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Title: Spherical quartz crystals investigated with synchrotron radiation

Abstract

The quality of x-ray spectra and images obtained from plasmas with spherically bent crystals depends in part on the crystal's x-ray diffraction across the entire crystal surface. We employ the energy selectivity and high intensity of synchrotron radiation to examine typical spherical crystals from alpha-quartz for their diffraction quality, in a perpendicular geometry that is particularly convenient to examine sagittal focusing. The crystal's local diffraction is not ideal: the most noticeable problems come from isolated regions that so far have failed to correlate with visible imperfections. In conclusion, excluding diffraction from such problem spots has little effect on the focus beyond a decrease in background.

Authors:
ORCiD logo [1];  [2];  [3];  [4];  [5];  [5]
  1. Ecopulse, Inc., Springfield, VA (United States)
  2. Argonne National Lab. (ANL), Argonne, IL (United States)
  3. Princeton Plasma Physics Lab. (PPPL), Princeton, NJ (United States)
  4. Kurchatov Institute, Moscow (Russia)
  5. The Ohio State Univ., Columbus, OH (United States)
Publication Date:
Research Org.:
Princeton Plasma Physics Lab. (PPPL), Princeton, NJ (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1259462
Grant/Contract Number:  
AC02-09CH11466
Resource Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 86; Journal Issue: 10; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; instruments; instrumentation; X-ray diffraction; quartz; X-ray reflectometry; X-ray spectra; reflectivity

Citation Formats

Pereira, N. R., Macrander, A. T., Hill, K. W., Baronova, E. O., George, K. M., and Kotick, J. Spherical quartz crystals investigated with synchrotron radiation. United States: N. p., 2015. Web. doi:10.1063/1.4934197.
Pereira, N. R., Macrander, A. T., Hill, K. W., Baronova, E. O., George, K. M., & Kotick, J. Spherical quartz crystals investigated with synchrotron radiation. United States. https://doi.org/10.1063/1.4934197
Pereira, N. R., Macrander, A. T., Hill, K. W., Baronova, E. O., George, K. M., and Kotick, J. Tue . "Spherical quartz crystals investigated with synchrotron radiation". United States. https://doi.org/10.1063/1.4934197. https://www.osti.gov/servlets/purl/1259462.
@article{osti_1259462,
title = {Spherical quartz crystals investigated with synchrotron radiation},
author = {Pereira, N. R. and Macrander, A. T. and Hill, K. W. and Baronova, E. O. and George, K. M. and Kotick, J.},
abstractNote = {The quality of x-ray spectra and images obtained from plasmas with spherically bent crystals depends in part on the crystal's x-ray diffraction across the entire crystal surface. We employ the energy selectivity and high intensity of synchrotron radiation to examine typical spherical crystals from alpha-quartz for their diffraction quality, in a perpendicular geometry that is particularly convenient to examine sagittal focusing. The crystal's local diffraction is not ideal: the most noticeable problems come from isolated regions that so far have failed to correlate with visible imperfections. In conclusion, excluding diffraction from such problem spots has little effect on the focus beyond a decrease in background.},
doi = {10.1063/1.4934197},
journal = {Review of Scientific Instruments},
number = 10,
volume = 86,
place = {United States},
year = {Tue Oct 27 00:00:00 EDT 2015},
month = {Tue Oct 27 00:00:00 EDT 2015}
}

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Cited by: 16 works
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Works referenced in this record:

Experimental characterization of bent focusing crystals
journal, May 2001

  • Lider, V. V.; Baronova, E. O.; Stepanenko, M. M.
  • Crystallography Reports, Vol. 46, Issue 3
  • DOI: 10.1134/1.1376456

Imaging x-ray crystal spectrometers for the National Spherical Torus Experiment
journal, January 1999

  • Bitter, M.; Hill, K. W.; Roquemore, A. L.
  • Review of Scientific Instruments, Vol. 70, Issue 1
  • DOI: 10.1063/1.1149344

Spatially resolved spectra from a new x-ray imaging crystal spectrometer for measurements of ion and electron temperature profiles (invited)
journal, October 2004

  • Bitter, M.; Hill, K. W.; Stratton, B.
  • Review of Scientific Instruments, Vol. 75, Issue 10
  • DOI: 10.1063/1.1791747

Spatially resolved high resolution x-ray spectroscopy for magnetically confined fusion plasmas (invited)
journal, October 2008

  • Ince-Cushman, A.; Rice, J. E.; Bitter, M.
  • Review of Scientific Instruments, Vol. 79, Issue 10, Article No. 10E302
  • DOI: 10.1063/1.2968707

4.5- and 8-keV emission and absorption x-ray imaging using spherically bent quartz 203 and 211 crystals (invited)
journal, March 2003

  • Koch, J. A.; Aglitskiy, Y.; Brown, C.
  • Review of Scientific Instruments, Vol. 74, Issue 3, p. 2130-2135
  • DOI: 10.1063/1.1537448

Invited Review Article: Development of crystal lenses for energetic photons
journal, August 2014

  • Smither, Robert K.
  • Review of Scientific Instruments, Vol. 85, Issue 8
  • DOI: 10.1063/1.4893585

Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments
journal, November 2014

  • Hill, K. W.; Bitter, M.; Delgado-Aparacio, L.
  • Review of Scientific Instruments, Vol. 85, Issue 11
  • DOI: 10.1063/1.4890260

Relative x-ray collection efficiency, spatial resolution, and spectral resolution of spherically-bent quartz, mica, germanium, and pyrolytic graphite crystals
journal, September 2014

  • Ao, T.; Harding, E. C.; Bailey, J. E.
  • Journal of Quantitative Spectroscopy and Radiative Transfer, Vol. 144
  • DOI: 10.1016/j.jqsrt.2014.03.023

X-ray Reflectivity of Curved Alpha-Quartz Crystals
journal, January 2004


Analysis and implementation of a space resolving spherical crystal spectrometer for x-ray Thomson scattering experiments
journal, April 2015

  • Harding, E. C.; Ao, T.; Bailey, J. E.
  • Review of Scientific Instruments, Vol. 86, Issue 4
  • DOI: 10.1063/1.4918619

High-performance x-ray spectroscopic devices for plasma microsources investigations
journal, October 1994


Pulsed-power-driven high energy density physics and inertial confinement fusion research
journal, May 2005

  • Matzen, M. Keith; Sweeney, M. A.; Adams, R. G.
  • Physics of Plasmas, Vol. 12, Issue 5
  • DOI: 10.1063/1.1891746

Development of a spatially resolving x-ray crystal spectrometer for measurement of ion-temperature (Ti) and rotation-velocity (v) profiles in ITER
journal, October 2010

  • Hill, K. W.; Bitter, M.; Delgado-Aparicio, L.
  • Review of Scientific Instruments, Vol. 81, Issue 10
  • DOI: 10.1063/1.3492414

Measurement of reflectivity of spherically bent crystals using K α signal from hot electrons produced by laser-matter interaction
journal, July 2015

  • Antonelli, L.; Forestier-Colleoni, P.; Folpini, G.
  • Review of Scientific Instruments, Vol. 86, Issue 7
  • DOI: 10.1063/1.4926740

X-ray polarization spectroscopy for measurement of anisotropy of hot electrons generated with ultraintense laser pulse
journal, October 2004

  • Inubushi, Yuichi; Nishimura, Hiroaki; Ochiai, Masayuki
  • Review of Scientific Instruments, Vol. 75, Issue 10
  • DOI: 10.1063/1.1789602

Works referencing / citing this record:

High resolution, high signal-to-noise crystal spectrometer for measurements of line shifts in high-density plasmas
journal, October 2018

  • Beiersdorfer, P.; Magee, E. W.; Brown, G. V.
  • Review of Scientific Instruments, Vol. 89, Issue 10
  • DOI: 10.1063/1.5035303

On evaluating x-ray imaging crystals with synchrotron radiation
journal, October 2018

  • Pereira, N. R.; Macrander, A. T.; Stoeckl, C.
  • Review of Scientific Instruments, Vol. 89, Issue 10
  • DOI: 10.1063/1.5045569

A streaked parabolic crystal imaging diagnostic at the Orion laser
journal, March 2019

  • James, Steven F.; Allan, Peter; Brown, Colin R. D.
  • Review of Scientific Instruments, Vol. 90, Issue 3
  • DOI: 10.1063/1.5049129