High temperature oxidation of Ni alloys in CO2 containing impurities

Oleksak, Richard P.; Tylczak, Joseph H.; Holcomb, Gordon R.; Doğan, Ömer N.

doi:10.1016/j.corsci.2019.05.019

Title: High temperature oxidation of Ni alloys in CO₂ containing impurities

Abstract

Next-generation power systems need structural alloys resistant to high-temperature oxidation in CO₂ containing combustion impurities. In this report we evaluate the oxidation performance of several commercial Ni alloys exposed to 95%CO₂-4%H₂O-1%O₂, with/without 0.1% SO₂, at 750°C and 1 atm. All alloys formed protective chromia layers and showed no signs of carburization or sulfidation, and minimal chromia volatilization. The microstructural evolution of the alloy surface, secondary oxidants, and minor alloy additions all played a part in promoting protective chromia formation/growth. The results show that Ni alloys are promising candidates for high-temperature portions of next-generation CO₂-based power systems.

Authors:

Oleksak, Richard P. ^[1]; Tylczak, Joseph H. ^[2]; Holcomb, Gordon R. ^[2]; Doğan, Ömer N. ^[2]

National Energy Technology Lab. (NETL), Albany, OR (United States); Leidos, Pittsburgh, PA (United States)
National Energy Technology Lab. (NETL), Albany, OR (United States)

Publication Date:: Wed May 22 00:00:00 EDT 2019

Research Org.:: National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV, and Albany, OR (United States)

Sponsoring Org.:: USDOE Office of Fossil Energy (FE); USDOE Office of Fossil Energy and Carbon Management (FECM)

OSTI Identifier:: 1582376

Alternate Identifier(s):: OSTI ID: 1775691

Report Number(s):: NA
Journal ID: ISSN 0010-938X

Grant/Contract Number:: 89243318CFE000003

Resource Type:: Accepted Manuscript

Journal Name:: Corrosion Science

Additional Journal Information:: Journal Volume: 157; Journal Issue: C; Journal ID: ISSN 0010-938X

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Oleksak, Richard P., Tylczak, Joseph H., Holcomb, Gordon R., and Doğan, Ömer N. High temperature oxidation of Ni alloys in CO2 containing impurities.  United States: N. p., 2019. 
Web.  doi:10.1016/j.corsci.2019.05.019.

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                    Oleksak, Richard P., Tylczak, Joseph H., Holcomb, Gordon R., & Doğan, Ömer N. High temperature oxidation of Ni alloys in CO2 containing impurities.  United States.  https://doi.org/10.1016/j.corsci.2019.05.019

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                    Oleksak, Richard P., Tylczak, Joseph H., Holcomb, Gordon R., and Doğan, Ömer N. Wed .  
"High temperature oxidation of Ni alloys in CO2 containing impurities".  United States.  https://doi.org/10.1016/j.corsci.2019.05.019.  https://www.osti.gov/servlets/purl/1582376.

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@article{osti_1582376,

  title        = {High temperature oxidation of Ni alloys in CO2 containing impurities},

  author       = {Oleksak, Richard P. and Tylczak, Joseph H. and Holcomb, Gordon R. and Doğan, Ömer N.},

  abstractNote = {Next-generation power systems need structural alloys resistant to high-temperature oxidation in CO2 containing combustion impurities. In this report we evaluate the oxidation performance of several commercial Ni alloys exposed to 95%CO2-4%H2O-1%O2, with/without 0.1% SO2, at 750°C and 1 atm. All alloys formed protective chromia layers and showed no signs of carburization or sulfidation, and minimal chromia volatilization. The microstructural evolution of the alloy surface, secondary oxidants, and minor alloy additions all played a part in promoting protective chromia formation/growth. The results show that Ni alloys are promising candidates for high-temperature portions of next-generation CO2-based power systems.},

  doi          = {10.1016/j.corsci.2019.05.019},

  journal      = {Corrosion Science},

  number       = C,

  volume       = 157,

  place        = {United States},

  year         = {Wed May 22 00:00:00 EDT 2019},

  month        = {Wed May 22 00:00:00 EDT 2019}

}

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Works referencing / citing this record:

Effect of Surface Finish on High-Temperature Oxidation of Steels in CO2, Supercritical CO2, and Air
journal, October 2019

Oleksak, Richard P.; Holcomb, Gordon R.; Carney, Casey S.
Oxidation of Metals, Vol. 92, Issue 5-6
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Title: High temperature oxidation of Ni alloys in CO2 containing impurities

Abstract

Citation Formats

Oxy-fuel combustion technology for coal-fired power generation journal, January 2005

Thermodynamic Modelling of the Corrosive Deposits in Oxy-Fuel Fired Boilers journal, September 2008

Influence of novel cycle concepts on the high-temperature corrosion of power plants journal, May 2008

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Chromium Volatilization Rates from Cr2O3 Scales into Flowing Gases Containing Water Vapor journal, November 2006

Steam Oxidation and Chromia Evaporation in Ultrasupercritical Steam Boilers and Turbines journal, January 2009

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Title: High temperature oxidation of Ni alloys in CO₂ containing impurities

Oxy-fuel combustion technology for coal-fired power generation
journal, January 2005

Thermodynamic Modelling of the Corrosive Deposits in Oxy-Fuel Fired Boilers
journal, September 2008

Influence of novel cycle concepts on the high-temperature corrosion of power plants
journal, May 2008

Demonstration of the Allam Cycle: An Update on the Development Status of a High Efficiency Supercritical Carbon Dioxide Power Process Employing Full Carbon Capture
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journal, July 2012

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Effect of pressure on supercritical CO ₂ compatibility of structural alloys at 750 °C : Effect of pressure on supercritical CO
journal, April 2016

Corrosion of Alloy Haynes 230 in High Temperature Supercritical Carbon Dioxide with Oxygen Impurity Additions
journal, October 2016

High-Temperature Oxidation of Commercial Alloys in Supercritical CO2 and Related Power Cycle Environments
journal, June 2018

Effect of Sulphur on the Oxidation Behaviour of Possible Construction Materials for Heat Exchangers in Oxyfuel Plants in the Temperature Range 550–700 °C
journal, September 2017

Effects of Corrosion in Supercritical CO2 on the Microstructural Evolution in 800H Alloy
journal, May 2018

Modeling carbide dissolution in alloy 602 CA during high temperature oxidation
journal, July 2015

Oxidation behaviour and microstructural stability of alloy 625 during long-term exposure in steam
journal, June 2014

Steam Oxidation Evaluation of Fe–Cr Alloys for Accident Tolerant Nuclear Fuel Cladding
journal, March 2017

Hydrogen transport during steam oxidation of iron and nickel alloys
journal, March 2019

Differences in growth mechanisms of oxide scales formed on ODS and conventional wrought alloys
journal, August 1989

Chromium Volatilization Rates from Cr2O3 Scales into Flowing Gases Containing Water Vapor
journal, November 2006

Steam Oxidation and Chromia Evaporation in Ultrasupercritical Steam Boilers and Turbines
journal, January 2009

Theoretical and Experimental Investigation of the Thermochemistry of CrO ₂ (OH) ₂ (g)
journal, March 2007

The effect of manganese additions on the reactive evaporation of chromium in Ni–Cr alloys
journal, May 2006

A review of the oxidation behaviour of structural alloys in steam
journal, May 2010

Indication of Chromium Oxide Hydroxide Evaporation During Oxidation of 304L at 873 K in the Presence of 10% Water Vapor
journal, January 1999

Predicting Oxidation-Limited Lifetime of Thin-Walled Components of NiCrW Alloy 230
journal, October 2016

Type 304 Stainless Steel vs Flowing CO ₂ At Atmospheric Pressure and 1100-1800F
journal, March 1965

Effect of Alloy Composition and Exposure Conditions on the Selective Oxidation Behavior of Ferritic Fe–Cr and Fe–Cr–X Alloys
journal, September 2010

Mechanisms of Oxide Scale Formation on Ferritic Interconnect Steel in Simulated Low and High pO2 Service Environments of Solid Oxide Fuel Cells
journal, June 2014

Oxidation behaviour of some modern heat-resistant cast steels
journal, November 1982

Influence of silicon additions on the oxidation resistance of a stainless steel
journal, February 1983

Effects of Silicon on the Oxidation Behavior of Ni-Base Chromia-Forming Alloys
journal, June 2006

Chromia layer growth on a Ni-based superalloy: Sub-parabolic kinetics and the role of titanium
journal, October 2013

Phase studies in the chromium-manganese-titanium oxide system at different oxygen partial pressures
journal, January 1991

Effect of Surface Finish on High-Temperature Oxidation of Steels in CO2, Supercritical CO2, and Air
journal, October 2019