In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys]

Chang, L. L.; Wang, Y. D.; Ren, Y.

doi:10.1016/j.msea.2015.11.005

Title: In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys]

Abstract

Microstructure evolution, mechanical behaviors of cold rolled Ti-Nb alloys with different Nb contents subjected to different heat treatments were investigated. Here, optical microstructure and phase compositions of Ti-Nb alloys were characterized using optical microscopy and X-ray diffractometre, while mechanical behaviors of Ti-Nb alloys were examined by using tension tests. Stress-induced martensitic transformation in a Ti-30. at%Nb binary alloy was in-situ explored by synchrotron-based high-energy X-ray diffraction (HE-XRD). The results obtained suggested that mechanical behavior of Ti-Nb alloys, especially Young's modulus was directly dependent on chemical compositions and heat treatment process. According to the results of HE-XRD, α"-V1 martensite generated prior to the formation of α"-V2 during loading and a partial reversible transformation from α"-V1 to β phase was detected while α"-V2 tranformed to β completely during unloading.

Authors:

Chang, L. L. ^[1]; Wang, Y. D. ^[2]; Ren, Y. ^[3]

Shandong Univ., Jinan (China)
Univ. of Science and Technology Beijing, Beijing (China)
Argonne National Lab. (ANL), Argonne, IL (United States)

Publication Date:: Wed Nov 04 00:00:00 EST 2015

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1256711

Alternate Identifier(s):: OSTI ID: 1397994

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing

Additional Journal Information:: Journal Volume: 651; Journal Issue: C; Journal ID: ISSN 0921-5093

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Ti-Nb alloys; martensite transformation; mechanical properties; microstructure

Citation Formats


                    Chang, L. L., Wang, Y. D., and Ren, Y. In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys].  United States: N. p., 2015. 
Web.  doi:10.1016/j.msea.2015.11.005.

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                    Chang, L. L., Wang, Y. D., & Ren, Y. In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys].  United States.  https://doi.org/10.1016/j.msea.2015.11.005

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                    Chang, L. L., Wang, Y. D., and Ren, Y. Wed .  
"In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys]".  United States.  https://doi.org/10.1016/j.msea.2015.11.005.  https://www.osti.gov/servlets/purl/1256711.

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@article{osti_1256711,

  title        = {In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys]},

  author       = {Chang, L. L. and Wang, Y. D. and Ren, Y.},

  abstractNote = {Microstructure evolution, mechanical behaviors of cold rolled Ti-Nb alloys with different Nb contents subjected to different heat treatments were investigated. Here, optical microstructure and phase compositions of Ti-Nb alloys were characterized using optical microscopy and X-ray diffractometre, while mechanical behaviors of Ti-Nb alloys were examined by using tension tests. Stress-induced martensitic transformation in a Ti-30. at%Nb binary alloy was in-situ explored by synchrotron-based high-energy X-ray diffraction (HE-XRD). The results obtained suggested that mechanical behavior of Ti-Nb alloys, especially Young's modulus was directly dependent on chemical compositions and heat treatment process. According to the results of HE-XRD, α"-V1 martensite generated prior to the formation of α"-V2 during loading and a partial reversible transformation from α"-V1 to β phase was detected while α"-V2 tranformed to β completely during unloading.},

  doi          = {10.1016/j.msea.2015.11.005},

  journal      = {Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing},

  number       = C,

  volume       = 651,

  place        = {United States},

  year         = {Wed Nov 04 00:00:00 EST 2015},

  month        = {Wed Nov 04 00:00:00 EST 2015}

}

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Microstructural and Mechanical Properties of β-Type Ti–Nb–Sn Biomedical Alloys with Low Elastic Modulus
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Li, Peiyou; Ma, Xindi; Wang, Duo
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Title: In-situ investigation of stress-induced martensitic transformation in Ti–Nb binary alloys with low Young's modulus [In-situ high-energy X-ray diffraction investigation on stress-induced martensitic transformation in Ti-Nb binary alloys]

Abstract

Citation Formats

Mechanical behavior and tensile/compressive strength asymmetry of ultrafine structured Ti–Nb–Ni–Co–Al alloys with bi-modal grain size distribution journal, October 2014

Fabrication of Ti–Nb–Ag alloy via powder metallurgy for biomedical applications journal, April 2014

Investigation of initial structures of aged ω-phase crystals in β-titanium alloys using high resolution electron microscopy journal, August 1997

Effects of ω-phase precipitation on β→α, α′′ transformations in a metastable β titanium alloy journal, August 2001

Heating-induced martensitic transformation and time-dependent shape memory behavior of Ti–Nb–O alloy journal, November 2014

Modelling and design of stress-induced martensite formation in metastable β Ti alloys journal, January 2014

Effect of solution heat treatment on the stress-induced martensite transformation in two new titanium alloys journal, August 2015

Effect of stress-induced α″ martensite on Young's modulus of β Ti–33.6Nb–4Sn alloy journal, December 2013

Thermal cycling of stress-induced martensite for high-performance shape memory effect journal, June 2014

Effect of heat treatment on shape memory effect and superelasticity in Ti–Mo–Sn alloys journal, November 2006

First principles theoretical investigations of low Young's modulus beta Ti–Nb and Ti–Nb–Zr alloys compositions for biomedical applications journal, May 2015

Thermal stability and phase transformations of martensitic Ti–Nb alloys journal, March 2013

Martensitic transformation, shape memory effect and superelasticity of Ti–Nb binary alloys journal, May 2006

First-principles calculations for development of low elastic modulus Ti alloys journal, November 2004

Microstructures and mechanical properties of Ti–Mo alloys cold-rolled and heat treated journal, October 2011

Non-isothermal phase transformation kinetics of ω phase in TB-13 titanium alloys journal, July 2010

Effects of annealing and deforming temperature on microstructure and deformation characteristics of Ti–Ni–V shape memory alloy journal, July 2012

Lattice parameter and hardness variations resulting from precipitation and misfit accommodation in a particle-reinforced AlSiCuMg alloy journal, May 1993

Beta Ti Alloys with Low Young's Modulus journal, January 2004

Structure-property relationship of cast Ti-Nb alloys journal, April 2002

Phase transformations and mechanical properties of biocompatible Ti–16.1Nb processed by severe plastic deformation journal, April 2015

Lattice modulation and superelasticity in oxygen-added β-Ti alloys journal, September 2011

Microstructural and Mechanical Properties of β-Type Ti–Nb–Sn Biomedical Alloys with Low Elastic Modulus journal, June 2019

Microstructure and mechanical properties of additive manufactured porous Ti–33Nb–4Sn scaffolds for orthopaedic applications journal, August 2019

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Fabrication of Ti–Nb–Ag alloy via powder metallurgy for biomedical applications
journal, April 2014

Investigation of initial structures of aged ω-phase crystals in β-titanium alloys using high resolution electron microscopy
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Effects of ω-phase precipitation on β→α, α′′ transformations in a metastable β titanium alloy
journal, August 2001

Heating-induced martensitic transformation and time-dependent shape memory behavior of Ti–Nb–O alloy
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Modelling and design of stress-induced martensite formation in metastable β Ti alloys
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Effect of solution heat treatment on the stress-induced martensite transformation in two new titanium alloys
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journal, May 2015

Thermal stability and phase transformations of martensitic Ti–Nb alloys
journal, March 2013

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First-principles calculations for development of low elastic modulus Ti alloys
journal, November 2004

Microstructures and mechanical properties of Ti–Mo alloys cold-rolled and heat treated
journal, October 2011

Non-isothermal phase transformation kinetics of ω phase in TB-13 titanium alloys
journal, July 2010

Effects of annealing and deforming temperature on microstructure and deformation characteristics of Ti–Ni–V shape memory alloy
journal, July 2012

Lattice parameter and hardness variations resulting from precipitation and misfit accommodation in a particle-reinforced AlSiCuMg alloy
journal, May 1993

Beta Ti Alloys with Low Young's Modulus
journal, January 2004

Structure-property relationship of cast Ti-Nb alloys
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Phase transformations and mechanical properties of biocompatible Ti–16.1Nb processed by severe plastic deformation
journal, April 2015

Lattice modulation and superelasticity in oxygen-added β-Ti alloys
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