Process-Defect-Structure-Property Correlations During Laser Powder Bed Fusion of Alloy 718: Role of In Situ and Ex Situ Characterizations
Abstract
Components made by laser powder bed fusion (L-PBF) additive processes require extensive trial and error optimization to minimize defects and arrive at targeted microstructure and properties. In this paper, in situ infrared thermography and ex situ surface roughness measurements were explored as methodologies to ensure Inconel® 718-part quality. For a given laser energy of 200 Watts, prismatic samples were produced with different exposure times (80 to 110 µs) and point spacings (80 to 110 µm). The infrared intensities from laser–material interaction zones were measured spatially and temporally. The conditions leading to higher IR intensity and lowest surface roughness values correlated well with less porosity and coarse solidification grain structure. The transition from highly columnar to misoriented growth is attributed to changes in thermal gradients and liquid–solid interface velocities. Hardness measurements and electron microscopy of the as-processed and post-processed heat-treated samples show complex transitions in microstructural states including the heavily dislocated FCC matrix, reduction of dislocation density, and copious precipitation, respectively. These results show that the geometry-process-structure-property correlations are dynamic, and they cascade depending on the transitions of phase states from powder to liquid to solid, as well as phase decompositions and deformations within the solid FCC phase. Finally, validity ofmore »
- Authors:
-
- Univ. of Tennessee, Knoxville, TN (United States). Dept. of Materials Science and Engineering; Oerlikon AM US, Charlotte, NC (United States)
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science and Technology Division. Manufacturing Demonstration Facility
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Materials Science and Technology Division
- Applied Optimization Inc., Dayton, OH (United States)
- Univ. of Tennessee, Knoxville, TN (United States). Dept. of Materials Science and Engineering. Dept. of Mechanical and Aerospace and Biomedical Engineering; Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Manufacturing Demonstration Facility
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States); Applied Optimization Inc., Dayton, OH (United States)
- Sponsoring Org.:
- USDOE Office of Energy Efficiency and Renewable Energy (EERE), Energy Efficiency Office. Advanced Manufacturing Office; USDOE Office of Nuclear Energy (NE), Fuel Cycle Technologies (NE-5); National Aeronautics and Space Administration (NASA)
- OSTI Identifier:
- 1468183
- Grant/Contract Number:
- AC05-00OR22725; NNX15CA24C
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science
- Additional Journal Information:
- Journal Volume: 49; Journal Issue: 11; Journal ID: ISSN 1073-5623
- Publisher:
- ASM International
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Foster, S. J., Carver, K., Dinwiddie, R. B., List, F., Unocic, K. A., Chaudhary, A., and Babu, S. S. Process-Defect-Structure-Property Correlations During Laser Powder Bed Fusion of Alloy 718: Role of In Situ and Ex Situ Characterizations. United States: N. p., 2018.
Web. doi:10.1007/s11661-018-4870-2.
Foster, S. J., Carver, K., Dinwiddie, R. B., List, F., Unocic, K. A., Chaudhary, A., & Babu, S. S. Process-Defect-Structure-Property Correlations During Laser Powder Bed Fusion of Alloy 718: Role of In Situ and Ex Situ Characterizations. United States. https://doi.org/10.1007/s11661-018-4870-2
Foster, S. J., Carver, K., Dinwiddie, R. B., List, F., Unocic, K. A., Chaudhary, A., and Babu, S. S. Tue .
"Process-Defect-Structure-Property Correlations During Laser Powder Bed Fusion of Alloy 718: Role of In Situ and Ex Situ Characterizations". United States. https://doi.org/10.1007/s11661-018-4870-2. https://www.osti.gov/servlets/purl/1468183.
@article{osti_1468183,
title = {Process-Defect-Structure-Property Correlations During Laser Powder Bed Fusion of Alloy 718: Role of In Situ and Ex Situ Characterizations},
author = {Foster, S. J. and Carver, K. and Dinwiddie, R. B. and List, F. and Unocic, K. A. and Chaudhary, A. and Babu, S. S.},
abstractNote = {Components made by laser powder bed fusion (L-PBF) additive processes require extensive trial and error optimization to minimize defects and arrive at targeted microstructure and properties. In this paper, in situ infrared thermography and ex situ surface roughness measurements were explored as methodologies to ensure Inconel® 718-part quality. For a given laser energy of 200 Watts, prismatic samples were produced with different exposure times (80 to 110 µs) and point spacings (80 to 110 µm). The infrared intensities from laser–material interaction zones were measured spatially and temporally. The conditions leading to higher IR intensity and lowest surface roughness values correlated well with less porosity and coarse solidification grain structure. The transition from highly columnar to misoriented growth is attributed to changes in thermal gradients and liquid–solid interface velocities. Hardness measurements and electron microscopy of the as-processed and post-processed heat-treated samples show complex transitions in microstructural states including the heavily dislocated FCC matrix, reduction of dislocation density, and copious precipitation, respectively. These results show that the geometry-process-structure-property correlations are dynamic, and they cascade depending on the transitions of phase states from powder to liquid to solid, as well as phase decompositions and deformations within the solid FCC phase. Finally, validity of using analytical weld process models to describe the above phenomena is also highlighted.},
doi = {10.1007/s11661-018-4870-2},
journal = {Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science},
number = 11,
volume = 49,
place = {United States},
year = {Tue Aug 14 00:00:00 EDT 2018},
month = {Tue Aug 14 00:00:00 EDT 2018}
}
Web of Science
Works referenced in this record:
Weld pool geometry during keyhole laser welding of thin steel sheets
journal, December 2004
- Krasnoperov, M. Y.; Pieters, R. R. G. M.; Richardson, I. M.
- Science and Technology of Welding and Joining, Vol. 9, Issue 6
Infrared thermography for laser-based powder bed fusion additive manufacturing processes
conference, January 2014
- Moylan, Shawn; Whitenton, Eric; Lane, Brandon
- 40TH ANNUAL REVIEW OF PROGRESS IN QUANTITATIVE NONDESTRUCTIVE EVALUATION: Incorporating the 10th International Conference on Barkhausen Noise and Micromagnetic Testing, AIP Conference Proceedings
Toward prediction of microstructural evolution during laser surface alloying
journal, April 2002
- Babu, S. S.; David, S. A.; Martukanitz, R. P.
- Metallurgical and Materials Transactions A, Vol. 33, Issue 4
Additive manufacturing: Toward holistic design
journal, July 2017
- Jared, Bradley H.; Aguilo, Miguel A.; Beghini, Lauren L.
- Scripta Materialia, Vol. 135
Kinetics of the Simultaneous Decomposition of Austenite into Several Transformation Products
journal, July 1997
- Jones, S. J.; Bhadeshia, H. K. D. H.
- Acta Materialia, Vol. 45, Issue 7
Definition of brightness temperature and restoration of true temperature in laser cladding using infrared camera
journal, April 2013
- Doubenskaia, M.; Pavlov, M.; Grigoriev, S.
- Surface and Coatings Technology, Vol. 220
Trends in Solidification Grain Size and Morphology for Additive Manufacturing of Ti-6Al-4V
journal, September 2017
- Gockel, Joy; Sheridan, Luke; Narra, Sneha P.
- JOM, Vol. 69, Issue 12
Thermographic Microstructure Monitoring in Electron Beam Additive Manufacturing
journal, March 2017
- Raplee, J.; Plotkowski, A.; Kirka, M. M.
- Scientific Reports, Vol. 7, Issue 1
Feasibility of in situ controlled heat treatment (ISHT) of Inconel 718 during electron beam melting additive manufacturing
journal, January 2017
- Sames, W. J.; Unocic, K. A.; Helmreich, G. W.
- Additive Manufacturing, Vol. 13
Deformation in the heat affected zone during spot welding of a nickel-based single crystal
journal, July 2003
- Barabash, O. M.; Babu, S. S.; David, S. A.
- Journal of Applied Physics, Vol. 94, Issue 1
Surface Morphology in Selective Laser Melting of Metal Powders
journal, January 2011
- Yadroitsev, I.; Smurov, I.
- Physics Procedia, Vol. 12
Approximation of absolute surface temperature measurements of powder bed fusion additive manufacturing technology using in situ infrared thermography
journal, January 2015
- Rodriguez, Emmanuel; Mireles, Jorge; Terrazas, Cesar A.
- Additive Manufacturing, Vol. 5
Prediction of lack-of-fusion porosity for powder bed fusion
journal, March 2017
- Tang, Ming; Pistorius, P. Chris; Beuth, Jack L.
- Additive Manufacturing, Vol. 14
Localized melt-scan strategy for site specific control of grain size and primary dendrite arm spacing in electron beam additive manufacturing
journal, November 2017
- Raghavan, Narendran; Simunovic, Srdjan; Dehoff, Ryan
- Acta Materialia, Vol. 140
Thermal effects on microstructural heterogeneity of Inconel 718 materials fabricated by electron beam melting
journal, July 2014
- Sames, William J.; Unocic, Kinga A.; Dehoff, Ryan R.
- Journal of Materials Research, Vol. 29, Issue 17
The metallurgy and processing science of metal additive manufacturing
journal, March 2016
- Sames, W. J.; List, F. A.; Pannala, S.
- International Materials Reviews, Vol. 61, Issue 5
Thermodynamic and kinetic models for describing microstructure evolution during joining of metals and alloys
journal, November 2009
- Babu, S. S.
- International Materials Reviews, Vol. 54, Issue 6
Statistical study of ductility-dip cracking induced plastic deformation in polycrystalline laser 3D printed Ni-based superalloy
journal, June 2017
- Qian, Dan; Xue, Jiawei; Zhang, Anfeng
- Scientific Reports, Vol. 7, Issue 1
Nucleation and growth of chimney pores during electron-beam additive manufacturing
journal, December 2016
- Cordero, Zachary C.; Dinwiddie, Ralph B.; Immel, David
- Journal of Materials Science, Vol. 52, Issue 6
Site specific control of crystallographic grain orientation through electron beam additive manufacturing
journal, November 2014
- Dehoff, R. R.; Kirka, M. M.; Sames, W. J.
- Materials Science and Technology, Vol. 31, Issue 8
Thermo-Calc & DICTRA, computational tools for materials science
journal, June 2002
- Andersson, J-O; Helander, Thomas; Höglund, Lars
- Calphad, Vol. 26, Issue 2
Review of in-situ process monitoring and in-situ metrology for metal additive manufacturing
journal, April 2016
- Everton, Sarah K.; Hirsch, Matthias; Stravroulakis, Petros
- Materials & Design, Vol. 95
In situ quality control of the selective laser melting process using a high-speed, real-time melt pool monitoring system
journal, August 2014
- Clijsters, S.; Craeghs, T.; Buls, S.
- The International Journal of Advanced Manufacturing Technology, Vol. 75, Issue 5-8
3D printing of high-strength aluminium alloys
journal, September 2017
- Martin, John H.; Yahata, Brennan D.; Hundley, Jacob M.
- Nature, Vol. 549, Issue 7672
Single-crystal laser deposition of superalloys: processing–microstructure maps
journal, April 2001
- Gäumann, M.; Bezençon, C.; Canalis, P.
- Acta Materialia, Vol. 49, Issue 6
High speed imaging technique Part 1 – high speed imaging of arc welding phenomena
journal, January 2011
- Ogawa, Y.
- Science and Technology of Welding and Joining, Vol. 16, Issue 1
Single track formation in selective laser melting of metal powders
journal, September 2010
- Yadroitsev, I.; Gusarov, A.; Yadroitsava, I.
- Journal of Materials Processing Technology, Vol. 210, Issue 12
High speed imaging technique Part 2 – High speed imaging of power beam welding phenomena
journal, January 2011
- Tsukamoto, S.
- Science and Technology of Welding and Joining, Vol. 16, Issue 1
Solidification Phase and Microstructure Selection Maps for Fe-Cr-Ni Alloys.
journal, January 1999
- Fukumoto, Shigeo; Kurz, Wilfried
- ISIJ International, Vol. 39, Issue 12
Model for solute redistribution during rapid solidification
journal, February 1982
- Aziz, M. J.
- Journal of Applied Physics, Vol. 53, Issue 2
Calibrating IR cameras for in-situ temperature measurement during the electron beam melt processing of Inconel 718 and Ti-Al6-V4
conference, June 2016
- Dinwiddie, R. B.; Kirka, M. M.; Lloyd, P. D.
- SPIE Commercial + Scientific Sensing and Imaging, SPIE Proceedings
Analysis of the Metal Vapour during Laser Beam Welding
journal, January 2011
- Huber, S.; Glasschroeder, J.; Zaeh, M. F.
- Physics Procedia, Vol. 12
Design of an Optical system for the In Situ Process Monitoring of Selective Laser Melting (SLM)
journal, January 2011
- Lott, Philipp; Schleifenbaum, Henrich; Meiners, Wilhelm
- Physics Procedia, Vol. 12
Progress Towards Metal Additive Manufacturing Standardization to Support Qualification and Certification
journal, February 2017
- Seifi, Mohsen; Gorelik, Michael; Waller, Jess
- JOM, Vol. 69, Issue 3
Cluster 1: commercializing additive manufacturing—hurdles in materials characterization and testing
journal, October 2017
- Roach, R. A.; Gardner, S. H.
- Translational Materials Research, Vol. 4, Issue 4
Numerical modeling of heat-transfer and the influence of process parameters on tailoring the grain morphology of IN718 in electron beam additive manufacturing
journal, June 2016
- Raghavan, Narendran; Dehoff, Ryan; Pannala, Sreekanth
- Acta Materialia, Vol. 112
Evaluation of an Al-Ce alloy for laser additive manufacturing
journal, March 2017
- Plotkowski, A.; Rios, O.; Sridharan, N.
- Acta Materialia, Vol. 126
Reactive gas shielding during laser surface alloying for production of hard coatings
journal, January 2006
- Babu, S. S.; Kelly, S. M.; Murugananth, M.
- Surface and Coatings Technology, Vol. 200, Issue 8
Additively manufactured hierarchical stainless steels with high strength and ductility
journal, October 2017
- Wang, Y. Morris; Voisin, Thomas; McKeown, Joseph T.
- Nature Materials, Vol. 17, Issue 1
In-Situ Metrology System for Laser Powder Bed Fusion Additive Process
journal, January 2015
- Land, William S.; Zhang, Bin; Ziegert, John
- Procedia Manufacturing, Vol. 1
Characterization of topology optimized Ti-6Al-4V components using electron beam powder bed fusion
journal, January 2018
- Yoder, S.; Morgan, S.; Kinzy, C.
- Additive Manufacturing, Vol. 19
Verification and validation of a rapid heat transfer calculation methodology for transient melt pool solidification conditions in powder bed metal additive manufacturing
journal, December 2017
- Plotkowski, A.; Kirka, M. M.; Babu, S. S.
- Additive Manufacturing, Vol. 18
Mechanisms of equiaxed grain formation in ferritic stainless steel gas tungsten arc welds
journal, May 1995
- Villafuerte, J. C.; Kerr, H. W.; David, S. A.
- Materials Science and Engineering: A, Vol. 194, Issue 2
Residual stress. Part 2 – Nature and origins
journal, April 2001
- Withers, P. J.; Bhadeshia, H. K. D. H.
- Materials Science and Technology, Vol. 17, Issue 4
XCT analysis of the influence of melt strategies on defect population in Ti–6Al–4V components manufactured by Selective Electron Beam Melting
journal, April 2015
- Tammas-Williams, S.; Zhao, H.; Léonard, F.
- Materials Characterization, Vol. 102
Power–Velocity Process Design Charts for Powder Bed Additive Manufacturing
journal, August 2017
- Clymer, Daniel R.; Cagan, Jonathan; Beuth, Jack
- Journal of Mechanical Design, Vol. 139, Issue 10
Plasma Bursts in Deep Penetration Laser Welding
journal, January 2014
- Mrňa, L.; Šarbort, M.
- Physics Procedia, Vol. 56
Time-resolved X-ray diffraction investigation of primary weld solidification in Fe-C-Al-Mn steel welds
journal, November 2002
- Babu, S. S.; Elmer, J. W.; Vitek, J. M.
- Acta Materialia, Vol. 50, Issue 19
Selective laser melting technology: From the single laser melted track stability to 3D parts of complex shape
journal, January 2010
- Yadroitsev, I.; Smurov, I.
- Physics Procedia, Vol. 5
Identification and qualification of temperature signal for monitoring and control in laser cladding
journal, December 2006
- Bi, Guijun; Gasser, Andres; Wissenbach, Konrad
- Optics and Lasers in Engineering, Vol. 44, Issue 12