Role of Tartaric Acid in Chemical, Mechanical and Self-Healing Behaviors of a Calcium-Aluminate Cement Blend with Fly Ash F under Steam and Alkali Carbonate Environments at 270°C
Abstract
Tartaric acid (TA) changes short-term mechanical behavior and phase composition of sodium-metasilicate activated calcium-aluminate cement blend with fly ash, type F, when used as a set control additive to allow sufficient pumping time for underground well placement. The present work focuses on TA effect on self-healing properties of the blend under steam or alkali carbonate environments at 270°C applicable to geothermal wells. Compressive strength recoveries and cracks sealing were examined to evaluate self-healing of the cement after repeated crush tests followed by two consecutive healing periods of 10 and 5 days at 270°C. Optical and scanning electron microscopes, X-ray diffraction, Fourier Transform infrared and EDX measurements along with thermal gravimetric analyses were used to identify phases participating in the healing processes. Samples with 1% mass fraction of TA by weight of blend demonstrated improved strength recoveries and crack plugging properties, especially in alkali carbonate environment. This effect was attributed to silicon-rich (C,N)-A-S-H amorphous phase predominant in TA-modified samples, high-temperature stable zeolite phases along with the formation of tobermorite-type crystals in the presence of tartaric acid.
- Authors:
-
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Publication Date:
- Research Org.:
- Brookhaven National Laboratory (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Energy Efficiency and Renewable Energy (EERE), Renewable Power Office. Geothermal Technologies Office; USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1392214
- Report Number(s):
- BNL-114134-2017-JA
Journal ID: ISSN 1996-1944; MATEG9; R&D Project: 22444
- Grant/Contract Number:
- SC0012704; AC02-98CH10886
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Materials
- Additional Journal Information:
- Journal Volume: 10; Journal Issue: 4; Journal ID: ISSN 1996-1944
- Publisher:
- MDPI
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 15 GEOTHERMAL ENERGY; 54 ENVIRONMENTAL SCIENCES; 36 MATERIALS SCIENCE; calcium aluminate cement; self-healing cement; alkali activated cement; fly ash; retardation; microstructure
Citation Formats
Pyatina, Tatiana, and Sugama, Toshifumi. Role of Tartaric Acid in Chemical, Mechanical and Self-Healing Behaviors of a Calcium-Aluminate Cement Blend with Fly Ash F under Steam and Alkali Carbonate Environments at 270°C. United States: N. p., 2017.
Web. doi:10.3390/ma10040342.
Pyatina, Tatiana, & Sugama, Toshifumi. Role of Tartaric Acid in Chemical, Mechanical and Self-Healing Behaviors of a Calcium-Aluminate Cement Blend with Fly Ash F under Steam and Alkali Carbonate Environments at 270°C. United States. https://doi.org/10.3390/ma10040342
Pyatina, Tatiana, and Sugama, Toshifumi. Sat .
"Role of Tartaric Acid in Chemical, Mechanical and Self-Healing Behaviors of a Calcium-Aluminate Cement Blend with Fly Ash F under Steam and Alkali Carbonate Environments at 270°C". United States. https://doi.org/10.3390/ma10040342. https://www.osti.gov/servlets/purl/1392214.
@article{osti_1392214,
title = {Role of Tartaric Acid in Chemical, Mechanical and Self-Healing Behaviors of a Calcium-Aluminate Cement Blend with Fly Ash F under Steam and Alkali Carbonate Environments at 270°C},
author = {Pyatina, Tatiana and Sugama, Toshifumi},
abstractNote = {Tartaric acid (TA) changes short-term mechanical behavior and phase composition of sodium-metasilicate activated calcium-aluminate cement blend with fly ash, type F, when used as a set control additive to allow sufficient pumping time for underground well placement. The present work focuses on TA effect on self-healing properties of the blend under steam or alkali carbonate environments at 270°C applicable to geothermal wells. Compressive strength recoveries and cracks sealing were examined to evaluate self-healing of the cement after repeated crush tests followed by two consecutive healing periods of 10 and 5 days at 270°C. Optical and scanning electron microscopes, X-ray diffraction, Fourier Transform infrared and EDX measurements along with thermal gravimetric analyses were used to identify phases participating in the healing processes. Samples with 1% mass fraction of TA by weight of blend demonstrated improved strength recoveries and crack plugging properties, especially in alkali carbonate environment. This effect was attributed to silicon-rich (C,N)-A-S-H amorphous phase predominant in TA-modified samples, high-temperature stable zeolite phases along with the formation of tobermorite-type crystals in the presence of tartaric acid.},
doi = {10.3390/ma10040342},
journal = {Materials},
number = 4,
volume = 10,
place = {United States},
year = {Sat Mar 25 00:00:00 EDT 2017},
month = {Sat Mar 25 00:00:00 EDT 2017}
}
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Self-healing ability of fly ash–cement systems
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Self-healing behavior of strain hardening cementitious composites incorporating local waste materials
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Self-healing of surface cracks in mortars with expansive additive and crystalline additive
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Self-healing capability of cementitious composites incorporating different supplementary cementitious materials
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Comparison of ground waste glass with other supplementary cementitious materials
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Compatibility studies between N-A-S-H and C-A-S-H gels. Study in the ternary diagram Na2O–CaO–Al2O3–SiO2–H2O
journal, September 2011
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Effect of blast furnace slag on self-healing of microcracks in cementitious materials
journal, June 2014
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Improved γ-alumina support based pseudo-boehmite shaped by micro-extrusion process for oxygen carrier support application
journal, September 2012
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Low hydrothermal temperature synthesis of porous calcium silicate hydrate with enhanced reactivity SiO2
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Assessment of phase formation in alkali activated low and high calcium fly ashes in building materials
journal, June 2010
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- Construction and Building Materials, Vol. 24, Issue 6
Durability properties of a concrete with waste glass sludge exposed to freeze-and-thaw condition and de-icing salt
journal, September 2014
- Kim, Jihwan; Moon, Jae-Heum; Shim, Jae Won
- Construction and Building Materials, Vol. 66
Influence of cracking and healing on the gas permeability of cementitious composites
journal, June 2015
- Yildirim, Gurkan; Sahmaran, Mustafa; Balcikanli, Muzeyyen
- Construction and Building Materials, Vol. 85
Glass encapsulated minerals for self-healing in cement based composites
journal, November 2015
- Kanellopoulos, A.; Qureshi, T. S.; Al-Tabbaa, A.
- Construction and Building Materials, Vol. 98
A review of intrinsic self-healing capability of engineered cementitious composites: Recovery of transport and mechanical properties
journal, December 2015
- Yıldırım, Gürkan; Keskin, Özlem Kasap; Keskin, Süleyman Bahadır
- Construction and Building Materials, Vol. 101
Tests and methods of evaluating the self-healing efficiency of concrete: A review
journal, June 2016
- Muhammad, Nasiru Zakari; Shafaghat, Arezou; Keyvanfar, Ali
- Construction and Building Materials, Vol. 112
Impact of combined use of ground glass powder and crushed glass aggregate on selected properties of Portland cement concrete
journal, August 2016
- Afshinnia, Kaveh; Rangaraju, Prasada Rao
- Construction and Building Materials, Vol. 117
Transition alumina phases induced by heat treatment of boehmite: An X-ray diffraction and infrared spectroscopy study
journal, May 2009
- Boumaza, A.; Favaro, L.; Lédion, J.
- Journal of Solid State Chemistry, Vol. 182, Issue 5
Synthesis and characterization of epoxy encapsulating silica microcapsules and amine functionalized silica nanoparticles for development of an innovative self-healing concrete
journal, September 2015
- Perez, G.; Erkizia, E.; Gaitero, J. J.
- Materials Chemistry and Physics, Vol. 165
Generalized Structural Description of Calcium–Sodium Aluminosilicate Hydrate Gels: The Cross-Linked Substituted Tobermorite Model
journal, April 2013
- Myers, Rupert J.; Bernal, Susan A.; San Nicolas, Rackel
- Langmuir, Vol. 29, Issue 17
Structural investigation of silica gel films by infrared spectroscopy
journal, October 1990
- Almeida, Rui M.; Pantano, Carlo G.
- Journal of Applied Physics, Vol. 68, Issue 8
On the use of crystalline admixtures in cement based construction materials: from porosity reducers to promoters of self healing
journal, July 2016
- Ferrara, Liberato; Krelani, Visar; Moretti, Fabio
- Smart Materials and Structures, Vol. 25, Issue 8
Self-healing of drying shrinkage cracks in cement-based materials incorporating reactive MgO
journal, July 2016
- Qureshi, T. S.; Al-Tabbaa, A.
- Smart Materials and Structures, Vol. 25, Issue 8
Sol-Gel Kinetics Followed by Cylindrical Attenuated Total Reflectance Infrared Spectroscopy
journal, October 1991
- Kline, Andrew A.; Mullins, Michael E.; Cornilsen, Bahne C.
- Journal of the American Ceramic Society, Vol. 74, Issue 10
Self-Healing Efficiency of Cementitious Materials Containing Microcapsules Filled with Healing Adhesive: Mechanical Restoration and Healing Process Monitored by Water Absorption
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Resistance of fly ash–Portland cement blends to thermal shock
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Acid resistance of calcium aluminate cement–fly ash F blends
journal, July 2016
- Pyatina, Tatiana; Sugama, Toshifumi
- Advances in Cement Research, Vol. 28, Issue 7
Self-healing ability of cementitious composites: effect of addition of pre-soaked expanded perlite
journal, April 2014
- Şahmaran, Mustafa; Yildirim, Gurkan; Ozbay, Erdogan
- Magazine of Concrete Research, Vol. 66, Issue 8
Encapsulation of expansive powder minerals within a concentric glass capsule system for self-healing concrete
journalarticle, January 2016
- Qureshi, Ts; Kanellopoulos, A.; Al-Tabbaa, A.
- Elsevier BV
Crack Self-healing Behavior of Cementitious Composites Incorporating Various Mineral Admixtures
journal, January 2010
- Ahn, Tae-Ho; Kishi, Toshiharu
- Journal of Advanced Concrete Technology, Vol. 8, Issue 2
Self-Healing in Cementitious Materials—A Review
journal, May 2013
- Van Tittelboom, Kim; De Belie, Nele
- Materials, Vol. 6, Issue 6
Preparation and Properties of Melamine Urea-Formaldehyde Microcapsules for Self-Healing of Cementitious Materials
journal, March 2016
- Li, Wenting; Zhu, Xujing; Zhao, Nan
- Materials, Vol. 9, Issue 3
Effect of Tartaric Acid on Hydration of a Sodium-Metasilicate-Activated Blend of Calcium Aluminate Cement and Fly Ash F
journal, May 2016
- Pyatina, Tatiana; Sugama, Toshifumi; Moon, Juhyuk
- Materials, Vol. 9, Issue 6