Atom Probe Tomography for Catalysis Applications: A Review
Abstract
Atom probe tomography is a well-established analytical instrument for imaging the 3D structure and composition of materials with high mass resolution, sub-nanometer spatial resolution and ppm elemental sensitivity. Thanks to recent hardware developments in Atom Probe Tomography (APT), combined with progress on site-specific focused ion beam (FIB)-based sample preparation methods and improved data treatment software, complex materials can now be routinely investigated. From model samples to complex, usable porous structures, there is currently a growing interest in the analysis of catalytic materials. APT is able to probe the end state of atomic-scale processes, providing information needed to improve the synthesis of catalysts and to unravel structure/composition/reactivity relationships. This review focuses on the study of catalytic materials with increasing complexity (tip-sample, unsupported and supported nanoparticles, powders, self-supported catalysts and zeolites), as well as sample preparation methods developed to obtain suitable specimens for APT experiments.
- Authors:
-
[1];
- Université Libre de Bruxelles, Brussels (Belgium); Harvard Univ., Cambridge, MA (United States)
- Harvard Univ., Cambridge, MA (United States)
- Publication Date:
- Research Org.:
- Energy Frontier Research Centers (EFRC) (United States). Integrated Mesoscale Architectures for Sustainable Catalysis (IMASC); Harvard Univ., Cambridge, MA (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF)
- OSTI Identifier:
- 1595104
- Grant/Contract Number:
- SC0012573; 1541959
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Applied Sciences
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 13; Journal ID: ISSN 2076-3417
- Publisher:
- MDPI
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; atom probe tomography; APT; FIB sample preparation; alloy engineering; core-shell structure; nanoporous catalyst; zeolite; correlative techniques
Citation Formats
Barroo, Cédric, Akey, Austin J., and Bell, David C. Atom Probe Tomography for Catalysis Applications: A Review. United States: N. p., 2019.
Web. doi:10.3390/app9132721.
Barroo, Cédric, Akey, Austin J., & Bell, David C. Atom Probe Tomography for Catalysis Applications: A Review. United States. https://doi.org/10.3390/app9132721
Barroo, Cédric, Akey, Austin J., and Bell, David C. Fri .
"Atom Probe Tomography for Catalysis Applications: A Review". United States. https://doi.org/10.3390/app9132721. https://www.osti.gov/servlets/purl/1595104.
@article{osti_1595104,
title = {Atom Probe Tomography for Catalysis Applications: A Review},
author = {Barroo, Cédric and Akey, Austin J. and Bell, David C.},
abstractNote = {Atom probe tomography is a well-established analytical instrument for imaging the 3D structure and composition of materials with high mass resolution, sub-nanometer spatial resolution and ppm elemental sensitivity. Thanks to recent hardware developments in Atom Probe Tomography (APT), combined with progress on site-specific focused ion beam (FIB)-based sample preparation methods and improved data treatment software, complex materials can now be routinely investigated. From model samples to complex, usable porous structures, there is currently a growing interest in the analysis of catalytic materials. APT is able to probe the end state of atomic-scale processes, providing information needed to improve the synthesis of catalysts and to unravel structure/composition/reactivity relationships. This review focuses on the study of catalytic materials with increasing complexity (tip-sample, unsupported and supported nanoparticles, powders, self-supported catalysts and zeolites), as well as sample preparation methods developed to obtain suitable specimens for APT experiments.},
doi = {10.3390/app9132721},
journal = {Applied Sciences},
number = 13,
volume = 9,
place = {United States},
year = {Fri Jul 05 00:00:00 EDT 2019},
month = {Fri Jul 05 00:00:00 EDT 2019}
}
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