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Title: Mass independent kinetic energy reducing inlet system for vacuum environment

Patent ·
OSTI ID:1131018

A particle inlet system comprises a first chamber having a limiting orifice for an incoming gas stream and a micrometer controlled expansion slit. Lateral components of the momentum of the particles are substantially cancelled due to symmetry of the configuration once the laminar flow converges at the expansion slit. The particles and flow into a second chamber, which is maintained at a lower pressure than the first chamber, and then moves into a third chamber including multipole guides for electromagnetically confining the particle. The vertical momentum of the particles descending through the center of the third chamber is minimized as an upward stream of gases reduces the downward momentum of the particles. The translational kinetic energy of the particles is near-zero irrespective of the mass of the particles at an exit opening of the third chamber, which may be advantageously employed to provide enhanced mass resolution in mass spectrometry.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-00OR22725
Assignee:
UT-Battelle, LLC (Oak Ridge, TN)
Patent Number(s):
8,723,105
Application Number:
14/067,352
OSTI ID:
1131018
Resource Relation:
Patent File Date: 2013 Oct 30
Country of Publication:
United States
Language:
English

References (12)

Apparatus for analyzing trace components patent May 1977
Method of separating condensible vapors from particles in highly compressed gases patent October 1990
Mass spectrometer system including an ion source operable under high pressure conditions, and a two-stage pumping arrangement patent November 1992
Ion source for mass analyzer patent March 2004
Atmospheric and vacuum pressure MALDI ion source patent March 2004
Ultra high mass range mass spectrometer systems patent December 2005
Aerodynamic focusing of nanoparticle or cluster beams patent January 2009
Methods and apparatus for ion sources, ion control and ion measurement for macromolecules patent August 2011
FAIMS with non-destructive detection of selectively transmitted ions patent-application August 2003
Mass spectrometry apparatus and method patent-application December 2005
Atmospheric pressure charged particle discriminator for mass spectrometry patent-application June 2006
Computerized Method and System for Designing an Aerodynamic Focusing Lens Stack patent-application September 2008

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