Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe0.5Cr0.5O3

Shi, Jianhang; Seehra, Mohindar S.; Dang, Yanliu; Suib, Steven L.; Jain, Menka

doi:10.1063/5.0048828

Title: Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe_0.5Cr_0.5O₃

Abstract

Here, we report a comparison of the magnetic, magnetocaloric, and dielectric properties of 50% iron substituted GdCrO₃ (GdFe_0.5Cr_0.5O₃) bulk pellet and 960 nm thick film of GdFe_0.5Cr_0.5O₃ (GFCO). The 960 nm film was synthesized on a platinized-silicon substrate by chem. soln. deposition and spin-coating methods. The X-ray diffraction scans of the bulk sample and the film as well as the morphology of the film as examined by the field-emission scanning electron microscope indicate phase-pure and polycrystalline nature of these samples. XPS was used to deermine the valence states of Gd, Fe, and Cr. The temp. dependence of the dielectric const. from 225 to 700 K shows peaks at T_C = 525 K for the bulk and ≈450 K for the film due to ferroelectric to paraelectric transitions, since elec. polarization vs elec. field hysteresis loops are observed. at room temp. The dielectric studies in the bulk GFCO for T > T_C indicate a relaxor-like behavior. The measurements of the magnetization (M) of the samples as a function of temp. (5-350 K) and magnetic field (H) up to 7 T (=70 kOe) depict hysteresis behavior at low temps. due to the canted antiferromagnetic order of Fe³⁺/Cr³⁺ below the Néel temp. ofmore »« less

Authors:

^[1];

^[2]; Dang, Yanliu ^[1]; Suib, Steven L. ^[1];

^[1]

Univ. of Connecticut, Storrs, CT (United States)
West Virginia Univ., Morgantown, WV (United States)

Publication Date:: Mon Jun 28 00:00:00 EDT 2021

Research Org.:: Univ. of Connecticut, Storrs, CT (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division; USDOE

OSTI Identifier:: 1838052

Alternate Identifier(s):: OSTI ID: 1798932

Grant/Contract Number:: FG02-86ER13622

Resource Type:: Accepted Manuscript

Journal Name:: Journal of Applied Physics

Additional Journal Information:: Journal Volume: 129; Journal Issue: 24; Journal ID: ISSN 0021-8979

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Thin films; Cooling technology; Cryogenics; Dielectric properties; Multiferroics; Spin coating; Polycrystalline material; Magnetic hysteresis; Scanning electron microscopy

Citation Formats


                    Shi, Jianhang, Seehra, Mohindar S., Dang, Yanliu, Suib, Steven L., and Jain, Menka. Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe0.5Cr0.5O3.  United States: N. p., 2021. 
Web.  doi:10.1063/5.0048828.

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                    Shi, Jianhang, Seehra, Mohindar S., Dang, Yanliu, Suib, Steven L., & Jain, Menka. Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe0.5Cr0.5O3.  United States.  https://doi.org/10.1063/5.0048828

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                    Shi, Jianhang, Seehra, Mohindar S., Dang, Yanliu, Suib, Steven L., and Jain, Menka. Mon .  
"Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe0.5Cr0.5O3".  United States.  https://doi.org/10.1063/5.0048828.  https://www.osti.gov/servlets/purl/1838052.

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@article{osti_1838052,

  title        = {Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe0.5Cr0.5O3},

  author       = {Shi, Jianhang and Seehra, Mohindar S. and Dang, Yanliu and Suib, Steven L. and Jain, Menka},

  abstractNote = {Here, we report a comparison of the magnetic, magnetocaloric, and dielectric properties of 50% iron substituted GdCrO3 (GdFe0.5Cr0.5O3) bulk pellet and 960 nm thick film of GdFe0.5Cr0.5O3 (GFCO). The 960 nm film was synthesized on a platinized-silicon substrate by chem. soln. deposition and spin-coating methods. The X-ray diffraction scans of the bulk sample and the film as well as the morphology of the film as examined by the field-emission scanning electron microscope indicate phase-pure and polycrystalline nature of these samples. XPS was used to deermine the valence states of Gd, Fe, and Cr. The temp. dependence of the dielectric const. from 225 to 700 K shows peaks at TC = 525 K for the bulk and ≈450 K for the film due to ferroelectric to paraelectric transitions, since elec. polarization vs elec. field hysteresis loops are observed. at room temp. The dielectric studies in the bulk GFCO for T > TC indicate a relaxor-like behavior. The measurements of the magnetization (M) of the samples as a function of temp. (5-350 K) and magnetic field (H) up to 7 T (=70 kOe) depict hysteresis behavior at low temps. due to the canted antiferromagnetic order of Fe3+/Cr3+ below the Néel temp. of ≈275 K. The M vs H isotherms at various temps. are used to det. and compare the magnetic entropy change (-ΔS) and relative cooling power (RCP) of the two samples, yielding (-ΔS) = 30.7 J/kg K (18.8 J/kg K) and RCP = 566.5 J/kg (375 J/kg) for the bulk (960 nm film) samples of GFCO at 7 K and 7 T, resp. The plot of RCP vs T shows that magnetic cooling for this system is most effective for T < 30 K. Comparatively smaller magnitudes of (-ΔS) and RCP for the film vis-a-vis the bulk sample of GFCO scale with its reduced magnetization. This suggests that further improvements in the quality of the films are needed to improve their magnetization and hence their magnetocaloric properties, possibly making them useful for on-chip cooling in miniaturized devices.},

  doi          = {10.1063/5.0048828},

  journal      = {Journal of Applied Physics},

  number       = 24,

  volume       = 129,

  place        = {United States},

  year         = {Mon Jun 28 00:00:00 EDT 2021},

  month        = {Mon Jun 28 00:00:00 EDT 2021}

}

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Abstract

Citation Formats

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Structure-property correlations and scaling in the magnetic and magnetocaloric properties of GdCrO 3 particles journal, April 2021

Enhancement in magnetocaloric properties of holmium chromite by gadolinium substitution journal, July 2016

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Giant anisotropy of magnetocaloric effect in TbMnO 3 single crystals journal, May 2011

Nonlinear magnetodielectric effect of disordered perovskite HoCr0.5Fe0.5O3: Role of magnetic rare-earth ions journal, May 2019

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Title: Comparison of the dielectric and magnetocaloric properties of bulk and film of GdFe_0.5Cr_0.5O₃

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journal, March 2013

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journal, January 2007

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journal, May 2008

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book, January 1998

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journal, September 2003

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journal, May 2020

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journal, June 2012

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journal, July 2016

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journal, September 1990

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journal, April 2010

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journal, January 2006

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journal, February 2017

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journal, August 2011

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journal, September 2020

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journal, May 2010

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journal, January 2013

The Magnetocaloric Effect and Magnetic Refrigeration Near Room Temperature: Materials and Models
journal, August 2012

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journal, December 2012

Unusual rotating magnetocaloric effect in the hexagonal $ErMn O_{3}$ single crystal
journal, November 2018

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journal, January 2018

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journal, December 2012

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journal, August 2014

Magnetocaloric Materials
journal, August 2000

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journal, April 2010

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journal, November 2008

Recent developments in magnetocaloric materials
journal, May 2005

Effect of Gd polarization on the large magnetocaloric effect of ${GdCrO}_{4}$ in a broad temperature range
journal, February 2016

Reduction of hysteresis losses in the magnetic refrigerant Gd5Ge2Si2 by the addition of iron
journal, June 2004

Ferroelectrics go bananas
journal, December 2007

Magnetocaloric materials: The search for new systems
journal, September 2012

Dielectric studies of multiferroic orthochromites Ho0.9(RE)0.1CrO3 (where RE=Gd and Yb)
journal, July 2016

The influence of chromium substitution on crystal structure and shift of Néel transition in GdFe1−xCrxO3 mixed oxides
journal, October 2016

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journal, February 2017

GdCrO ₃ : a potential candidate for low temperature magnetic refrigeration
journal, July 2018

Novel Pd/GdCrO3 composite for photo-catalytic reduction of nitrate to N2 with high selectivity and activity
journal, September 2018

Epoxy-bonded La–Fe–Co–Si magnetocaloric plates
journal, February 2015

Analysis of dielectric and magnetic phase transitions in Yb(Fe0.5Cr0.5)O3 bulk perovskite
journal, March 2019

Low temperature giant magnetocaloric effect in multiferroic GdMnO ₃ single crystals
journal, March 2015

Magnetic exchange interactions of rare-earth-substituted ${DyCrO}_{3}$ bulk powders
journal, June 2015

Cubic GdFeO3 particle by a simple hydrothermal synthesis route and its photoluminescence and magnetic properties
journal, January 2012

Magnetocaloric properties of rare-earth substituted DyCrO ₃
journal, July 2015

Giant Magnetocaloric Effect in ${Gd}_{5} ({Si}_{2} {Ge}_{2})$
journal, June 1997

Magnetocaloric effect in nanoscale thin films and heterostructures
journal, July 2014

Multiferroicity and magnetoelectric coupling enhanced large magnetocaloric effect in DyFe _0.5 Cr _0.5 O ₃
journal, January 2014

Selective laser melting of La(Fe,Co,Si) ₁₃ geometries for magnetic refrigeration
journal, July 2013

Coupled caloric effects in multiferroics
journal, February 2013

Packing-density calculation of thin fluoride films from infrared transmission spectra
journal, January 1996

Glassy magnetic phase driven by short-range charge and magnetic ordering in nanocrystalline La $_{1 / 3}$ Sr $_{2 / 3}$ FeO $_{3 - δ}$ : Magnetization, Mössbauer, and polarized neutron studies
journal, September 2012

Stress and strain in polycrystalline thin films
journal, June 2007

Giant magnetocaloric effect and temperature induced magnetization jump in GdCrO ₃ single crystal
journal, April 2015

Magnetic and magnetocaloric properties of $HoCr O_{3}$ tuned by selective rare-earth doping
journal, May 2017

Antiferromagnetic and dielectric behavior in polycrystalline GdFe _0.5 Cr _0.5 O ₃ thin film
journal, March 2020

Influence of growth morphology on the Néel temperature of CrRu thin films and heterostructures
journal, May 2010

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journal, December 1985

A novel multiferroic system: Rare earth chromates
journal, May 2010

Magnetic properties of pure and Fe doped HoCrO3 thin films fabricated via a solution route
journal, April 2017

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journal, November 2017

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journal, November 2019

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journal, May 2012

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journal, June 2013

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journal, August 2012

Colossal dielectric, relaxor ferroelectric, diamagnetic and weak ferromagnetic properties of NdCrO3 perovskite nanoparticles
journal, December 2018

Synthesis, Photocatalytic and Electrocatalytic Activities of Wormlike GdFeO ₃ Nanoparticles by a Glycol-Assisted Sol–Gel Process
journal, May 2013

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journal, July 2011

Analysis of Ferroelectric, Dielectric and Magnetic Properties of GdFeO ₃ Nanoparticles
journal, October 2014

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journal, April 2021

Enhancement in magnetocaloric properties of holmium chromite by gadolinium substitution
journal, July 2016

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journal, October 2012

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journal, May 2011

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journal, May 2019

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journal, March 2020

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journal, September 2018

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journal, May 2018

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journal, September 2010

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journal, February 2017

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journal, September 2013

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journal, October 1999

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journal, August 2004