Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source

Li, Luxi; Xie, Yingying; Maxey, Evan; Harder, Ross

doi:10.1107/S1600577518016697

Title: Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source

Abstract

Bragg coherent X-ray diffraction imaging has become valuable for visualization of the structural, morphological and strain evolution of crystals in operando electrode materials. As the electrode material particles (either in a single-crystal form or an aggregation form of single crystals) are evenly dispersed and randomly oriented in the electrode laminate, the submicrometer-sized coherent X-ray beam can be used to probe the local properties of electrode material crystals using two approaches. Coherent multi-crystal diffraction provides collective structural information of phase transitions in tens of crystals simultaneously as well as the individual behavior from single crystals, which are oriented at the Bragg condition in the X-ray illumination volume. Bragg coherent diffractive imaging enables one to monitor the evolution of the morphology and strain in individual crystals. This work explores and highlights the Bragg coherent X-ray diffraction measurements of battery electrode materials in operando conditions at the 34-ID-C beamline at the Advanced Photon Source. The experiment is demonstrated with NaNi_1/3Fe_1/3Mn_1/3O₂, a sodium-ion cathode material loaded in a half cell. Furthermore, the paper will discuss, in detail, the beamline setup, sample mounting and handling, alignment strategies and the data acquisition protocols.

Authors:

Li, Luxi ^[1]; Xie, Yingying ^[2];

^[1];

^[1]

Argonne National Lab. (ANL), Lemont, IL (United States)
Shanghai Jiao Tong Univ., Shanghai (People's Republic of China); Argonne National Lab. (ANL), Lemont, IL (United States)

Publication Date:: Tue Jan 01 00:00:00 EST 2019

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC)

OSTI Identifier:: 1494301

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Journal of Synchrotron Radiation (Online)

Additional Journal Information:: Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 26; Journal Issue: 1; Journal ID: ISSN 1600-5775

Publisher:: International Union of Crystallography

Country of Publication:: United States

Language:: English

Subject:: 73 NUCLEAR PHYSICS AND RADIATION PHYSICS; coherent multi-crystal diffraction; Bragg coherent diffractive imaging; in operando characterization of battery materials; experimental protocols

Citation Formats


                    Li, Luxi, Xie, Yingying, Maxey, Evan, and Harder, Ross. Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source.  United States: N. p., 2019. 
Web.  doi:10.1107/S1600577518016697.

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                    Li, Luxi, Xie, Yingying, Maxey, Evan, & Harder, Ross. Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source.  United States.  https://doi.org/10.1107/S1600577518016697

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                    Li, Luxi, Xie, Yingying, Maxey, Evan, and Harder, Ross. Tue .  
"Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source".  United States.  https://doi.org/10.1107/S1600577518016697.  https://www.osti.gov/servlets/purl/1494301.

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@article{osti_1494301,

  title        = {Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source},

  author       = {Li, Luxi and Xie, Yingying and Maxey, Evan and Harder, Ross},

  abstractNote = {Bragg coherent X-ray diffraction imaging has become valuable for visualization of the structural, morphological and strain evolution of crystals in operando electrode materials. As the electrode material particles (either in a single-crystal form or an aggregation form of single crystals) are evenly dispersed and randomly oriented in the electrode laminate, the submicrometer-sized coherent X-ray beam can be used to probe the local properties of electrode material crystals using two approaches. Coherent multi-crystal diffraction provides collective structural information of phase transitions in tens of crystals simultaneously as well as the individual behavior from single crystals, which are oriented at the Bragg condition in the X-ray illumination volume. Bragg coherent diffractive imaging enables one to monitor the evolution of the morphology and strain in individual crystals. This work explores and highlights the Bragg coherent X-ray diffraction measurements of battery electrode materials in operando conditions at the 34-ID-C beamline at the Advanced Photon Source. The experiment is demonstrated with NaNi1/3Fe1/3Mn1/3O2, a sodium-ion cathode material loaded in a half cell. Furthermore, the paper will discuss, in detail, the beamline setup, sample mounting and handling, alignment strategies and the data acquisition protocols.},

  doi          = {10.1107/S1600577518016697},

  journal      = {Journal of Synchrotron Radiation (Online)},

  number       = 1,

  volume       = 26,

  place        = {United States},

  year         = {Tue Jan 01 00:00:00 EST 2019},

  month        = {Tue Jan 01 00:00:00 EST 2019}

}

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Works referencing / citing this record:

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Title: Methods for operando coherent X-ray diffraction of battery materials at the Advanced Photon Source

Abstract

Citation Formats

The effect of exit beam phase aberrations on parallel beam coherent x-ray reconstructions journal, December 2010

Synchrotron X-Ray and Neutron Diffraction, Total Scattering, and Small-Angle Scattering Techniques for Rechargeable Battery Research journal, June 2018

Three-dimensional imaging of strain in a single ZnO nanorod journal, December 2009

Topological defect dynamics in operando battery nanoparticles journal, June 2015

Extending the methodology of X-ray crystallography to allow imaging of micrometre-sized non-crystalline specimens journal, July 1999

Performance evaluation of Bragg coherent diffraction imaging journal, October 2017

Three-Dimensional Imaging of Microstructure in Au Nanocrystals journal, April 2003

Reconstructing symmetric images from their undersampled Fourier intensities journal, January 1997

Observation of x-ray radiation pressure effects on nanocrystals journal, October 2016

Watching the Growth of Bulk Grains During Recrystallization of Deformed Metals journal, July 2004

Electron microscopy by specimen design: application to strain measurements journal, September 2017

High-resolution three-dimensional partially coherent diffraction imaging journal, January 2012

Formation of Optical Images by X-Rays journal, January 1948

Phase retrieval algorithms: a comparison journal, January 1982

Mechanical breakdown of bent silicon nanowires imaged by coherent x-ray diffraction journal, December 2013

In situ chemical mapping of a lithium-ion battery using full-field hard X-ray spectroscopic imaging journal, January 2013

Single Particle Nanomechanics in Operando Batteries via Lensless Strain Mapping journal, August 2014

Radiation-driven rotational motion of nanoparticles journal, April 2018

Nonequilibrium Structural Dynamics of Nanoparticles in LiNi 1/2 Mn 3/2 O 4 Cathode under Operando Conditions journal, August 2014

Nucleation of dislocations and their dynamics in layered oxide cathode materials during battery charging journal, July 2018

Three-dimensional X-ray structural microscopy with submicrometre resolution journal, February 2002

Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction journal, October 2001

The AMPIX electrochemical cell: a versatile apparatus for in situ X-ray scattering and spectroscopic measurements journal, November 2012

Some implications of a theorem due to Shannon journal, November 1952

In situ strain evolution during a disconnection event in a battery nanoparticle journal, January 2015

Three-dimensional imaging of dislocation propagation during crystal growth and dissolution journal, June 2015

Nanoscale holographic interferometry for strain measurements in electronic devices journal, June 2008

Nanoscale strain mapping in battery nanostructures journal, February 2014

Visualization of Electrochemical Reactions in Battery Materials with X-ray Microscopy and Mapping journal, April 2017

Nucleation of dislocations and their dynamics in layered oxide cathode materials during battery charging text, January 2018

Performance evaluation of Bragg coherent diffraction imaging text, January 2017

Watching the Growth of Bulk Grains During Recrystallization of Deformed Metals. journal, September 2004

Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction text, January 2001

Domain Texture of the Orthorhombic Phase of La2−xBaxCuO4 journal, August 2019

Coherent Bragg imaging of 60 nm Au nanoparticles under electrochemical control at the NanoMAX beamline journal, August 2019

The effect of exit beam phase aberrations on parallel beam coherent x-ray reconstructions
journal, December 2010

Synchrotron X-Ray and Neutron Diffraction, Total Scattering, and Small-Angle Scattering Techniques for Rechargeable Battery Research
journal, June 2018

Three-dimensional imaging of strain in a single ZnO nanorod
journal, December 2009

Topological defect dynamics in operando battery nanoparticles
journal, June 2015

Extending the methodology of X-ray crystallography to allow imaging of micrometre-sized non-crystalline specimens
journal, July 1999

Performance evaluation of Bragg coherent diffraction imaging
journal, October 2017

Three-Dimensional Imaging of Microstructure in Au Nanocrystals
journal, April 2003

Reconstructing symmetric images from their undersampled Fourier intensities
journal, January 1997

Observation of x-ray radiation pressure effects on nanocrystals
journal, October 2016

Watching the Growth of Bulk Grains During Recrystallization of Deformed Metals
journal, July 2004

Electron microscopy by specimen design: application to strain measurements
journal, September 2017

High-resolution three-dimensional partially coherent diffraction imaging
journal, January 2012

Formation of Optical Images by X-Rays
journal, January 1948

Phase retrieval algorithms: a comparison
journal, January 1982

Mechanical breakdown of bent silicon nanowires imaged by coherent x-ray diffraction
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In situ chemical mapping of a lithium-ion battery using full-field hard X-ray spectroscopic imaging
journal, January 2013

Single Particle Nanomechanics in Operando Batteries via Lensless Strain Mapping
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Radiation-driven rotational motion of nanoparticles
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Some implications of a theorem due to Shannon
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In situ strain evolution during a disconnection event in a battery nanoparticle
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Three-dimensional imaging of dislocation propagation during crystal growth and dissolution
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Nanoscale holographic interferometry for strain measurements in electronic devices
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Nanoscale strain mapping in battery nanostructures
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Visualization of Electrochemical Reactions in Battery Materials with X-ray Microscopy and Mapping
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Nucleation of dislocations and their dynamics in layered oxide cathode materials during battery charging
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Performance evaluation of Bragg coherent diffraction imaging
text, January 2017

Watching the Growth of Bulk Grains During Recrystallization of Deformed Metals.
journal, September 2004

Reconstruction of the Shapes of Gold Nanocrystals Using Coherent X-Ray Diffraction
text, January 2001

Domain Texture of the Orthorhombic Phase of La2−xBaxCuO4
journal, August 2019

Coherent Bragg imaging of 60 nm Au nanoparticles under electrochemical control at the NanoMAX beamline
journal, August 2019