Measuring grain rotation at the nanoscale
Abstract
In this paper, we introduced a method to measure grain rotation of nanomaterials under external stress using a high pressure diamond anvil cell and the Laue microdiffraction technique at a synchrotron facility. We used tungsten carbide marker crystals to investigate grain rotation activities of 3 and 500 nm nickel media. Our results show that the grain rotation of 3 and 500 nm nickel nanocrystals increase with pressure and finally rotation of 500 nm nickel tends to stop at a lower pressure/stress level than 3 nm nickel. 3 nm nickel nanocrystals show a higher rotation magnitude than 500 nm nickel nanocrystals. Our measurements show an effective method to study the grain rotation of nanomaterials especially in ultrafine nanocrystals.
- Authors:
-
- Center for High Pressure Science and Technology Advanced Research, Pudong, Shanghai,(China); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS)
- Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS)
- Center for High Pressure Science and Technology Advanced Research, Pudong, Shanghai,(China)
- Publication Date:
- Research Org.:
- Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22), Scientific User Facilities Division (SC-22.3 )
- OSTI Identifier:
- 1787999
- Grant/Contract Number:
- AC02-05CH11231
- Resource Type:
- Accepted Manuscript
- Journal Name:
- High Pressure Research
- Additional Journal Information:
- Journal Volume: 37; Journal Issue: 3; Journal ID: ISSN 0895-7959
- Publisher:
- Taylor & Francis
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Diamond anvil cell; laue microdiffraction; grain rotation; deformation; nanomaterials
Citation Formats
Zhou, Xiaoling, Tamura, Nobumichi, Mi, Zhongying, Zhang, Lingkong, Ke, Feng, and Chen, Bin. Measuring grain rotation at the nanoscale. United States: N. p., 2017.
Web. doi:10.1080/08957959.2017.1334775.
Zhou, Xiaoling, Tamura, Nobumichi, Mi, Zhongying, Zhang, Lingkong, Ke, Feng, & Chen, Bin. Measuring grain rotation at the nanoscale. United States. https://doi.org/10.1080/08957959.2017.1334775
Zhou, Xiaoling, Tamura, Nobumichi, Mi, Zhongying, Zhang, Lingkong, Ke, Feng, and Chen, Bin. Thu .
"Measuring grain rotation at the nanoscale". United States. https://doi.org/10.1080/08957959.2017.1334775. https://www.osti.gov/servlets/purl/1787999.
@article{osti_1787999,
title = {Measuring grain rotation at the nanoscale},
author = {Zhou, Xiaoling and Tamura, Nobumichi and Mi, Zhongying and Zhang, Lingkong and Ke, Feng and Chen, Bin},
abstractNote = {In this paper, we introduced a method to measure grain rotation of nanomaterials under external stress using a high pressure diamond anvil cell and the Laue microdiffraction technique at a synchrotron facility. We used tungsten carbide marker crystals to investigate grain rotation activities of 3 and 500 nm nickel media. Our results show that the grain rotation of 3 and 500 nm nickel nanocrystals increase with pressure and finally rotation of 500 nm nickel tends to stop at a lower pressure/stress level than 3 nm nickel. 3 nm nickel nanocrystals show a higher rotation magnitude than 500 nm nickel nanocrystals. Our measurements show an effective method to study the grain rotation of nanomaterials especially in ultrafine nanocrystals.},
doi = {10.1080/08957959.2017.1334775},
journal = {High Pressure Research},
number = 3,
volume = 37,
place = {United States},
year = {Thu Jun 08 00:00:00 EDT 2017},
month = {Thu Jun 08 00:00:00 EDT 2017}
}
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