In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium

Miao, Yinbin; Mo, Kun; Park, Jun-Sang; Almer, Jonathan; Massey, Caleb; Havrilak, Cody; Nelson, Andrew T.; Connaway, Heather; Yacout, Abdellatif M.

doi:10.1016/j.jnucmat.2022.153843

Title: In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium

Abstract

The microstructure evolution during room temperature uniaxial tensile straining of ultrasonic additive manufactured (UAM) zirconium was evaluated using the Advanced Photon Source (APS) facility. Miniature dog-bone tensile specimens of two orientations were cut from a UAM-fabricated zirconium bar for in situ synchrotron tensile tests. Wide-angle X-ray scattering (WAXS) scanning was used to unveil the changes in microstructure of the entire gauge regions throughout the straining. A series of WAXS data analysis methods were utilized to quantify both elastic and plastic deformation mechanisms within the strained specimens. Stress concentrations were identified during early stages of plastic deformation, which become candidate necking positions and eventually lead to failure. Additionally, fracture surface analysis implied that these stress concentration locations may be correlated to the fabrication defects, providing insightful guidance for future improvements of the UAM zirconium fabrication process.

Authors:

^[1];

^[1]; Massey, Caleb ^[2];

^[2];

^[2]; Connaway, Heather ^[1];

^[1]

Argonne National Lab. (ANL), Lemont, IL (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Publication Date:: Mon Jun 06 00:00:00 EDT 2022

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA), Office of Defense Nuclear Nonproliferation

OSTI Identifier:: 1875366

Alternate Identifier(s):: OSTI ID: 1915451

Grant/Contract Number:: AC05-00OR22725; AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Journal of Nuclear Materials

Additional Journal Information:: Journal Volume: 568; Journal Issue: 1; Journal ID: ISSN 0022-3115

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; ultrasonic additive manufacturing; synchrotron; wide-angle x-ray scattering; microstructure

Citation Formats


                    Miao, Yinbin, Mo, Kun, Park, Jun-Sang, Almer, Jonathan, Massey, Caleb, Havrilak, Cody, Nelson, Andrew T., Connaway, Heather, and Yacout, Abdellatif M. In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium.  United States: N. p., 2022. 
Web.  doi:10.1016/j.jnucmat.2022.153843.

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                    Miao, Yinbin, Mo, Kun, Park, Jun-Sang, Almer, Jonathan, Massey, Caleb, Havrilak, Cody, Nelson, Andrew T., Connaway, Heather, & Yacout, Abdellatif M. In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium.  United States.  https://doi.org/10.1016/j.jnucmat.2022.153843

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                    Miao, Yinbin, Mo, Kun, Park, Jun-Sang, Almer, Jonathan, Massey, Caleb, Havrilak, Cody, Nelson, Andrew T., Connaway, Heather, and Yacout, Abdellatif M. Mon .  
"In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium".  United States.  https://doi.org/10.1016/j.jnucmat.2022.153843.  https://www.osti.gov/servlets/purl/1875366.

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@article{osti_1875366,

  title        = {In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium},

  author       = {Miao, Yinbin and Mo, Kun and Park, Jun-Sang and Almer, Jonathan and Massey, Caleb and Havrilak, Cody and Nelson, Andrew T. and Connaway, Heather and Yacout, Abdellatif M.},

  abstractNote = {The microstructure evolution during room temperature uniaxial tensile straining of ultrasonic additive manufactured (UAM) zirconium was evaluated using the Advanced Photon Source (APS) facility. Miniature dog-bone tensile specimens of two orientations were cut from a UAM-fabricated zirconium bar for in situ synchrotron tensile tests. Wide-angle X-ray scattering (WAXS) scanning was used to unveil the changes in microstructure of the entire gauge regions throughout the straining. A series of WAXS data analysis methods were utilized to quantify both elastic and plastic deformation mechanisms within the strained specimens. Stress concentrations were identified during early stages of plastic deformation, which become candidate necking positions and eventually lead to failure. Additionally, fracture surface analysis implied that these stress concentration locations may be correlated to the fabrication defects, providing insightful guidance for future improvements of the UAM zirconium fabrication process.},

  doi          = {10.1016/j.jnucmat.2022.153843},

  journal      = {Journal of Nuclear Materials},

  number       = 1,

  volume       = 568,

  place        = {United States},

  year         = {Mon Jun 06 00:00:00 EDT 2022},

  month        = {Mon Jun 06 00:00:00 EDT 2022}

}

Copy to clipboard

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Title: In situ synchrotron tensile investigations on ultrasonic additive manufactured (UAM) zirconium

Abstract

Citation Formats

Grain to grain slip activity in plastically deformed Zr determined by X-ray micro-diffraction line profile analysis journal, February 2007

High energy X-ray diffraction study of the relationship between the macroscopic mechanical properties and microstructure of irradiated HT-9 steel journal, July 2016

Characterization of interfacial microstructures in 3003 aluminum alloy blocks fabricated by ultrasonic additive manufacturing journal, August 2010

Hall–Petch relation and boundary strengthening journal, October 2004

The development and applications of zirconium alloys journal, April 1985

X-ray line broadening from filed aluminium and wolfram journal, January 1953

Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation journal, April 2017

Investigation of thermal aging effects on the tensile properties of Alloy 617 by in-situ synchrotron wide-angle X-ray scattering journal, January 2016

Prismatic slip in zirconium single crystals at elevated temperatures journal, June 1975

Study of the mechanical behavior of the hydride blister/rim structure in Zircaloy-4 using in-situ synchrotron X-ray diffraction journal, April 2016

Dislocations and Grain Size in Electrodeposited Nanocrystalline Ni Determined by the Modified Williamson–Hall and Warren–Averbach Procedures journal, August 1998

Rationalization of anisotropic mechanical properties of Al-6061 fabricated using ultrasonic additive manufacturing journal, September 2016

Stacking faults and twin boundaries in fcc crystals determined by x-ray diffraction profile analysis journal, July 2006

Twinning on pyramidal planes in hexagonal close packed crystals determined along with other defects by X-ray line profile analysis journal, June 2009

dislocations in zirconium alloys journal, November 1979

Spatial Strain Sensing Using Embedded Fiber Optics journal, January 2019

Ultrasonic additive manufacturing of zirconium: Pilot results journal, November 2021

First-Principles Study of Secondary Slip in Zirconium journal, February 2014

Deformation and fracture characteristics of zirconium plate produced via ultrasonic additive manufacturing journal, October 2021

MWP-fit : a program for multiple whole-profile fitting of diffraction peak profiles by ab initio theoretical functions journal, September 2001

The determination of a continuum mechanics equivalent elastic strain from the analysis of multiple diffraction peaks journal, October 2004

Contrast factors of dislocations in the hexagonal crystal system journal, September 2002

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Dislocation evolution during tensile deformation in ferritic–martensitic steels revealed by high-energy X-rays journal, September 2014

Grain to grain slip activity in plastically deformed Zr determined by X-ray micro-diffraction line profile analysis
journal, February 2007

High energy X-ray diffraction study of the relationship between the macroscopic mechanical properties and microstructure of irradiated HT-9 steel
journal, July 2016

Characterization of interfacial microstructures in 3003 aluminum alloy blocks fabricated by ultrasonic additive manufacturing
journal, August 2010

Hall–Petch relation and boundary strengthening
journal, October 2004

The development and applications of zirconium alloys
journal, April 1985

X-ray line broadening from filed aluminium and wolfram
journal, January 1953

Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation
journal, April 2017

Investigation of thermal aging effects on the tensile properties of Alloy 617 by in-situ synchrotron wide-angle X-ray scattering
journal, January 2016

Prismatic slip in zirconium single crystals at elevated temperatures
journal, June 1975

Study of the mechanical behavior of the hydride blister/rim structure in Zircaloy-4 using in-situ synchrotron X-ray diffraction
journal, April 2016

Dislocations and Grain Size in Electrodeposited Nanocrystalline Ni Determined by the Modified Williamson–Hall and Warren–Averbach Procedures
journal, August 1998

Rationalization of anisotropic mechanical properties of Al-6061 fabricated using ultrasonic additive manufacturing
journal, September 2016

Stacking faults and twin boundaries in fcc crystals determined by x-ray diffraction profile analysis
journal, July 2006

Twinning on pyramidal planes in hexagonal close packed crystals determined along with other defects by X-ray line profile analysis
journal, June 2009

dislocations in zirconium alloys
journal, November 1979

Spatial Strain Sensing Using Embedded Fiber Optics
journal, January 2019

Ultrasonic additive manufacturing of zirconium: Pilot results
journal, November 2021

First-Principles Study of Secondary Slip in Zirconium
journal, February 2014

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journal, October 2021

MWP-fit : a program for multiple whole-profile fitting of diffraction peak profiles by ab initio theoretical functions
journal, September 2001

The determination of a continuum mechanics equivalent elastic strain from the analysis of multiple diffraction peaks
journal, October 2004

Contrast factors of dislocations in the hexagonal crystal system
journal, September 2002

Evolution of dislocation density in a hot rolled Zr–2.5Nb alloy with plastic deformation studied by neutron diffraction and transmission electron microscopy
journal, July 2017

Additive manufacturing (3D printing): A review of materials, methods, applications and challenges
journal, June 2018

On the microstructure and strengthening mechanism in oxide dispersion-strengthened 316 steel: A coordinated electron microscopy, atom probe tomography and in situ synchrotron tensile investigation
journal, July 2015

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journal, April 2016

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journal, February 2015

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journal, March 2017

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journal, March 2018

Correlation between strength and microstructure of ball-milled Al–Mg alloys determined by X-ray diffraction
journal, December 2004

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journal, April 2014

Effect of quenching rate on the β-to-α phase transformation structure in zirconium alloy
journal, November 2003

Dislocation evolution during tensile deformation in ferritic–martensitic steels revealed by high-energy X-rays
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