Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation

Gan, Yingye; Mo, Kun; Yun, Di; Hoelzer, David T.; Miao, Yinbin; Liu, Xiang; Lan, Kuan -Che; Park, Jun -Sang; Almer, Jonathan; Chen, Tianyi; Zhao, Huijuan

doi:10.1016/j.msea.2017.03.068

Title: Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation

Abstract

Nanostructured ferritic alloys (NFAs) are promising structural materials for advanced nuclear systems due to their exceptional radiation tolerance and high-temperature mechanical properties. Their remarkable properties result from the ultrafine ultrahigh density Y-Ti-O nanoclusters dispersed within the ferritic matrix. In this work, we performed in-situ synchrotron X-ray diffraction tests to study the tensile deformation process of the three types of NFAs: 9YWTV, 14YWT-sm13, and 14YWT-sm170 at both room temperature and elevated temperatures. A technique was developed, combining Kroner's model and X-ray measurement, to determine the intrinsic monocrystal elastic-stiffness constants, and polycrystal Young's modulus and Poisson's ratio of the NFAs. Temperature dependence of elastic anisotropy was observed in the NFAs. Lastly, an analysis of intergranular strain and strengthening factors determined that 14YWT-sm13 had a higher resistance to temperature softening compared to 9YWTV, attributed to the more effective nanoparticle strengthening during high-temperature mechanical loading.

Authors:

Gan, Yingye ^[1]; Mo, Kun ^[2]; Yun, Di ^[3]; Hoelzer, David T. ^[4]; Miao, Yinbin ^[2]; Liu, Xiang ^[5]; Lan, Kuan -Che ^[5]; Park, Jun -Sang ^[2]; Almer, Jonathan ^[2]; Chen, Tianyi ^[2]; Zhao, Huijuan ^[1]

Clemson Univ., Clemson, SC (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)
Xi'an Jiaotong Univ., Xi'an (China)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Univ. of Illinois at Urbana-Champaign, Urbana, IL (United States)

Publication Date:: Sun Mar 19 00:00:00 EDT 2017

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: Work for Others (WFO); USDOE

OSTI Identifier:: 1351786

Alternate Identifier(s):: OSTI ID: 1397427

Grant/Contract Number:: AC05-00OR22725; 13-5408; AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing

Additional Journal Information:: Journal Volume: 692; Journal Issue: C; Journal ID: ISSN 0921-5093

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; oxide dispersion strengthened (ODS) alloy; nanostructure; deformation; in-situ tensile test; high-energy X-ray diffraction

Citation Formats


                    Gan, Yingye, Mo, Kun, Yun, Di, Hoelzer, David T., Miao, Yinbin, Liu, Xiang, Lan, Kuan -Che, Park, Jun -Sang, Almer, Jonathan, Chen, Tianyi, and Zhao, Huijuan. Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation.  United States: N. p., 2017. 
Web.  doi:10.1016/j.msea.2017.03.068.

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                    Gan, Yingye, Mo, Kun, Yun, Di, Hoelzer, David T., Miao, Yinbin, Liu, Xiang, Lan, Kuan -Che, Park, Jun -Sang, Almer, Jonathan, Chen, Tianyi, & Zhao, Huijuan. Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation.  United States.  https://doi.org/10.1016/j.msea.2017.03.068

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                    Gan, Yingye, Mo, Kun, Yun, Di, Hoelzer, David T., Miao, Yinbin, Liu, Xiang, Lan, Kuan -Che, Park, Jun -Sang, Almer, Jonathan, Chen, Tianyi, and Zhao, Huijuan. Sun .  
"Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation".  United States.  https://doi.org/10.1016/j.msea.2017.03.068.  https://www.osti.gov/servlets/purl/1351786.

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@article{osti_1351786,

  title        = {Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation},

  author       = {Gan, Yingye and Mo, Kun and Yun, Di and Hoelzer, David T. and Miao, Yinbin and Liu, Xiang and Lan, Kuan -Che and Park, Jun -Sang and Almer, Jonathan and Chen, Tianyi and Zhao, Huijuan},

  abstractNote = {Nanostructured ferritic alloys (NFAs) are promising structural materials for advanced nuclear systems due to their exceptional radiation tolerance and high-temperature mechanical properties. Their remarkable properties result from the ultrafine ultrahigh density Y-Ti-O nanoclusters dispersed within the ferritic matrix. In this work, we performed in-situ synchrotron X-ray diffraction tests to study the tensile deformation process of the three types of NFAs: 9YWTV, 14YWT-sm13, and 14YWT-sm170 at both room temperature and elevated temperatures. A technique was developed, combining Kroner's model and X-ray measurement, to determine the intrinsic monocrystal elastic-stiffness constants, and polycrystal Young's modulus and Poisson's ratio of the NFAs. Temperature dependence of elastic anisotropy was observed in the NFAs. Lastly, an analysis of intergranular strain and strengthening factors determined that 14YWT-sm13 had a higher resistance to temperature softening compared to 9YWTV, attributed to the more effective nanoparticle strengthening during high-temperature mechanical loading.},

  doi          = {10.1016/j.msea.2017.03.068},

  journal      = {Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing},

  number       = C,

  volume       = 692,

  place        = {United States},

  year         = {Sun Mar 19 00:00:00 EDT 2017},

  month        = {Sun Mar 19 00:00:00 EDT 2017}

}

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https://doi.org/10.1016/j.msea.2017.03.068

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Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography
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Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography
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Zhang, Lei; Wang, Shaogang
Materials, Vol. 11, Issue 10
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Title: Temperature effect of elastic anisotropy and internal strain development in advanced nanostructured alloys: An in-situ synchrotron X-ray investigation

Abstract

Citation Formats

Recent results of the reduced activation ferritic/martensitic steel development journal, August 2004

A review of refractory metal alloys and mechanically alloyed-oxide dispersion strengthened steels for space nuclear power systems journal, April 2005

Tensile and creep properties of an oxide dispersion-strengthened ferritic steel journal, December 2002

Creep response and deformation processes in nanocluster-strengthened ferritic steels journal, April 2008

Defect and void evolution in oxide dispersion strengthened ferritic steels under 3.2 MeV Fe+ ion irradiation with simultaneous helium injection journal, August 2000

Helium bubble distributions in a nanostructured ferritic alloy journal, March 2013

Investigation of High-Energy Ion-Irradiated MA957 Using Synchrotron Radiation under In-Situ Tension journal, January 2016

Recent Developments in Irradiation-Resistant Steels journal, August 2008

Stability of ferritic MA/ODS alloys at high temperatures journal, March 2005

TEM Characterization of Tensile-Tested 14YWT Nanostructured Ferritic Alloys journal, August 2008

Mechanical properties of neutron irradiated nanostructured ferritic alloy 14YWT journal, April 2009

Atom probe tomography of nanoscale particles in ODS ferritic alloys journal, July 2003

Present development status of EUROFER and ODS-EUROFER for application in blanket concepts journal, November 2005

Nanoscale characterisation of ODS–Eurofer 97 steel: An atom-probe tomography study journal, May 2010

Effect of strain on the stabilization of oxygen-enriched nanoclusters in Fe-based alloys journal, October 2011

Vacancy Mechanism of High Oxygen Solubility and Nucleation of Stable Oxygen-Enriched Clusters in Fe journal, November 2007

Formation mechanism and the role of nanoparticles in Fe-Cr ODS steels developed for radiation tolerance journal, November 2010

Vacancies as a constitutive element for the design of nanocluster-strengthened ferritic steels journal, November 2008

Characterization of precipitates in MA/ODS ferritic alloys journal, June 2006

Role of alloying elements in nanostructured ferritic steels journal, April 2011

Three-dimensional atom probe observation of nanoscale titanium-oxygen clustering in an oxide-dispersion-strengthened Fe-12Cr-3W-0.4Ti + Y2O3 ferritic alloy journal, February 2001

Stability of nanometer-sized oxide clusters in mechanically-alloyed steel under ion-induced displacement cascade damage conditions journal, February 2007

Stability of nanoclusters in 14YWT oxide dispersion strengthened steel under heavy ion-irradiation by atom probe tomography journal, December 2014

Temperature dependence of strengthening mechanisms in the nanostructured ferritic alloy 14YWT: Part I—Mechanical and microstructural observations journal, January 2013

Size-dependent characteristics of ultra-fine oxygen-enriched nanoparticles in austenitic steels journal, November 2016

The comparison of microstructures and mechanical properties between 14Cr-Al and 14Cr-Ti ferritic ODS alloys journal, May 2016

The microstructure and mechanical properties of Al-containing 9Cr ODS ferritic alloy journal, November 2015

In situ synchrotron tensile investigations on 14YWT, MA957, and 9-Cr ODS alloys journal, April 2016

Load partitioning between ferrite/martensite and dispersed nanoparticles of a 9Cr ferritic/martensitic (F/M) ODS steel at high temperatures journal, June 2015

Fracture behavior of 9Cr nanostructured ferritic alloy with improved fracture toughness journal, June 2014

Process development for 9Cr nanostructured ferritic alloy (NFA) with high fracture toughness journal, June 2014

Influence of processing on the microstructure and mechanical properties of 14YWT journal, April 2016

EFTEM and Spectrum Imaging of Mechanically Alloyed Oxide-Dispersion-Strengthened 12YWT and 14YWT Ferritic Steels journal, August 2004

Structural origins for the high plasticity of a Zr–Cu–Ni–Al bulk metallic glass journal, January 2013

Synchrotron study on load partitioning between ferrite/martensite and nanoparticles of a 9Cr ODS steel journal, December 2014

The interfacial orientation relationship of oxide nanoparticles in a hafnium-containing oxide dispersion-strengthened austenitic stainless steel journal, March 2015

Temperature and particle size effects on flow localization of 9–12%Cr ferritic/martensitic steel by in situ X-ray diffraction and small angle scattering journal, March 2010

Lattice strain and damage evolution of 9–12%Cr ferritic/martensitic steel during in situ tensile test by X-ray diffraction and small angle scattering journal, December 2010

Introduction to two-dimensional X-ray diffraction journal, June 2003

Load partitioning between ferrite and cementite during elasto-plastic deformation of an ultrahigh-carbon steel journal, April 2007

Load Partitioning and Strain-Induced Martensite Formation during Tensile Loading of a Metastable Austenitic Stainless Steel journal, March 2009

An assessment of the contributing factors to the superior properties of a nanostructured steel using in situ high-energy X-ray diffraction journal, April 2010

The determination of the elastic field of an ellipsoidal inclusion, and related problems journal, August 1957

Temperature-dependent elastic anisotropy and mesoscale deformation in a nanostructured ferritic alloy journal, October 2014

In situ generation of intergranular strains in an Al7050 alloy journal, March 1998

Intergranular stresses in ZIRCALOY-2 journal, March 2002

Measured and predicted intergranular strains in textured austenitic steel journal, January 2000

The evolution of internal stress and dislocation during tensile deformation in a 9Cr ferritic/martensitic (F/M) ODS steel investigated by high-energy X-rays journal, December 2015

The determination of a continuum mechanics equivalent elastic strain from the analysis of multiple diffraction peaks journal, October 2004

Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography journal, September 2018

Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography journal, September 2018

Recent results of the reduced activation ferritic/martensitic steel development
journal, August 2004

A review of refractory metal alloys and mechanically alloyed-oxide dispersion strengthened steels for space nuclear power systems
journal, April 2005

Tensile and creep properties of an oxide dispersion-strengthened ferritic steel
journal, December 2002

Creep response and deformation processes in nanocluster-strengthened ferritic steels
journal, April 2008

Defect and void evolution in oxide dispersion strengthened ferritic steels under 3.2 MeV Fe+ ion irradiation with simultaneous helium injection
journal, August 2000

Helium bubble distributions in a nanostructured ferritic alloy
journal, March 2013

Investigation of High-Energy Ion-Irradiated MA957 Using Synchrotron Radiation under In-Situ Tension
journal, January 2016

Recent Developments in Irradiation-Resistant Steels
journal, August 2008

Stability of ferritic MA/ODS alloys at high temperatures
journal, March 2005

TEM Characterization of Tensile-Tested 14YWT Nanostructured Ferritic Alloys
journal, August 2008

Mechanical properties of neutron irradiated nanostructured ferritic alloy 14YWT
journal, April 2009

Atom probe tomography of nanoscale particles in ODS ferritic alloys
journal, July 2003

Present development status of EUROFER and ODS-EUROFER for application in blanket concepts
journal, November 2005

Nanoscale characterisation of ODS–Eurofer 97 steel: An atom-probe tomography study
journal, May 2010

Effect of strain on the stabilization of oxygen-enriched nanoclusters in Fe-based alloys
journal, October 2011

Vacancy Mechanism of High Oxygen Solubility and Nucleation of Stable Oxygen-Enriched Clusters in Fe
journal, November 2007

Formation mechanism and the role of nanoparticles in Fe-Cr ODS steels developed for radiation tolerance
journal, November 2010

Vacancies as a constitutive element for the design of nanocluster-strengthened ferritic steels
journal, November 2008

Characterization of precipitates in MA/ODS ferritic alloys
journal, June 2006

Role of alloying elements in nanostructured ferritic steels
journal, April 2011

Three-dimensional atom probe observation of nanoscale titanium-oxygen clustering in an oxide-dispersion-strengthened Fe-12Cr-3W-0.4Ti + Y2O3 ferritic alloy
journal, February 2001

Stability of nanometer-sized oxide clusters in mechanically-alloyed steel under ion-induced displacement cascade damage conditions
journal, February 2007

Stability of nanoclusters in 14YWT oxide dispersion strengthened steel under heavy ion-irradiation by atom probe tomography
journal, December 2014

Temperature dependence of strengthening mechanisms in the nanostructured ferritic alloy 14YWT: Part I—Mechanical and microstructural observations
journal, January 2013

Size-dependent characteristics of ultra-fine oxygen-enriched nanoparticles in austenitic steels
journal, November 2016

The comparison of microstructures and mechanical properties between 14Cr-Al and 14Cr-Ti ferritic ODS alloys
journal, May 2016

The microstructure and mechanical properties of Al-containing 9Cr ODS ferritic alloy
journal, November 2015

In situ synchrotron tensile investigations on 14YWT, MA957, and 9-Cr ODS alloys
journal, April 2016

Load partitioning between ferrite/martensite and dispersed nanoparticles of a 9Cr ferritic/martensitic (F/M) ODS steel at high temperatures
journal, June 2015

Fracture behavior of 9Cr nanostructured ferritic alloy with improved fracture toughness
journal, June 2014

Process development for 9Cr nanostructured ferritic alloy (NFA) with high fracture toughness
journal, June 2014

Influence of processing on the microstructure and mechanical properties of 14YWT
journal, April 2016

EFTEM and Spectrum Imaging of Mechanically Alloyed Oxide-Dispersion-Strengthened 12YWT and 14YWT Ferritic Steels
journal, August 2004

Structural origins for the high plasticity of a Zr–Cu–Ni–Al bulk metallic glass
journal, January 2013

Synchrotron study on load partitioning between ferrite/martensite and nanoparticles of a 9Cr ODS steel
journal, December 2014

The interfacial orientation relationship of oxide nanoparticles in a hafnium-containing oxide dispersion-strengthened austenitic stainless steel
journal, March 2015

Temperature and particle size effects on flow localization of 9–12%Cr ferritic/martensitic steel by in situ X-ray diffraction and small angle scattering
journal, March 2010

Lattice strain and damage evolution of 9–12%Cr ferritic/martensitic steel during in situ tensile test by X-ray diffraction and small angle scattering
journal, December 2010

Introduction to two-dimensional X-ray diffraction
journal, June 2003

Load partitioning between ferrite and cementite during elasto-plastic deformation of an ultrahigh-carbon steel
journal, April 2007

Load Partitioning and Strain-Induced Martensite Formation during Tensile Loading of a Metastable Austenitic Stainless Steel
journal, March 2009

An assessment of the contributing factors to the superior properties of a nanostructured steel using in situ high-energy X-ray diffraction
journal, April 2010

The determination of the elastic field of an ellipsoidal inclusion, and related problems
journal, August 1957

Temperature-dependent elastic anisotropy and mesoscale deformation in a nanostructured ferritic alloy
journal, October 2014

In situ generation of intergranular strains in an Al7050 alloy
journal, March 1998

Intergranular stresses in ZIRCALOY-2
journal, March 2002

Measured and predicted intergranular strains in textured austenitic steel
journal, January 2000

The evolution of internal stress and dislocation during tensile deformation in a 9Cr ferritic/martensitic (F/M) ODS steel investigated by high-energy X-rays
journal, December 2015

The determination of a continuum mechanics equivalent elastic strain from the analysis of multiple diffraction peaks
journal, October 2004

Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography
journal, September 2018

Correlation of Materials Property and Performance with Internal Structures Evolvement Revealed by Laboratory X-ray Tomography
journal, September 2018