Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO2

Xu, Jing; Lin, Feng; Nordlund, Dennis; Crumlin, Ethan J.; Wang, Feng; Bai, Jianming; Doeff, Marca M.; Tong, Wei

doi:10.1039/c5cc09434h

Title: Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO₂

Abstract

Phase pure LiNiO 2 was prepared using a solid-state method and the optimal synthesis conditions led to a remarkably high capacity of 200 mA h g -1 with excellent retention. The combination of bulk and surface characterization elucidated an essential role of the excess Li in phase formation during synthesis and the subsequent electrochemical performance.

Authors:

Xu, Jing ^[1]; Lin, Feng ^[1]; Nordlund, Dennis ^[2]; Crumlin, Ethan J. ^[3]; Wang, Feng ^[4]; Bai, Jianming ^[5]; Doeff, Marca M. ^[1]; Tong, Wei ^[1]

Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
SLAC National Accelerator Lab., Menlo Park, CA (United States). Stanford Synchrotron Radiation Lightsource (SSRL)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). Advanced Light Source (ALS)
Brookhaven National Lab. (BNL), Upton, NY (United States). Dept. of Sustainable Energy Technologies
Brookhaven National Lab. (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)

Publication Date:: Thu Feb 25 00:00:00 EST 2016

Research Org.:: Brookhaven National Laboratory (BNL), Upton, NY (United States); Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)

Sponsoring Org.:: USDOE Office of Energy Efficiency and Renewable Energy (EERE), Vehicle Technologies Office (EE-3V); USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE Office of Energy Efficiency and Renewable Energy (EERE)

OSTI Identifier:: 1342627

Alternate Identifier(s):: OSTI ID: 1378755

Report Number(s):: BNL-112702-2016-JA
Journal ID: ISSN 1359-7345; CHCOFS

Grant/Contract Number:: SC0012704; AC02-05CH11231; AC02-76SF00515

Resource Type:: Accepted Manuscript

Journal Name:: ChemComm

Additional Journal Information:: Journal Volume: 52; Journal Issue: 22; Journal ID: ISSN 1359-7345

Publisher:: Royal Society of Chemistry

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 25 ENERGY STORAGE

Citation Formats


                    Xu, Jing, Lin, Feng, Nordlund, Dennis, Crumlin, Ethan J., Wang, Feng, Bai, Jianming, Doeff, Marca M., and Tong, Wei. Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO2.  United States: N. p., 2016. 
Web.  doi:10.1039/c5cc09434h.

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                    Xu, Jing, Lin, Feng, Nordlund, Dennis, Crumlin, Ethan J., Wang, Feng, Bai, Jianming, Doeff, Marca M., & Tong, Wei. Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO2.  United States.  https://doi.org/10.1039/c5cc09434h

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                    Xu, Jing, Lin, Feng, Nordlund, Dennis, Crumlin, Ethan J., Wang, Feng, Bai, Jianming, Doeff, Marca M., and Tong, Wei. Thu .  
"Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO2".  United States.  https://doi.org/10.1039/c5cc09434h.  https://www.osti.gov/servlets/purl/1342627.

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@article{osti_1342627,

  title        = {Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO2},

  author       = {Xu, Jing and Lin, Feng and Nordlund, Dennis and Crumlin, Ethan J. and Wang, Feng and Bai, Jianming and Doeff, Marca M. and Tong, Wei},

  abstractNote = {Phase pure LiNiO 2 was prepared using a solid-state method and the optimal synthesis conditions led to a remarkably high capacity of 200 mA h g -1 with excellent retention. The combination of bulk and surface characterization elucidated an essential role of the excess Li in phase formation during synthesis and the subsequent electrochemical performance.},

  doi          = {10.1039/c5cc09434h},

  journal      = {ChemComm},

  number       = 22,

  volume       = 52,

  place        = {United States},

  year         = {Thu Feb 25 00:00:00 EST 2016},

  month        = {Thu Feb 25 00:00:00 EST 2016}

}

Copy to clipboard

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Mei, Jun; Liao, Ting; Kou, Liangzhi
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Title: Elucidation of the surface characteristics and electrochemistry of high-performance LiNiO2

Abstract

Citation Formats

Soft Chemistry Synthesis and Characterization of Layered Li1-xNi1-yCoyO2-δ (0 ≤ x ≤ 1 and 0 ≤ y ≤ 1) journal, September 2001

Atomic-Resolution Visualization of Distinctive Chemical Mixing Behavior of Ni, Co, and Mn with Li in Layered Lithium Transition-Metal Oxide Cathode Materials journal, July 2015

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Atomic subshell photoionization cross sections and asymmetry parameters: 1 ⩽ Z ⩽ 103 journal, January 1985

Influence of synthesis conditions on the surface passivation and electrochemical behavior of layered cathode materials journal, January 2014

Electrochemistry and Structural Chemistry of LiNiO[sub 2] (R3m) for 4 Volt Secondary Lithium Cells journal, January 1993

Optimization of the Composition of the Li[sub 1−z]Ni[sub 1+z]O[sub 2] Electrode Materials: Structural, Magnetic, and Electrochemical Studies journal, January 1996

Reaction mechanism and kinetics analysis of lithium nickel oxide during solid-state reaction journal, January 2000

Surface Characterization of Electrodes from High Power Lithium-Ion Batteries journal, January 2002

Effect of oxygen flow rate on the structural and electrochemical properties of lithium nickel oxides synthesized by the sol–gel method journal, November 2002

Role of Mn Content on the Electrochemical Properties of Nickel-Rich Layered LiNi 0.8– x Co 0.1 Mn 0.1+ x O 2 (0.0 ≤ x ≤ 0.08) Cathodes for Lithium-Ion Batteries journal, March 2015

Profiling the nanoscale gradient in stoichiometric layered cathode particles for lithium-ion batteries journal, January 2014

Characterization and cathode performance of Li1 − xNi1 + xO2 prepared with the excess lithium method journal, September 1995

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Comparison of the structural and electrochemical properties of layered Li[NixCoyMnz]O2 (x = 1/3, 0.5, 0.6, 0.7, 0.8 and 0.85) cathode material for lithium-ion batteries journal, July 2013

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Atomic-Resolution Visualization of Distinctive Chemical Mixing Behavior of Ni, Co, and Mn with Li in Layered Lithium Transition-Metal Oxide Cathode Materials
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