Sensitive and Selective NH3 Monitoring at Room Temperature Using ZnO Ceramic Nanofibers Decorated with Poly(styrene sulfonate)
Abstract
Ammonia (NH3) gas is a prominent air pollutant that is frequently found in industrial and livestock production environments. Due to the importance in controlling pollution and protecting public health, the development of new platforms for sensing NH3 at room temperature has attracted great attention. In this study, a sensitive NH3 gas device with enhanced selectivity is developed based on zinc oxide nanofibers (ZnO NFs) decorated with poly(styrene sulfonate) (PSS) and operated at room temperature. ZnO NFs were prepared by electrospinning followed by calcination at 500 °C for 3 h. The electrospun ZnO NFs are characterized to evaluate the properties of the as-prepared sensing materials. The loading of PSS to prepare ZnO NFs/PSS composite is also optimized based on the best sensing performance. Under the optimal composition, ZnO NFs/PSS displays rapid, reversible, and sensitive response upon NH3 exposure at room temperature. The device shows a dynamic linear range up to 100 ppm and a limit of detection of 3.22 ppm and enhanced selectivity toward NH3 in synthetic air, against NO2 and CO, compared to pure ZnO NFs. Additionally, a sensing mechanism is proposed to illustrate the sensing performance using ZnO NFs/PSS composite. Therefore, this study provides a simple methodology to designmore »
- Authors:
-
[5];
- Univ. of Connecticut, Storrs, CT (United States). Dept. of Chemical and Biomolecular Engineering; Nanotechnology National Lab. for Agriculture (LNNA), Sao Paulo (Brazil). Embrapa Instrumentacao; Federal University of São Carlos (UFSCar), Sao Paulo (Brazil). Center for Exact Sciences and Technology. Dept. of Chemistry. PPGQ
- Univ. of Connecticut, Storrs, CT (United States). Dept. of Materials Science and Engineering
- Univ. of Connecticut, Storrs, CT (United States). Dept. of Biomedical Engineering
- Univ. of Connecticut, Storrs, CT (United States). Dept. of Chemistry
- Nanotechnology National Lab. for Agriculture (LNNA), Sao Paulo (Brazil). Embrapa Instrumentacao; Federal University of São Carlos (UFSCar), Sao Paulo (Brazil). Center for Exact Sciences and Technology. Dept. of Chemistry. PPGQ
- Univ. of Connecticut, Storrs, CT (United States). Dept. of Chemical and Biomolecular Engineering
- Publication Date:
- Research Org.:
- Univ. of Connecticut, Storrs, CT (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC)
- OSTI Identifier:
- 1628552
- Grant/Contract Number:
- FG02-00ER41132
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Sensors
- Additional Journal Information:
- Journal Volume: 18; Journal Issue: 4; Journal ID: ISSN 1424-8220
- Publisher:
- MDPI AG
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; Chemistry; Engineering; Instruments & Instrumentation; ZnO NFs; PSS; NH3 sensor; room temperature sensing; good sensitivity
Citation Formats
Andre, Rafaela, Kwak, Dongwook, Dong, Qiuchen, Zhong, Wei, Correa, Daniel, Mattoso, Luiz, and Lei, Yu. Sensitive and Selective NH3 Monitoring at Room Temperature Using ZnO Ceramic Nanofibers Decorated with Poly(styrene sulfonate). United States: N. p., 2018.
Web. doi:10.3390/s18041058.
Andre, Rafaela, Kwak, Dongwook, Dong, Qiuchen, Zhong, Wei, Correa, Daniel, Mattoso, Luiz, & Lei, Yu. Sensitive and Selective NH3 Monitoring at Room Temperature Using ZnO Ceramic Nanofibers Decorated with Poly(styrene sulfonate). United States. https://doi.org/10.3390/s18041058
Andre, Rafaela, Kwak, Dongwook, Dong, Qiuchen, Zhong, Wei, Correa, Daniel, Mattoso, Luiz, and Lei, Yu. Sun .
"Sensitive and Selective NH3 Monitoring at Room Temperature Using ZnO Ceramic Nanofibers Decorated with Poly(styrene sulfonate)". United States. https://doi.org/10.3390/s18041058. https://www.osti.gov/servlets/purl/1628552.
@article{osti_1628552,
title = {Sensitive and Selective NH3 Monitoring at Room Temperature Using ZnO Ceramic Nanofibers Decorated with Poly(styrene sulfonate)},
author = {Andre, Rafaela and Kwak, Dongwook and Dong, Qiuchen and Zhong, Wei and Correa, Daniel and Mattoso, Luiz and Lei, Yu},
abstractNote = {Ammonia (NH3) gas is a prominent air pollutant that is frequently found in industrial and livestock production environments. Due to the importance in controlling pollution and protecting public health, the development of new platforms for sensing NH3 at room temperature has attracted great attention. In this study, a sensitive NH3 gas device with enhanced selectivity is developed based on zinc oxide nanofibers (ZnO NFs) decorated with poly(styrene sulfonate) (PSS) and operated at room temperature. ZnO NFs were prepared by electrospinning followed by calcination at 500 °C for 3 h. The electrospun ZnO NFs are characterized to evaluate the properties of the as-prepared sensing materials. The loading of PSS to prepare ZnO NFs/PSS composite is also optimized based on the best sensing performance. Under the optimal composition, ZnO NFs/PSS displays rapid, reversible, and sensitive response upon NH3 exposure at room temperature. The device shows a dynamic linear range up to 100 ppm and a limit of detection of 3.22 ppm and enhanced selectivity toward NH3 in synthetic air, against NO2 and CO, compared to pure ZnO NFs. Additionally, a sensing mechanism is proposed to illustrate the sensing performance using ZnO NFs/PSS composite. Therefore, this study provides a simple methodology to design a sensitive platform for NH3 monitoring at room temperature.},
doi = {10.3390/s18041058},
journal = {Sensors},
number = 4,
volume = 18,
place = {United States},
year = {Sun Apr 01 00:00:00 EDT 2018},
month = {Sun Apr 01 00:00:00 EDT 2018}
}
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Facial development of high performance room temperature NO2 gas sensors based on ZnO nanowalls decorated rGO nanosheets
journal, November 2017
- Liu, Zongyuan; Yu, Lingmin; Guo, Fen
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Weekly agricultural emissions and ambient concentrations of ammonia: Validation of an emission inventory
journal, July 2015
- Bittman, Shabtai; Jones, Keith; Vingarzan, Roxanne
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journal, November 2017
- Thungon, Phurpa Dema; Kakoti, Ankana; Ngashangva, Lightson
- Biosensors and Bioelectronics, Vol. 97
Gas sensing properties of single crystalline ZnO nanowires grown by thermal evaporation technique
journal, October 2013
- Rai, Prabhakar; Khan, Rizwan; Ahmad, Rafiq
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Vertical ZnO nanorod array as an effective hydrogen gas sensor
journal, January 2013
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A room temperature ammonia gas sensor based on cellulose/TiO 2 /PANI composite nanofibers
journal, April 2016
- Pang, Zengyuan; Yang, Zhanping; Chen, Yun
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Enhanced NH3 gas sensing performance based on electrospun alkaline-earth metals composited SnO2 nanofibers
journal, January 2015
- Xu, Shuang; Kan, Kan; Yang, Ying
- Journal of Alloys and Compounds, Vol. 618
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journal, January 2016
- Loyon, L.; Burton, C. H.; Misselbrook, T.
- Journal of Environmental Management, Vol. 166
Facile synthesis of doped ZnO-CdO nanoblocks as solid-phase adsorbent and efficient solar photo-catalyst applications
journal, July 2014
- Rahman, Mohammed M.; Khan, Sher Bahadar; Marwani, Hadi M.
- Journal of Industrial and Engineering Chemistry, Vol. 20, Issue 4
Gas-sensing property improvement of ZnO by hierarchical flower-like architectures
journal, December 2011
- Guo, Weiwei; Liu, Tianmo; Zeng, Wen
- Materials Letters, Vol. 65, Issue 23-24
Identification of adulteration in uncooked Jasmine rice by a portable low-cost artificial olfactory system
journal, October 2017
- Timsorn, Kriengkri; Lorjaroenphon, Yaowapa; Wongchoosuk, Chatchawal
- Measurement, Vol. 108
Recent progress in the ZnO nanostructure-based sensors
journal, November 2011
- Wei, Ang; Pan, Liuhua; Huang, Wei
- Materials Science and Engineering: B, Vol. 176, Issue 18
A highly selective and wide range ammonia sensor—Nanostructured ZnO:Co thin film
journal, January 2015
- Mani, Ganesh Kumar; Rayappan, John Bosco Balaguru
- Materials Science and Engineering: B, Vol. 191
Improved gas sensing performance of Al doped ZnO/CuO nanocomposite based ammonia gas sensor
journal, January 2018
- Poloju, Madhukar; Jayababu, Nagabandi; Ramana Reddy, M. V.
- Materials Science and Engineering: B, Vol. 227
Low-cost and flexible printed graphene–PEDOT:PSS gas sensor for ammonia detection
journal, November 2014
- Seekaew, Yotsarayuth; Lokavee, Shongpun; Phokharatkul, Ditsayut
- Organic Electronics, Vol. 15, Issue 11
Ammonia sensors and their applications—a review
journal, June 2005
- Timmer, Björn; Olthuis, Wouter; Berg, Albert van den
- Sensors and Actuators B: Chemical, Vol. 107, Issue 2
Hierarchical α-Fe2O3/SnO2 semiconductor composites: Hydrothermal synthesis and gas sensing properties
journal, June 2013
- Sun, Peng; Cai, Yaxin; Du, Sisi
- Sensors and Actuators B: Chemical, Vol. 182
Isopropanol sensing properties of coral-like ZnO–CdO composites by flash preparation via self-sustained decomposition of metal–organic complexes
journal, July 2014
- Cai, Xiaoyan; Hu, Dan; Deng, Shaojuan
- Sensors and Actuators B: Chemical, Vol. 198
Fully gravure-printed NO2 gas sensor on a polyimide foil using WO3-PEDOT:PSS nanocomposites and Ag electrodes
journal, September 2015
- Lin, Youjie; Huang, Lei; Chen, Lu
- Sensors and Actuators B: Chemical, Vol. 216
Reduced graphene oxide (rGO) encapsulated Co3O4 composite nanofibers for highly selective ammonia sensors
journal, January 2016
- Feng, Qiuxia; Li, Xiaogan; Wang, Jing
- Sensors and Actuators B: Chemical, Vol. 222
NH 3 gas sensor based on Pd/SnO 2 /RGO ternary composite operated at room-temperature
journal, February 2016
- Su, Pi-Guey; Yang, Ling-Yu
- Sensors and Actuators B: Chemical, Vol. 223
Enhanced H2S gas sensing properties of undoped ZnO nanocrystalline films from QDs by low-temperature processing
journal, March 2016
- Deng, Jianfeng; Fu, Qiuyun; Luo, Wei
- Sensors and Actuators B: Chemical, Vol. 224
Hybrid layer-by-layer (LbL) films of polyaniline, graphene oxide and zinc oxide to detect ammonia
journal, January 2017
- Andre, Rafaela S.; Shimizu, Flávio M.; Miyazaki, Celina M.
- Sensors and Actuators B: Chemical, Vol. 238
Flower-like ZnO hollow microspheres loaded with CdO nanoparticles as high performance sensing material for gas sensors
journal, October 2017
- Wang, Tianshuang; Kou, Xueying; Zhao, Liupeng
- Sensors and Actuators B: Chemical, Vol. 250
Portable cyber-physical system for indoor and outdoor gas sensing
journal, November 2017
- Järvinen, Topias; Lorite, Gabriela Simone; Rautio, Anne-Riikka
- Sensors and Actuators B: Chemical, Vol. 252
Low-temperature and fast response H2S gas sensor using semiconducting chitosan film
journal, December 2017
- Abu-Hani, Ayah F. S.; Greish, Yaser E.; Mahmoud, Saleh T.
- Sensors and Actuators B: Chemical, Vol. 253
Abnormal n-p-n type conductivity transition of hollow ZnO/ZnFe2O4 nanostructures during gas sensing process: The role of ZnO-ZnFe2O4 hetero-interface
journal, December 2017
- Li, Wenhui; Wu, Xiaofeng; Chen, Jiayuan
- Sensors and Actuators B: Chemical, Vol. 253
Fast response and highly sensitive humidity sensors based on CaCl2-doped sulfonated poly (ether ether ketone)s
journal, December 2017
- Zhuang, Zhuang; Qi, Duo; Ru, Chunyu
- Sensors and Actuators B: Chemical, Vol. 253
Semiconductor-type SnO2-based NO2 sensors operated at room temperature under UV-light irradiation
journal, December 2017
- Hyodo, Takeo; Urata, Kaoru; Kamada, Kai
- Sensors and Actuators B: Chemical, Vol. 253
Sensitivity enhancement of ammonia gas sensor based on Ag/ZnO flower and nanoellipsoids at low temperature
journal, February 2018
- R., Sankar Ganesh; M., Navaneethan; Patil, V. L.
- Sensors and Actuators B: Chemical, Vol. 255
Triple-shelled ZnO/ZnFe2O4 heterojunctional hollow microspheres derived from Prussian Blue analogue as high-performance acetone sensors
journal, March 2018
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