermally assisted self-healing ability
journal, January 2018

Sustained delivery of growth factors with high loading efficiency in a layer by layer assembly
journal, January 2020

Fabrication of biocompatible super stable lubricant-immobilized slippery surfaces by grafting a polydimethylsiloxane brush: excellent boiling water resistance, hot liquid repellency and long-term slippery stability
journal, January 2019