In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys

Singh, Sudhanshu S.; Stannard, Tyler J.; Xiao, Xianghui; Chawla, Nikhilesh

doi:10.1007/s11837-017-2413-8

Title: In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys

Abstract

Structural materials are subjected to combinations of stress and corrosive environments that work synergistically to cause premature failure. Therefore, studies on the combined effect of stress and corrosive environments on material behavior are required. Existing studies have been performed in two dimensions that are inadequate for full comprehension of the three-dimensional (3D) processes related to stress corrosion cracking (SCC) and corrosion-fatigue (CF) behavior. Recently, x-ray synchrotron tomography has evolved as an excellent technique to obtain the microstructure in 3D. Moreover, being nondestructive in nature, x-ray synchrotron tomography is well suited to study the evolution of microstructure with time (4D, or fourth dimension in time). Furthermore, this article presents our recent 4D studies on SCC and CF of Al 7075 alloys using x-ray synchrotron tomography.

Authors:

Singh, Sudhanshu S. ^[1]; Stannard, Tyler J. ^[2]; Xiao, Xianghui ^[3]; Chawla, Nikhilesh ^[2]

Indian Institute of Technology Kanpur, Kanpur (India)
Arizona State Univ., Tempe, AZ (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)

Publication Date:: Mon Jun 12 00:00:00 EDT 2017

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: US Department of the Navy, Office of Naval Research (ONR); USDOE

OSTI Identifier:: 1477005

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: JOM. Journal of the Minerals, Metals & Materials Society

Additional Journal Information:: Journal Volume: 69; Journal Issue: 8; Journal ID: ISSN 1047-4838

Publisher:: Springer

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; aluminum alloys; corrosion-fatigue; in situ; loading stage; stress corrosion cracking; x-ray tomography

Citation Formats


                    Singh, Sudhanshu S., Stannard, Tyler J., Xiao, Xianghui, and Chawla, Nikhilesh. In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys.  United States: N. p., 2017. 
Web.  doi:10.1007/s11837-017-2413-8.

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                    Singh, Sudhanshu S., Stannard, Tyler J., Xiao, Xianghui, & Chawla, Nikhilesh. In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys.  United States.  https://doi.org/10.1007/s11837-017-2413-8

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                    Singh, Sudhanshu S., Stannard, Tyler J., Xiao, Xianghui, and Chawla, Nikhilesh. Mon .  
"In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys".  United States.  https://doi.org/10.1007/s11837-017-2413-8.  https://www.osti.gov/servlets/purl/1477005.

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@article{osti_1477005,

  title        = {In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys},

  author       = {Singh, Sudhanshu S. and Stannard, Tyler J. and Xiao, Xianghui and Chawla, Nikhilesh},

  abstractNote = {Structural materials are subjected to combinations of stress and corrosive environments that work synergistically to cause premature failure. Therefore, studies on the combined effect of stress and corrosive environments on material behavior are required. Existing studies have been performed in two dimensions that are inadequate for full comprehension of the three-dimensional (3D) processes related to stress corrosion cracking (SCC) and corrosion-fatigue (CF) behavior. Recently, x-ray synchrotron tomography has evolved as an excellent technique to obtain the microstructure in 3D. Moreover, being nondestructive in nature, x-ray synchrotron tomography is well suited to study the evolution of microstructure with time (4D, or fourth dimension in time). Furthermore, this article presents our recent 4D studies on SCC and CF of Al 7075 alloys using x-ray synchrotron tomography.},

  doi          = {10.1007/s11837-017-2413-8},

  journal      = {JOM. Journal of the Minerals, Metals & Materials Society},

  number       = 8,

  volume       = 69,

  place        = {United States},

  year         = {Mon Jun 12 00:00:00 EDT 2017},

  month        = {Mon Jun 12 00:00:00 EDT 2017}

}

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Initiation and short crack growth behaviour of environmentally induced cracks in AA5083 H131 investigated across time and length scales
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Title: In Situ X-ray Microtomography of Stress Corrosion Cracking and Corrosion Fatigue in Aluminum Alloys

Abstract

Citation Formats

Electrochemical aspects of exfoliation corrosion of aluminium alloys: The effects of heat treatment journal, April 2011

Effect of Loading History on Stress Corrosion Cracking of 7075-T651 Aluminum Alloy in Saline Aqueous Environment journal, November 2010

In situ 3D quantification of the evolution of creep cavity size, shape, and spatial orientation using synchrotron X-ray tomography journal, April 2008

Discontinuous surface cracks during stress corrosion cracking of stainless steel single crystal journal, November 2011

Three dimensional observations and modelling of intergranular stress corrosion cracking in austenitic stainless steel journal, June 2006

Electrochemical Behavior and Localized Corrosion Associated with Mg2Si Particles in Al and Mg Alloys journal, January 2012

Development of a lab-scale, high-resolution, tube-generated X-ray computed-tomography system for three-dimensional (3D) materials characterization journal, June 2014

Recent advances in X-ray microtomography applied to materials journal, May 2008

On the Application of X-ray Microtomography in the Field of Materials Science journal, August 2001

In situ X-ray synchrotron tomographic imaging during the compression of hyper-elastic polymeric materials journal, September 2015

Assessment of the fatigue crack closure phenomenon in damage-tolerant aluminium alloy by in-situ high-resolution synchrotron X-ray microtomography journal, July 2003

Stability Analysis of the Mg2Si Phase in AA 6061 Aluminum Alloy journal, January 2012

Relationship between alloy composition, microstructure and exfoliation corrosion in Al–Zn–Mg–Cu alloys journal, October 2011

Fast X-ray tomography and acoustic emission study of damage in metals during continuous tensile tests journal, December 2007

Characterisation of thermal cycling induced cavitation in particle reinforced metal matrix composites by three-dimensional (3D) X-ray synchrotron tomography journal, May 2014

Direct observation of crack opening as a function of applied load in the interior of a notched tensile sample of AlLi 2090 journal, May 1997

Fatigue crack growth in SiC particle reinforced Al alloy matrix composites at high and low R-ratios by in situ X-ray synchrotron tomography journal, November 2014

Influence of temper and surface condition on the exfoliation behaviour of high strength Al–Zn–Mg–Cu alloys journal, March 2007

A Study of Pb-Rich Dendrites in a Near-Eutectic 63Sn-37Pb Solder Microstructure via Laboratory-Scale Micro X-ray Computed Tomography (μXCT) journal, September 2014

Understanding fatigue crack growth in aluminum alloys by in situ X-ray synchrotron tomography journal, December 2013

Investigation and Discussion of Characteristics for Intermetallic Phases Common to Aluminum Alloys as a Function of Solution pH journal, January 2008

Three-Dimensional Microstructure Visualization of Porosity and Fe-Rich Inclusions in SiC Particle-Reinforced Al Alloy Matrix Composites by X-Ray Synchrotron Tomography journal, May 2010

Elastic-plastic analysis of edge-notched panels subjected to fixed grip loading journal, January 1991

Characterization of Damage Evolution in SiC Particle Reinforced Al Alloy Matrix Composites by In-Situ X-Ray Synchrotron Tomography journal, May 2011

Fatigue and Damage in Structural Materials Studied by X-Ray Tomography journal, August 2012

Measurement of localized corrosion rates at inclusion particles in AA7075 by in situ three dimensional (3D) X-ray synchrotron tomography journal, March 2016

Synchrotron-Based X-ray Computed Tomography During Compression Loading of Cellular Materials journal, April 2015

Observations of Intergranular Stress Corrosion Cracking in a Grain-Mapped Polycrystal journal, July 2008

In situ high resolution synchrotron x-ray tomography of fatigue crack closure micromechanisms journal, August 2004

Mechanical properties of intermetallic inclusions in Al 7075 alloys by micropillar compression journal, July 2015

X-ray microtomographic observation of intergranular stress corrosion cracking in sensitised austenitic stainless steel journal, September 2006

In Situ Investigation of High Humidity Stress Corrosion Cracking of 7075 Aluminum Alloy by Three-Dimensional (3D) X-ray Synchrotron Tomography journal, May 2014

Quantitative X-ray tomography journal, December 2013

Damage quantification in aluminium alloys using in situ tensile tests in X-ray tomography journal, October 2011

Three dimensional microstructural characterization of nanoscale precipitates in AA7075-T651 by focused ion beam (FIB) tomography journal, August 2016

In Situ Experiments with X ray Tomography: an Attractive Tool for Experimental Mechanics journal, January 2010

In situ experimental techniques to study the mechanical behavior of materials using X-ray synchrotron tomography journal, April 2014

In-Situ Synchrotron X-Ray Microtomography Studies of Microstructure and Damage Evolution in Engineering Materials journal, November 2007

3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation journal, July 2014

3D imaging in material science: Application of X-ray tomography journal, November 2010

Damage evolution in SiC particle reinforced Al alloy matrix composites by X-ray synchrotron tomography journal, October 2010

Fracture Mechanics book, June 2005

Initiation and short crack growth behaviour of environmentally induced cracks in AA5083 H131 investigated across time and length scales journal, September 2019

Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography journal, September 2018

Electrochemical aspects of exfoliation corrosion of aluminium alloys: The effects of heat treatment
journal, April 2011

Effect of Loading History on Stress Corrosion Cracking of 7075-T651 Aluminum Alloy in Saline Aqueous Environment
journal, November 2010

In situ 3D quantification of the evolution of creep cavity size, shape, and spatial orientation using synchrotron X-ray tomography
journal, April 2008

Discontinuous surface cracks during stress corrosion cracking of stainless steel single crystal
journal, November 2011

Three dimensional observations and modelling of intergranular stress corrosion cracking in austenitic stainless steel
journal, June 2006

Electrochemical Behavior and Localized Corrosion Associated with Mg2Si Particles in Al and Mg Alloys
journal, January 2012

Development of a lab-scale, high-resolution, tube-generated X-ray computed-tomography system for three-dimensional (3D) materials characterization
journal, June 2014

Recent advances in X-ray microtomography applied to materials
journal, May 2008

On the Application of X-ray Microtomography in the Field of Materials Science
journal, August 2001

In situ X-ray synchrotron tomographic imaging during the compression of hyper-elastic polymeric materials
journal, September 2015

Assessment of the fatigue crack closure phenomenon in damage-tolerant aluminium alloy by in-situ high-resolution synchrotron X-ray microtomography
journal, July 2003

Stability Analysis of the Mg2Si Phase in AA 6061 Aluminum Alloy
journal, January 2012

Relationship between alloy composition, microstructure and exfoliation corrosion in Al–Zn–Mg–Cu alloys
journal, October 2011

Fast X-ray tomography and acoustic emission study of damage in metals during continuous tensile tests
journal, December 2007

Characterisation of thermal cycling induced cavitation in particle reinforced metal matrix composites by three-dimensional (3D) X-ray synchrotron tomography
journal, May 2014

Direct observation of crack opening as a function of applied load in the interior of a notched tensile sample of AlLi 2090
journal, May 1997

Fatigue crack growth in SiC particle reinforced Al alloy matrix composites at high and low R-ratios by in situ X-ray synchrotron tomography
journal, November 2014

Influence of temper and surface condition on the exfoliation behaviour of high strength Al–Zn–Mg–Cu alloys
journal, March 2007

A Study of Pb-Rich Dendrites in a Near-Eutectic 63Sn-37Pb Solder Microstructure via Laboratory-Scale Micro X-ray Computed Tomography (μXCT)
journal, September 2014

Understanding fatigue crack growth in aluminum alloys by in situ X-ray synchrotron tomography
journal, December 2013

Investigation and Discussion of Characteristics for Intermetallic Phases Common to Aluminum Alloys as a Function of Solution pH
journal, January 2008

Three-Dimensional Microstructure Visualization of Porosity and Fe-Rich Inclusions in SiC Particle-Reinforced Al Alloy Matrix Composites by X-Ray Synchrotron Tomography
journal, May 2010

Elastic-plastic analysis of edge-notched panels subjected to fixed grip loading
journal, January 1991

Characterization of Damage Evolution in SiC Particle Reinforced Al Alloy Matrix Composites by In-Situ X-Ray Synchrotron Tomography
journal, May 2011

Fatigue and Damage in Structural Materials Studied by X-Ray Tomography
journal, August 2012

Measurement of localized corrosion rates at inclusion particles in AA7075 by in situ three dimensional (3D) X-ray synchrotron tomography
journal, March 2016

Synchrotron-Based X-ray Computed Tomography During Compression Loading of Cellular Materials
journal, April 2015

Observations of Intergranular Stress Corrosion Cracking in a Grain-Mapped Polycrystal
journal, July 2008

In situ high resolution synchrotron x-ray tomography of fatigue crack closure micromechanisms
journal, August 2004

Mechanical properties of intermetallic inclusions in Al 7075 alloys by micropillar compression
journal, July 2015

X-ray microtomographic observation of intergranular stress corrosion cracking in sensitised austenitic stainless steel
journal, September 2006

In Situ Investigation of High Humidity Stress Corrosion Cracking of 7075 Aluminum Alloy by Three-Dimensional (3D) X-ray Synchrotron Tomography
journal, May 2014

Quantitative X-ray tomography
journal, December 2013

Damage quantification in aluminium alloys using in situ tensile tests in X-ray tomography
journal, October 2011

Three dimensional microstructural characterization of nanoscale precipitates in AA7075-T651 by focused ion beam (FIB) tomography
journal, August 2016

In Situ Experiments with X ray Tomography: an Attractive Tool for Experimental Mechanics
journal, January 2010

In situ experimental techniques to study the mechanical behavior of materials using X-ray synchrotron tomography
journal, April 2014

In-Situ Synchrotron X-Ray Microtomography Studies of Microstructure and Damage Evolution in Engineering Materials
journal, November 2007

3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation
journal, July 2014

3D imaging in material science: Application of X-ray tomography
journal, November 2010

Damage evolution in SiC particle reinforced Al alloy matrix composites by X-ray synchrotron tomography
journal, October 2010

Fracture Mechanics
book, June 2005

Initiation and short crack growth behaviour of environmentally induced cracks in AA5083 H131 investigated across time and length scales
journal, September 2019

Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography
journal, September 2018