Observation of the shock-induced β-Sn to b.c.t.-Sn transition using time-resolved X-ray diffraction
Abstract
Time-resolved X-ray diffraction measurements have been carried out here on dynamically compressed Sn up to a maximum pressure of ~13 GPa at the European Synchrotron Radiation Facility. The phase transition from β-Sn to body-centered tetragonal (b.c.t.) Sn has been observed using synchrotron X-ray diffraction for the first time undergoing shock compression and release. Following maximum compression, the sample releases to lower pressures for several nanoseconds until the reverse transition occurs. The data are in good agreement with previous shock boundaries that indicate that the β-Sn phase is stable ~2 GPa higher than the static boundary upon compression and the b.c.t.-Sn phase is stable ~1 GPa lower upon release. The transition to the high-pressure phase reveals a loss of texture in the X-ray diffraction data from the `quasi' single-crystal β-Sn structure to a more powder-like Debye–Scherrer ring.
- Authors:
-
- European Synchrotron Radiation Facility (ESRF), Grenoble (France); Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- European Synchrotron Radiation Facility (ESRF), Grenoble (France)
- Alternative Energies and Atomic Energy Commission (CEA), Arpajon (France)
- Publication Date:
- Research Org.:
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); European Synchrotron Radiation Facility (ESRF), Grenoble (France)
- Sponsoring Org.:
- USDOE National Nuclear Security Administration (NNSA); European Union (EU)
- OSTI Identifier:
- 1497280
- Report Number(s):
- LLNL-JRNL-747397
Journal ID: ISSN 1600-5775; 931131
- Grant/Contract Number:
- AC52-07NA27344; 654220
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Synchrotron Radiation (Online)
- Additional Journal Information:
- Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 26; Journal Issue: 1; Journal ID: ISSN 1600-5775
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; time-resolved X-ray diffraction; shock compression; phase boundaries
Citation Formats
Briggs, R., Torchio, R., Sollier, A., Occelli, F., Videau, L., Kretzschmar, N., and Wulff, M. Observation of the shock-induced β-Sn to b.c.t.-Sn transition using time-resolved X-ray diffraction. United States: N. p., 2019.
Web. doi:10.1107/S1600577518015059.
Briggs, R., Torchio, R., Sollier, A., Occelli, F., Videau, L., Kretzschmar, N., & Wulff, M. Observation of the shock-induced β-Sn to b.c.t.-Sn transition using time-resolved X-ray diffraction. United States. https://doi.org/10.1107/S1600577518015059
Briggs, R., Torchio, R., Sollier, A., Occelli, F., Videau, L., Kretzschmar, N., and Wulff, M. Tue .
"Observation of the shock-induced β-Sn to b.c.t.-Sn transition using time-resolved X-ray diffraction". United States. https://doi.org/10.1107/S1600577518015059. https://www.osti.gov/servlets/purl/1497280.
@article{osti_1497280,
title = {Observation of the shock-induced β-Sn to b.c.t.-Sn transition using time-resolved X-ray diffraction},
author = {Briggs, R. and Torchio, R. and Sollier, A. and Occelli, F. and Videau, L. and Kretzschmar, N. and Wulff, M.},
abstractNote = {Time-resolved X-ray diffraction measurements have been carried out here on dynamically compressed Sn up to a maximum pressure of ~13 GPa at the European Synchrotron Radiation Facility. The phase transition from β-Sn to body-centered tetragonal (b.c.t.) Sn has been observed using synchrotron X-ray diffraction for the first time undergoing shock compression and release. Following maximum compression, the sample releases to lower pressures for several nanoseconds until the reverse transition occurs. The data are in good agreement with previous shock boundaries that indicate that the β-Sn phase is stable ~2 GPa higher than the static boundary upon compression and the b.c.t.-Sn phase is stable ~1 GPa lower upon release. The transition to the high-pressure phase reveals a loss of texture in the X-ray diffraction data from the `quasi' single-crystal β-Sn structure to a more powder-like Debye–Scherrer ring.},
doi = {10.1107/S1600577518015059},
journal = {Journal of Synchrotron Radiation (Online)},
number = 1,
volume = 26,
place = {United States},
year = {Tue Jan 01 00:00:00 EST 2019},
month = {Tue Jan 01 00:00:00 EST 2019}
}
Web of Science
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