The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy

Harris, Zachary D.; Bhattacharyya, Jishnu J.; Ronevich, Joseph A.; Agnew, Sean R.; Burns, James T.

doi:10.1016/j.actamat.2020.01.033

Title: The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy

Abstract

The effect of hydrogen (H) on the deformation behavior of Monel K-500 in various isothermal heat treatment conditions (non-aged, under-aged, peak-aged, and over-aged) was assessed via uniaxial mechanical testing. H-charged and non-charged specimens were strained to failure to facilitate a comparison of ductility, fracture surface morphology, strength, and work hardening behavior. For all examined heat treatment conditions, H charging leads to a significant reduction in ductility, which is accompanied by a consistent change in fracture surface morphology from ductile microvoid coalescence to brittle intergranular fracture. While H charging led to a systematic enhancement in the yield strength of all heat treatments, the three age-hardened conditions exhibited a more than 2-fold increase relative to the non-aged heat treatment. This suggests that H modifies the dislocation–precipitate interactions, which also manifest themselves through changes in work hardening metrics related to the dislocation storage and recovery rates. In particular, the H-charged peak-aged specimen exhibited a significant increase in initial hardening (dislocation storage) rate relative to the H-charged under-aged specimen. Transmission electron microscopy of these samples revealed the onset of widespread dislocation looping in the H-charged peak-aged sample, in addition to the planar slip bands characteristic of the non-charged condition. This result suggests that hydrogenmore »« less

Authors:

^[1]; Bhattacharyya, Jishnu J. ^[1]; Ronevich, Joseph A. ^[2]; Agnew, Sean R. ^[1]; Burns, James T. ^[1]

Univ. of Virginia, Charlottesville, VA (United States)
Sandia National Lab. (SNL-CA), Livermore, CA (United States)

Publication Date:: Wed Jan 22 00:00:00 EST 2020

Research Org.:: Sandia National Lab. (SNL-CA), Livermore, CA (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA)

OSTI Identifier:: 1601433

Alternate Identifier(s):: OSTI ID: 1703873

Report Number(s):: SAND-2019-11536J
Journal ID: ISSN 1359-6454; 679587

Grant/Contract Number:: AC04-94AL85000; NA-0003525

Resource Type:: Accepted Manuscript

Journal Name:: Acta Materialia

Additional Journal Information:: Journal Volume: 186; Journal Issue: C; Journal ID: ISSN 1359-6454

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Hydrogen embrittlement; Monel K-500; Precipitate–dislocation interactions; Work hardening

Citation Formats


                    Harris, Zachary D., Bhattacharyya, Jishnu J., Ronevich, Joseph A., Agnew, Sean R., and Burns, James T. The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy.  United States: N. p., 2020. 
Web.  doi:10.1016/j.actamat.2020.01.033.

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                    Harris, Zachary D., Bhattacharyya, Jishnu J., Ronevich, Joseph A., Agnew, Sean R., & Burns, James T. The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy.  United States.  https://doi.org/10.1016/j.actamat.2020.01.033

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                    Harris, Zachary D., Bhattacharyya, Jishnu J., Ronevich, Joseph A., Agnew, Sean R., and Burns, James T. Wed .  
"The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy".  United States.  https://doi.org/10.1016/j.actamat.2020.01.033.  https://www.osti.gov/servlets/purl/1601433.

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@article{osti_1601433,

  title        = {The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy},

  author       = {Harris, Zachary D. and Bhattacharyya, Jishnu J. and Ronevich, Joseph A. and Agnew, Sean R. and Burns, James T.},

  abstractNote = {The effect of hydrogen (H) on the deformation behavior of Monel K-500 in various isothermal heat treatment conditions (non-aged, under-aged, peak-aged, and over-aged) was assessed via uniaxial mechanical testing. H-charged and non-charged specimens were strained to failure to facilitate a comparison of ductility, fracture surface morphology, strength, and work hardening behavior. For all examined heat treatment conditions, H charging leads to a significant reduction in ductility, which is accompanied by a consistent change in fracture surface morphology from ductile microvoid coalescence to brittle intergranular fracture. While H charging led to a systematic enhancement in the yield strength of all heat treatments, the three age-hardened conditions exhibited a more than 2-fold increase relative to the non-aged heat treatment. This suggests that H modifies the dislocation–precipitate interactions, which also manifest themselves through changes in work hardening metrics related to the dislocation storage and recovery rates. In particular, the H-charged peak-aged specimen exhibited a significant increase in initial hardening (dislocation storage) rate relative to the H-charged under-aged specimen. Transmission electron microscopy of these samples revealed the onset of widespread dislocation looping in the H-charged peak-aged sample, in addition to the planar slip bands characteristic of the non-charged condition. This result suggests that hydrogen induces the particle shearing-to-looping transition at smaller particle sizes. Possible mechanistic explanations for this observed behavior are presented.},

  doi          = {10.1016/j.actamat.2020.01.033},

  journal      = {Acta Materialia},

  number       = C,

  volume       = 186,

  place        = {United States},

  year         = {Wed Jan 22 00:00:00 EST 2020},

  month        = {Wed Jan 22 00:00:00 EST 2020}

}

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Precipitation hardening in metals
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Title: The combined effects of hydrogen and aging condition on the deformation and fracture behavior of a precipitation-hardened nickel-base superalloy

Abstract

Citation Formats

Mechanisms and Kinetics of Environmentally Assisted Cracking: Current Status, Issues, and Suggestions for Further Work journal, September 2012

Environmentally assisted cracking: Overview of evidence for an adsorption-induced localised-slip process journal, October 1988

Hydrogen-enhanced localized plasticity—a mechanism for hydrogen-related fracture journal, March 1994

The Role of Hydrogen and Other Interstitials in the Mechanical Behavior of Metals: (1959 Edward De Mille Campbell Memorial Lecture) journal, November 2016

Hydrogen related failure of steels – a new aspect journal, August 2004

Effects of grain size and deformation temperature on hydrogen-enhanced vacancy formation in Ni alloys journal, April 2017

Elucidating the contribution of mobile hydrogen-deformation interactions to hydrogen-induced intergranular cracking in polycrystalline nickel journal, October 2018

Hydrogen embrittlement revealed via novel in situ fracture experiments using notched micro-cantilever specimens journal, January 2018

Influence of hydrogen on dislocation self-organization in Ni journal, August 2017

Enumeration of the hydrogen-enhanced localized plasticity mechanism for hydrogen embrittlement in structural materials journal, February 2019

The predominant role of strain-induced vacancies in hydrogen embrittlement of steels: Overview journal, February 2019

The role of atomistic simulations in probing hydrogen effects on plasticity and embrittlement in metals journal, July 2019

A new model for hydrogen-assisted cracking (hydrogen “embrittlement”) journal, February 1972

Hydrogen effects on the interaction between dislocations journal, March 1998

Recent developments in the study of hydrogen embrittlement: Hydrogen effect on dislocation nucleation journal, September 2010

Hydrogen effect on dislocation nucleation in a vanadium (100) single crystal as observed during nanoindentation journal, November 2010

Hydrogen effects on dislocation activity in austenitic stainless steel journal, June 2006

Increase in dislocation density in cold-deformed Pd using H as a temporary alloying addition journal, May 2013

Hardening effects in plastically deformed Pd with the addition of H journal, March 2015

On the measure of dislocation densities from diffraction line profiles: A comparison with discrete dislocation methods journal, February 2012

Role of secondary γ′ precipitation and of hydrogen in the first stage of the plastic deformation of the γ matrix of a Ni base superalloy single crystal journal, January 2002

Mechanism of hydrogen embrittlement in a gamma-prime phase strengthened Fe–Ni based austenitic alloy journal, October 2012

Effect of hydrogen on the dislocation structure of deformed nickel journal, March 1984

The effect of hydrogen on the slip character of nickel journal, July 1980

Revealing deformation microstructures journal, September 2007

The orientation and strain dependence of dislocation structure evolution in monotonically deformed polycrystalline copper journal, June 2015

Physics and phenomenology of strain hardening: the FCC case journal, January 2003

Modelling of work hardening and stress saturation in FCC metals journal, July 1997

Kocks-Mecking analysis of the size effects on the mechanical behavior of nickel polycrystals journal, November 2017

Local strain hardening and nonuniformity of plastic deformation journal, December 1986

Kinetics of Uniaxial Tensile Flow and Work Hardening Behavior of Type 316L(N) Austenitic Stainless Steel in the Framework of Two-Internal-Variable Approach journal, November 2014

A simple model for dislocation behavior, strain and strain rate hardening evolution in deforming aluminum alloys journal, July 2002

Theory of plastic deformation: - properties of low energy dislocation structures journal, July 1989

The influence of precipitation on the work-hardening behavior of the aluminum alloys AA6111 and AA7030 journal, November 2003

Precipitation in the NiCu-base alloy monel K-500 journal, December 1986

A century of monel metal: 1906–2006 journal, September 2006

Precipitation hardening in nickel-copper base alloy monel K 500 journal, December 1993

Coarsening of TiC in austenitic stainless steel — experiments and simulations in comparison journal, July 2000

Hydrogen diffusion and trapping in a precipitation-hardened nickel–copper–aluminum alloy Monel K-500 (UNS N05500) journal, May 2013

A statistical, physical-based, micro-mechanical model of hydrogen-induced intergranular fracture in steel journal, February 2010

The effect of heat-to-heat variations in metallurgy and hydrogen-metal interactions on the hydrogen embrittlement of Monel K-500 journal, August 2017

The Effect of Microstructural Variation on the Hydrogen Environment-Assisted Cracking of Monel K-500 journal, April 2016

The effect of isothermal heat treatment on hydrogen environment-assisted cracking susceptibility in Monel K-500 journal, September 2019

Grain-boundary engineering markedly reduces susceptibility to intergranular hydrogen embrittlement in metallic materials journal, August 2009

The mathematics of diffusion journal, January 1977

Permeability, solubility and diffusivity of hydrogen isotopes in stainless steels at high gas pressures journal, January 2007

Solubility of hydrogen in solid Ni−Co and Ni−Cu alloys journal, September 1971

The thermodynamics of NiCuH solid solutions journal, August 1993

Diffusion Coefficients of Hydrogen in Ni–Cu and Ni–Co Alloys journal, January 1986

Permeation characteristics of some iron and nickel based alloys journal, June 1985

The diffusivity of hydrogen in nickel-based solid solutions journal, January 1988

Measurement and Modeling of Hydrogen Environment-Assisted Cracking in Monel K-500 journal, May 2014

The effect of diffusive hydrogen segregation on fracture of polycrystalline nickel journal, July 1986

Effects of Hydrogen on the Engineering Properties of MONEL Nickel-Copper Alloy K-500 journal, February 1972

Failures of Nickel/Copper Bolts in Subsea Application journal, August 1988

Measurement and Modeling of Hydrogen Environment-Assisted Cracking in a Ni-Cu-Al-Ti Superalloy journal, January 2016

Hydrogen-induced intergranular failure in nickel revisited journal, April 2012

Hydrogen-induced strain localization and failure of austenitic stainless steels at high hydrogen concentrations journal, June 1991

Grain growth phenomena in nickel journal, October 1994

Yielding in nickel as a function of grain or cell size journal, November 1975

Six decades of the Hall–Petch effect – a survey of grain-size strengthening studies on pure metals journal, June 2016

Effect of Interstitial Elements on Hall–Petch Coefficient of Ferritic Iron journal, January 2008

Effect of Grain Boundary Segregation of Interstitial Elements on Hall–Petch Coefficient in Steels journal, January 2014

Effect of ultrafine grain refinement on hydrogen embrittlement of metastable austenitic stainless steel journal, June 2017

The effect of hydrogen on the deformation of iron journal, April 1974

Effect of hydrogen on work hardening of type 304L austenitic stainless steel journal, November 1981

Intercrystalline fracture in hydrogen-charged nickel journal, March 1965

Solid Solution Hardening of Nickel —Role of Transition Metal and B-subgroup Solutes— journal, January 1986

Solid-solution hardening journal, January 1978

Computer simulation of solid solution strengthening in Fcc alloys: Part I. Friedel and mott limits journal, August 1989

Computationally efficient and quantitatively accurate multiscale simulation of solid-solution strengthening by ab initio calculation journal, February 2015

Solute strengthening from first principles and application to aluminum alloys journal, May 2012

Solid solution strengthening in Fe-N single crystals journal, July 1968

The volume increase of fcc metals and alloys due to interstitial hydrogen over a wide range of hydrogen contents journal, May 1971

The effect of solutes on the strength and strain hardening behavior of alloys journal, March 1982

The hardening of metal crystals by precipitate particles journal, May 1953

Work hardening of dispersion-hardened crystals journal, December 1966

Mechanisms and Kinetics of Environmentally Assisted Cracking: Current Status, Issues, and Suggestions for Further Work
journal, September 2012

Environmentally assisted cracking: Overview of evidence for an adsorption-induced localised-slip process
journal, October 1988

Hydrogen-enhanced localized plasticity—a mechanism for hydrogen-related fracture
journal, March 1994

The Role of Hydrogen and Other Interstitials in the Mechanical Behavior of Metals: (1959 Edward De Mille Campbell Memorial Lecture)
journal, November 2016

Hydrogen related failure of steels – a new aspect
journal, August 2004

Effects of grain size and deformation temperature on hydrogen-enhanced vacancy formation in Ni alloys
journal, April 2017

Elucidating the contribution of mobile hydrogen-deformation interactions to hydrogen-induced intergranular cracking in polycrystalline nickel
journal, October 2018

Hydrogen embrittlement revealed via novel in situ fracture experiments using notched micro-cantilever specimens
journal, January 2018

Influence of hydrogen on dislocation self-organization in Ni
journal, August 2017

Enumeration of the hydrogen-enhanced localized plasticity mechanism for hydrogen embrittlement in structural materials
journal, February 2019

The predominant role of strain-induced vacancies in hydrogen embrittlement of steels: Overview
journal, February 2019

The role of atomistic simulations in probing hydrogen effects on plasticity and embrittlement in metals
journal, July 2019

A new model for hydrogen-assisted cracking (hydrogen “embrittlement”)
journal, February 1972

Hydrogen effects on the interaction between dislocations
journal, March 1998

Recent developments in the study of hydrogen embrittlement: Hydrogen effect on dislocation nucleation
journal, September 2010

Hydrogen effect on dislocation nucleation in a vanadium (100) single crystal as observed during nanoindentation
journal, November 2010

Hydrogen effects on dislocation activity in austenitic stainless steel
journal, June 2006

Increase in dislocation density in cold-deformed Pd using H as a temporary alloying addition
journal, May 2013

Hardening effects in plastically deformed Pd with the addition of H
journal, March 2015

On the measure of dislocation densities from diffraction line profiles: A comparison with discrete dislocation methods
journal, February 2012

Role of secondary γ′ precipitation and of hydrogen in the first stage of the plastic deformation of the γ matrix of a Ni base superalloy single crystal
journal, January 2002

Mechanism of hydrogen embrittlement in a gamma-prime phase strengthened Fe–Ni based austenitic alloy
journal, October 2012

Effect of hydrogen on the dislocation structure of deformed nickel
journal, March 1984

The effect of hydrogen on the slip character of nickel
journal, July 1980

Revealing deformation microstructures
journal, September 2007

The orientation and strain dependence of dislocation structure evolution in monotonically deformed polycrystalline copper
journal, June 2015

Physics and phenomenology of strain hardening: the FCC case
journal, January 2003

Modelling of work hardening and stress saturation in FCC metals
journal, July 1997

Kocks-Mecking analysis of the size effects on the mechanical behavior of nickel polycrystals
journal, November 2017

Local strain hardening and nonuniformity of plastic deformation
journal, December 1986

Kinetics of Uniaxial Tensile Flow and Work Hardening Behavior of Type 316L(N) Austenitic Stainless Steel in the Framework of Two-Internal-Variable Approach
journal, November 2014

A simple model for dislocation behavior, strain and strain rate hardening evolution in deforming aluminum alloys
journal, July 2002

Theory of plastic deformation: - properties of low energy dislocation structures
journal, July 1989

The influence of precipitation on the work-hardening behavior of the aluminum alloys AA6111 and AA7030
journal, November 2003

Precipitation in the NiCu-base alloy monel K-500
journal, December 1986

A century of monel metal: 1906–2006
journal, September 2006

Precipitation hardening in nickel-copper base alloy monel K 500
journal, December 1993

Coarsening of TiC in austenitic stainless steel — experiments and simulations in comparison
journal, July 2000

Hydrogen diffusion and trapping in a precipitation-hardened nickel–copper–aluminum alloy Monel K-500 (UNS N05500)
journal, May 2013

A statistical, physical-based, micro-mechanical model of hydrogen-induced intergranular fracture in steel
journal, February 2010

The effect of heat-to-heat variations in metallurgy and hydrogen-metal interactions on the hydrogen embrittlement of Monel K-500
journal, August 2017

The Effect of Microstructural Variation on the Hydrogen Environment-Assisted Cracking of Monel K-500
journal, April 2016

The effect of isothermal heat treatment on hydrogen environment-assisted cracking susceptibility in Monel K-500
journal, September 2019

Grain-boundary engineering markedly reduces susceptibility to intergranular hydrogen embrittlement in metallic materials
journal, August 2009

The mathematics of diffusion
journal, January 1977

Permeability, solubility and diffusivity of hydrogen isotopes in stainless steels at high gas pressures
journal, January 2007

Solubility of hydrogen in solid Ni−Co and Ni−Cu alloys
journal, September 1971

The thermodynamics of NiCuH solid solutions
journal, August 1993

Diffusion Coefficients of Hydrogen in Ni–Cu and Ni–Co Alloys
journal, January 1986

Permeation characteristics of some iron and nickel based alloys
journal, June 1985

The diffusivity of hydrogen in nickel-based solid solutions
journal, January 1988

Measurement and Modeling of Hydrogen Environment-Assisted Cracking in Monel K-500
journal, May 2014

The effect of diffusive hydrogen segregation on fracture of polycrystalline nickel
journal, July 1986

Effects of Hydrogen on the Engineering Properties of MONEL Nickel-Copper Alloy K-500
journal, February 1972

Failures of Nickel/Copper Bolts in Subsea Application
journal, August 1988

Measurement and Modeling of Hydrogen Environment-Assisted Cracking in a Ni-Cu-Al-Ti Superalloy
journal, January 2016

Hydrogen-induced intergranular failure in nickel revisited
journal, April 2012

Hydrogen-induced strain localization and failure of austenitic stainless steels at high hydrogen concentrations
journal, June 1991

Grain growth phenomena in nickel
journal, October 1994

Yielding in nickel as a function of grain or cell size
journal, November 1975

Six decades of the Hall–Petch effect – a survey of grain-size strengthening studies on pure metals
journal, June 2016

Effect of Interstitial Elements on Hall–Petch Coefficient of Ferritic Iron
journal, January 2008

Effect of Grain Boundary Segregation of Interstitial Elements on Hall–Petch Coefficient in Steels
journal, January 2014

Effect of ultrafine grain refinement on hydrogen embrittlement of metastable austenitic stainless steel
journal, June 2017

The effect of hydrogen on the deformation of iron
journal, April 1974

Effect of hydrogen on work hardening of type 304L austenitic stainless steel
journal, November 1981

Intercrystalline fracture in hydrogen-charged nickel
journal, March 1965

Solid Solution Hardening of Nickel —Role of Transition Metal and B-subgroup Solutes—
journal, January 1986

Solid-solution hardening
journal, January 1978

Computer simulation of solid solution strengthening in Fcc alloys: Part I. Friedel and mott limits
journal, August 1989

Computationally efficient and quantitatively accurate multiscale simulation of solid-solution strengthening by ab initio calculation
journal, February 2015

Solute strengthening from first principles and application to aluminum alloys
journal, May 2012

Solid solution strengthening in Fe-N single crystals
journal, July 1968

The volume increase of fcc metals and alloys due to interstitial hydrogen over a wide range of hydrogen contents
journal, May 1971

The effect of solutes on the strength and strain hardening behavior of alloys
journal, March 1982

The hardening of metal crystals by precipitate particles
journal, May 1953

Work hardening of dispersion-hardened crystals
journal, December 1966

The deformation of plastically non-homogeneous materials
journal, February 1970

Work hardening due to internal stresses in composite materials
journal, July 1975

High-temperature deformation mechanisms in a polycrystalline nickel-base superalloy studied by neutron diffraction and electron microscopy
journal, August 2014