Detailed magnetic and structural analysis mapping a robust magnetic C4 dome in Sr1-xNaxFe2As2

Taddei, K. M.; Allred, J. M.; Bugaris, D. E.; Lapidus, S.; Krogstad, M. J.; Stadel, R.; Claus, H.; Chung, D. Y.; Kanatzidis, M. G.; Rosenkranz, S.; Osborn, R.; Chmaissem, O.

doi:10.1103/PhysRevB.93.134510

Title: Detailed magnetic and structural analysis mapping a robust magnetic $C_{4}$ dome in ${Sr}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$

Abstract

The recently discovered C₄ tetragonal magnetic phase in hole-doped members of the iron-based superconductors provides new insights into the origin of unconventional superconductivity. Previously observed in Ba_1-xNa_xFe₂As₂ (with A = K, Na), the C₄ magnetic phase exists within the well studied C₂ spin-density wave (SDW) dome, arising just before the complete suppression of antiferromagnetic (AFM) order but after the onset of superconductivity. Here in this paper, we present detailed x-ray and neutron diffraction studies of Sr_1-xNa_xFe₂As₂ (0.10 ≤ x ≤ 0.60) to determine their structural evolution and the extent of the C₄ phase. Spanning Δx ~ 0.14 in composition, the C₄ phase is found to extend over a larger range of compositions, and to exhibit a significantly higher transition temperature, T_r ~ 65K, than in either of the other systems in which it has been observed. The onset of this phase is seen near a composition (x~0:30) where the bonding angles of the Fe₂As₂ layers approach the perfect 109.46° tetrahedral angle. We discuss the possible role of this return to a higher symmetry environment for the magnetic iron site in triggering the magnetic reorientation and the coupled re-entrance to the tetragonal structure. Finally, we present a new phase diagram, completemore »« less

Authors:

Taddei, K. M. ^[1]; Allred, J. M. ^[2]; Bugaris, D. E. ^[3]; Lapidus, S. ^[4]; Krogstad, M. J. ^[1]; Stadel, R. ^[1]; Claus, H. ^[3]; Chung, D. Y. ^[3]; Kanatzidis, M. G. ^[5]; Rosenkranz, S. ^[3]; Osborn, R. ^[3]; Chmaissem, O. ^[1]

Northern Illinois Univ., DeKalb, IL (United States). Dept. of Physics; Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division; Univ. of Alabama, Tuscaloosa, AL (United States). Dept. of Chemistry
Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Argonne National Lab. (ANL), Argonne, IL (United States). Materials Science Division; Northwestern Univ., Evanston, IL (United States). Dept. of Chemistry

Publication Date:: Wed Apr 20 00:00:00 EDT 2016

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1352600

Alternate Identifier(s):: OSTI ID: 1248253

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 93; Journal Issue: 13; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Taddei, K. M., Allred, J. M., Bugaris, D. E., Lapidus, S., Krogstad, M. J., Stadel, R., Claus, H., Chung, D. Y., Kanatzidis, M. G., Rosenkranz, S., Osborn, R., and Chmaissem, O. Detailed magnetic and structural analysis mapping a robust magnetic C4 dome in Sr1-xNaxFe2As2.  United States: N. p., 2016. 
Web.  doi:10.1103/PhysRevB.93.134510.

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                    Taddei, K. M., Allred, J. M., Bugaris, D. E., Lapidus, S., Krogstad, M. J., Stadel, R., Claus, H., Chung, D. Y., Kanatzidis, M. G., Rosenkranz, S., Osborn, R., & Chmaissem, O. Detailed magnetic and structural analysis mapping a robust magnetic C4 dome in Sr1-xNaxFe2As2.  United States.  https://doi.org/10.1103/PhysRevB.93.134510

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                    Taddei, K. M., Allred, J. M., Bugaris, D. E., Lapidus, S., Krogstad, M. J., Stadel, R., Claus, H., Chung, D. Y., Kanatzidis, M. G., Rosenkranz, S., Osborn, R., and Chmaissem, O. Wed .  
"Detailed magnetic and structural analysis mapping a robust magnetic C4 dome in Sr1-xNaxFe2As2".  United States.  https://doi.org/10.1103/PhysRevB.93.134510.  https://www.osti.gov/servlets/purl/1352600.

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@article{osti_1352600,

  title        = {Detailed magnetic and structural analysis mapping a robust magnetic C4 dome in Sr1-xNaxFe2As2},

  author       = {Taddei, K. M. and Allred, J. M. and Bugaris, D. E. and Lapidus, S. and Krogstad, M. J. and Stadel, R. and Claus, H. and Chung, D. Y. and Kanatzidis, M. G. and Rosenkranz, S. and Osborn, R. and Chmaissem, O.},

  abstractNote = {The recently discovered C4 tetragonal magnetic phase in hole-doped members of the iron-based superconductors provides new insights into the origin of unconventional superconductivity. Previously observed in Ba1-xNaxFe2As2 (with A = K, Na), the C4 magnetic phase exists within the well studied C2 spin-density wave (SDW) dome, arising just before the complete suppression of antiferromagnetic (AFM) order but after the onset of superconductivity. Here in this paper, we present detailed x-ray and neutron diffraction studies of Sr1-xNaxFe2As2 (0.10 ≤ x ≤ 0.60) to determine their structural evolution and the extent of the C4 phase. Spanning Δx ~ 0.14 in composition, the C4 phase is found to extend over a larger range of compositions, and to exhibit a significantly higher transition temperature, Tr ~ 65K, than in either of the other systems in which it has been observed. The onset of this phase is seen near a composition (x~0:30) where the bonding angles of the Fe2As2 layers approach the perfect 109.46° tetrahedral angle. We discuss the possible role of this return to a higher symmetry environment for the magnetic iron site in triggering the magnetic reorientation and the coupled re-entrance to the tetragonal structure. Finally, we present a new phase diagram, complete with the C4 phase, and use its observation in a third hole-doped 122 system to suggest the universality of this phase.},

  doi          = {10.1103/PhysRevB.93.134510},

  journal      = {Physical Review B},

  number       = 13,

  volume       = 93,

  place        = {United States},

  year         = {Wed Apr 20 00:00:00 EDT 2016},

  month        = {Wed Apr 20 00:00:00 EDT 2016}

}

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Title: Detailed magnetic and structural analysis mapping a robust magnetic C 4 dome in Sr 1 - x Na x Fe 2 As 2

Abstract

Citation Formats

Magnetically driven suppression of nematic order in an iron-based superconductor journal, May 2014

Magnetic degeneracy and hidden metallicity of the spin-density-wave state in ferropnictides journal, January 2010

Effect of Fermi Surface Nesting on Resonant Spin Excitations in Ba 1 − x K x Fe 2 As 2 journal, October 2011

Scaling between Magnetic and Lattice Fluctuations in Iron Pnictide Superconductors journal, September 2013

Orbital ordering and unfrustrated ( π , 0 ) magnetism from degenerate double exchange in the iron pnictides journal, July 2010

Symmetry-breaking orbital anisotropy observed for detwinned Ba(Fe1-xCox)2As2 above the spin density wave transition journal, April 2011

Divergent Nematic Susceptibility in an Iron Arsenide Superconductor journal, August 2012

Magnetoelastic coupling in the phase diagram of Ba 1 − x K x Fe 2 As 2 as seen via neutron diffraction journal, May 2011

Phase diagram of Ba 1 − x K x Fe 2 As 2 journal, May 2012

Structural, magnetic, and superconducting properties of Ba 1 − x Na x Fe 2 As 2 journal, September 2013

Coincident structural and magnetic order in BaFe 2 ( As 1 − x P x ) 2 revealed by high-resolution neutron diffraction journal, September 2014

What drives nematic order in iron-based superconductors? journal, January 2014

Spin reorientation in Ba 0.65 Na 0.35 Fe 2 As 2 studied by single-crystal neutron diffraction journal, February 2015

Symmetry of reentrant tetragonal phase in Ba 1 − x Na x Fe 2 As 2 : Magnetic versus orbital ordering mechanism journal, November 2014

Double-Q spin-density wave in iron arsenide superconductors journal, January 2016

Muon spin rotation study of the magnetic structure in the tetragonal antiferromagnetic state of weakly underdoped Ba 1− x K x Fe 2 As 2 journal, September 2015

Structure, Magnetism, and Superconductivity of the Layered Iron Arsenides Sr 1- x Na x Fe 2 As 2 journal, February 2011

Synthesis, structure, and phase diagram of (Sr 1− x Na x )Fe 2 As 2 superconductors journal, April 2015

Topotactic Redox Chemistry of NaFeAs in Water and Air and Superconducting Behavior with Stoichiometry Change journal, July 2010

Tetragonal magnetic phase in Ba 1 − x K x Fe 2 As 2 from x-ray and neutron diffraction journal, September 2015

Superconductivity-induced re-entrance of the orthorhombic distortion in Ba1−xKxFe2As2 journal, July 2015

EXPGUI , a graphical user interface for GSAS journal, April 2001

Phenomenological model of anisotropic peak broadening in powder diffraction journal, April 1999

Superconductivity up to 29 K in SrFe 2 As 2 and BaFe 2 As 2 at high pressures journal, December 2008

Magnetism of Fe in SrFe2As2: Local investigation by time differential perturbed angular distribution (TDPAD) spectroscopy journal, November 2012

Cesium vacancy ordering in phase-separated C s x F e 2 − y S e 2 journal, September 2015

Structural and magnetic phase transitions in the ternary iron arsenides SrFe 2 As 2 and EuFe 2 As 2 journal, October 2008

Different resistivity response to spin-density wave and superconductivity at 20 K in Ca 1− x Na x Fe 2 As 2 journal, September 2008

Magnetic and structural transitions in layered iron arsenide systems: A Fe 2 As 2 versus R FeAsO journal, September 2008

Effect of pressure on the magnetostructural transition in SrFe 2 As 2 journal, November 2008

Structural transition and anisotropic properties of single-crystalline SrFe 2 As 2 journal, July 2008

Role of striction at magnetic and structural transitions in iron pnictides journal, April 2009

Interplay of magnetic and structural transitions in iron-based pnictide superconductors journal, July 2010

Effect of Uniaxial Strain on the Structural and Magnetic Phase Transitions in BaFe 2 As 2 journal, February 2012

Close correlation between magnetic properties and the soft phonon mode of the structural transition in BaFe 2 As 2 and SrFe 2 As 2 journal, April 2015

Competing magnetic double- Q phases and superconductivity-induced reentrance of C 2 magnetic stripe order in iron pnictides journal, October 2015

Complex phase diagram of Ba 1 − x Na x Fe 2 As 2 : A multitude of phases striving for the electronic entropy journal, January 2016

Spin and lattice structures of single-crystalline SrFe 2 As 2 journal, October 2008

Columnar magnetic structure coupled with orthorhombic distortion in the antiferromagnetic iron arsenide SrFe 2 As 2 journal, December 2008

Magnetic order in the CaFe 1 − x Co x AsF ( x = 0.00 , 0.06 , 0.12 ) superconducting compounds journal, February 2009

Interplay between tetragonal magnetic order, stripe magnetism, and superconductivity in iron-based materials journal, March 2015

Strong spin resonance mode associated with suppression of soft magnetic ordering in hole-doped Ba1-xNaxFe2As2 journal, December 2019

Single-crystal growth of the iron-based superconductor La 0.34 Na 0.66 Fe 2 As 2 journal, October 2018

Optical and photoemission investigation of structural and magnetic transitions in the iron-based superconductor Sr 0.67 Na 0.33 Fe 2 As 2 journal, December 2019

Preferred Magnetic Excitations in the Iron-Based Sr 1 − x Na x Fe 2 As 2 Superconductor journal, January 2019

Strong Spin Resonance Mode associated with suppression of soft magnetic ordering in Hole-doped Ba1-xNaxFe2As2 text, January 2019

Title: Detailed magnetic and structural analysis mapping a robust magnetic $C_{4}$ dome in ${Sr}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$

Magnetically driven suppression of nematic order in an iron-based superconductor
journal, May 2014

Magnetic degeneracy and hidden metallicity of the spin-density-wave state in ferropnictides
journal, January 2010

Effect of Fermi Surface Nesting on Resonant Spin Excitations in ${Ba}_{1 - x} K_{x} {Fe}_{2} {As}_{2}$
journal, October 2011

Scaling between Magnetic and Lattice Fluctuations in Iron Pnictide Superconductors
journal, September 2013

Orbital ordering and unfrustrated $(π, 0)$ magnetism from degenerate double exchange in the iron pnictides
journal, July 2010

Symmetry-breaking orbital anisotropy observed for detwinned Ba(Fe1-xCox)2As2 above the spin density wave transition
journal, April 2011

Divergent Nematic Susceptibility in an Iron Arsenide Superconductor
journal, August 2012

Magnetoelastic coupling in the phase diagram of Ba $_{1 - x}$ K $_{x}$ Fe $_{2}$ As $_{2}$ as seen via neutron diffraction
journal, May 2011

Phase diagram of Ba $_{1 - x}$ K $_{x}$ Fe $_{2}$ As $_{2}$
journal, May 2012

Structural, magnetic, and superconducting properties of Ba $_{1 - x}$ Na $_{x}$ Fe $_{2}$ As $_{2}$
journal, September 2013

Coincident structural and magnetic order in ${BaFe}_{2} {({As}_{1 - x} P_{x})}_{2}$ revealed by high-resolution neutron diffraction
journal, September 2014

What drives nematic order in iron-based superconductors?
journal, January 2014

Spin reorientation in ${Ba}_{0.65} {Na}_{0.35} {Fe}_{2} {As}_{2}$ studied by single-crystal neutron diffraction
journal, February 2015

Symmetry of reentrant tetragonal phase in ${Ba}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$ : Magnetic versus orbital ordering mechanism
journal, November 2014

Double-Q spin-density wave in iron arsenide superconductors
journal, January 2016

Muon spin rotation study of the magnetic structure in the tetragonal antiferromagnetic state of weakly underdoped Ba _{1− x} K _x Fe ₂ As ₂
journal, September 2015

Structure, Magnetism, and Superconductivity of the Layered Iron Arsenides Sr _{1- x} Na _x Fe ₂ As ₂
journal, February 2011

Synthesis, structure, and phase diagram of (Sr _{1− x} Na _x )Fe ₂ As ₂ superconductors
journal, April 2015

Topotactic Redox Chemistry of NaFeAs in Water and Air and Superconducting Behavior with Stoichiometry Change
journal, July 2010

Tetragonal magnetic phase in ${Ba}_{1 - x} K_{x} {Fe}_{2} {As}_{2}$ from x-ray and neutron diffraction
journal, September 2015

Superconductivity-induced re-entrance of the orthorhombic distortion in Ba1−xKxFe2As2
journal, July 2015

EXPGUI , a graphical user interface for GSAS
journal, April 2001

Phenomenological model of anisotropic peak broadening in powder diffraction
journal, April 1999

Superconductivity up to 29 K in SrFe ₂ As ₂ and BaFe ₂ As ₂ at high pressures
journal, December 2008

Magnetism of Fe in SrFe2As2: Local investigation by time differential perturbed angular distribution (TDPAD) spectroscopy
journal, November 2012

Cesium vacancy ordering in phase-separated $C s_{x} F e_{2 - y} S e_{2}$
journal, September 2015

Structural and magnetic phase transitions in the ternary iron arsenides SrFe ₂ As ₂ and EuFe ₂ As ₂
journal, October 2008

Different resistivity response to spin-density wave and superconductivity at 20 K in Ca _{1− x} Na _x Fe ₂ As ₂
journal, September 2008

Magnetic and structural transitions in layered iron arsenide systems: $A {Fe}_{2} {As}_{2}$ versus $R FeAsO$
journal, September 2008

Effect of pressure on the magnetostructural transition in ${SrFe}_{2} {As}_{2}$
journal, November 2008

Structural transition and anisotropic properties of single-crystalline ${SrFe}_{2} {As}_{2}$
journal, July 2008

Role of striction at magnetic and structural transitions in iron pnictides
journal, April 2009

Interplay of magnetic and structural transitions in iron-based pnictide superconductors
journal, July 2010

Effect of Uniaxial Strain on the Structural and Magnetic Phase Transitions in ${BaFe}_{2} {As}_{2}$
journal, February 2012

Close correlation between magnetic properties and the soft phonon mode of the structural transition in ${BaFe}_{2} {As}_{2}$ and ${SrFe}_{2} {As}_{2}$
journal, April 2015

Competing magnetic double- $Q$ phases and superconductivity-induced reentrance of $C_{2}$ magnetic stripe order in iron pnictides
journal, October 2015

Complex phase diagram of ${Ba}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$ : A multitude of phases striving for the electronic entropy
journal, January 2016

Spin and lattice structures of single-crystalline ${SrFe}_{2} {As}_{2}$
journal, October 2008

Columnar magnetic structure coupled with orthorhombic distortion in the antiferromagnetic iron arsenide ${SrFe}_{2} {As}_{2}$
journal, December 2008

Magnetic order in the ${CaFe}_{1 - x} {Co}_{x} AsF$ $(x = 0.00, 0.06, 0.12)$ superconducting compounds
journal, February 2009

Interplay between tetragonal magnetic order, stripe magnetism, and superconductivity in iron-based materials
journal, March 2015

Strong spin resonance mode associated with suppression of soft magnetic ordering in hole-doped Ba1-xNaxFe2As2
journal, December 2019

Single-crystal growth of the iron-based superconductor La _0.34 Na _0.66 Fe ₂ As ₂
journal, October 2018

Optical and photoemission investigation of structural and magnetic transitions in the iron-based superconductor ${Sr}_{0.67} {Na}_{0.33} {Fe}_{2} {As}_{2}$
journal, December 2019

Preferred Magnetic Excitations in the Iron-Based ${Sr}_{1 - x} {Na}_{x} {Fe}_{2} {As}_{2}$ Superconductor
journal, January 2019

Strong Spin Resonance Mode associated with suppression of soft magnetic ordering in Hole-doped Ba1-xNaxFe2As2
text, January 2019