Modified Bridgman anvils for high pressure synthesis and neutron scattering
Abstract
A simple modified Bridgman design for large volume pressure anvils usable in the Paris-Edinburgh (PE) press has been demonstrated at Oak Ridge National Laboratory Spallation Neutron Source. The design shows advantages over the toroidal anvils typically used in the PE press, mainly rapid compression/decompression rates, complete absence of blow-outs upon drastic phase transitions, simplified cooling, high reliability, and relative low loads (~40 tons) corresponding to relatively high pressures (~20 GPa). It also shows advantages over existing large-volume diamond cells as sample volumes of ~2-3 mm3 can be easily and rapidly synthesized. The anvils thus allow sample sizes sufficient for in situ neutron diffraction as well as rapid synthesis of adequate amounts of new materials for ex situ analysis via total neutron scattering and neutron spectroscopy.
- Authors:
-
[1];
[1];
[1];
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Sciences Directorate, Neutron Scattering Div.
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Neutron Sciences Directorate, Neutron Scattering Div.; Carnegie Inst. for Science, Washington, DC (United States). Geophysical Lab.
- Publication Date:
- Research Org.:
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1567003
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- High Pressure Research
- Additional Journal Information:
- Journal Volume: 39; Journal Issue: 3; Journal ID: ISSN 0895-7959
- Publisher:
- Taylor & Francis
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 73 NUCLEAR PHYSICS AND RADIATION PHYSICS; high pressure neutron scattering; high pressure materials synthesis; pure amorphous silicon; germanium
Citation Formats
Haberl, Bianca, Molaison, Jamie J., Neuefeind, Joerg C., Daemen, Luke L., and Boehler, Reinhard. Modified Bridgman anvils for high pressure synthesis and neutron scattering. United States: N. p., 2019.
Web. doi:10.1080/08957959.2019.1624744.
Haberl, Bianca, Molaison, Jamie J., Neuefeind, Joerg C., Daemen, Luke L., & Boehler, Reinhard. Modified Bridgman anvils for high pressure synthesis and neutron scattering. United States. https://doi.org/10.1080/08957959.2019.1624744
Haberl, Bianca, Molaison, Jamie J., Neuefeind, Joerg C., Daemen, Luke L., and Boehler, Reinhard. Sun .
"Modified Bridgman anvils for high pressure synthesis and neutron scattering". United States. https://doi.org/10.1080/08957959.2019.1624744. https://www.osti.gov/servlets/purl/1567003.
@article{osti_1567003,
title = {Modified Bridgman anvils for high pressure synthesis and neutron scattering},
author = {Haberl, Bianca and Molaison, Jamie J. and Neuefeind, Joerg C. and Daemen, Luke L. and Boehler, Reinhard},
abstractNote = {A simple modified Bridgman design for large volume pressure anvils usable in the Paris-Edinburgh (PE) press has been demonstrated at Oak Ridge National Laboratory Spallation Neutron Source. The design shows advantages over the toroidal anvils typically used in the PE press, mainly rapid compression/decompression rates, complete absence of blow-outs upon drastic phase transitions, simplified cooling, high reliability, and relative low loads (~40 tons) corresponding to relatively high pressures (~20 GPa). It also shows advantages over existing large-volume diamond cells as sample volumes of ~2-3 mm3 can be easily and rapidly synthesized. The anvils thus allow sample sizes sufficient for in situ neutron diffraction as well as rapid synthesis of adequate amounts of new materials for ex situ analysis via total neutron scattering and neutron spectroscopy.},
doi = {10.1080/08957959.2019.1624744},
journal = {High Pressure Research},
number = 3,
volume = 39,
place = {United States},
year = {Sun Jun 16 00:00:00 EDT 2019},
month = {Sun Jun 16 00:00:00 EDT 2019}
}
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