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Title: rac-6-Hydroxy-2,5,7,8-tetramethylchroman-2-carboxamide from synchrotron data

Journal Article · · Acta Crystallogr. E

The crystal structure of the title water-soluble analogue of vitamin E, trolox amide, C{sub 14}H{sub 19}NO{sub 3}, solved and refined against synchrotron diffraction data, contains two molecules in the asymmetric unit. In both molecules, the heterocyclic ring is in a half-chair conformation. The crystal packing features a herring-bone pattern generated by N-H...O hydrogen bonds between the hydroxy and amide groups. O-H...O hydrogen bonds also occur.

Research Organization:
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Organization:
FOREIGNNIH
OSTI ID:
1039447
Journal Information:
Acta Crystallogr. E, Vol. 67, Issue (2) ; 02, 2011; ISSN 1600-5368
Country of Publication:
United States
Language:
ENGLISH

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