Characterization of an aluminum alloy hemispherical shell fabricated via direct metal laser melting
Abstract
The ability of additive manufacturing to directly fabricate complex shapes provides characterization challenges for part qualification. The orientation of the microstructures produced by these processes will change relative to the surface normal of a complex part. In this work, the microscopy and x-ray tomography of an AlSi10Mg alloy hemispherical shell fabricated using powder bed metal additive manufacturing are used to illustrate some of these challenges. The shell was manufactured using an EOS M280 system in combination with EOS-specified powder and process parameters. The layer-by-layer process of building the shell with the powder bed additive manufacturing approach results in a position-dependent microstructure that continuously changes its orientation relative to the shell surface normal. X-ray tomography was utilized to examine the position-dependent size and distribution of porosity and surface roughness in the 98.6% dense part. Optical and electron microscopy were used to identify global and local position-dependent structures, grain morphologies, chemistry, and precipitate sizes and distributions. The rapid solidification processes within the fusion zone (FZ) after the laser transit results in a small dendrite size. Cell spacings taken from the structure in the middle of the FZ were used with published relationships to estimate a cooling rate of ~9 × 105 K/s.more »
- Authors:
-
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Publication Date:
- Research Org.:
- Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1240726
- Report Number(s):
- LA-UR-15-29591
Journal ID: ISSN 1047-4838; PII: 1798
- Grant/Contract Number:
- AC52-06NA25396
- Resource Type:
- Accepted Manuscript
- Journal Name:
- JOM. Journal of the Minerals, Metals & Materials Society
- Additional Journal Information:
- Journal Volume: 68; Journal Issue: 3; Journal ID: ISSN 1047-4838
- Publisher:
- Springer
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 42 ENGINEERING; 36 MATERIALS SCIENCE
Citation Formats
Holesinger, T. G., Carpenter, J. S., Lienert, T. J., Patterson, B. M., Papin, P. A., Swenson, H., and Cordes, N. L. Characterization of an aluminum alloy hemispherical shell fabricated via direct metal laser melting. United States: N. p., 2016.
Web. doi:10.1007/s11837-015-1798-5.
Holesinger, T. G., Carpenter, J. S., Lienert, T. J., Patterson, B. M., Papin, P. A., Swenson, H., & Cordes, N. L. Characterization of an aluminum alloy hemispherical shell fabricated via direct metal laser melting. United States. https://doi.org/10.1007/s11837-015-1798-5
Holesinger, T. G., Carpenter, J. S., Lienert, T. J., Patterson, B. M., Papin, P. A., Swenson, H., and Cordes, N. L. Mon .
"Characterization of an aluminum alloy hemispherical shell fabricated via direct metal laser melting". United States. https://doi.org/10.1007/s11837-015-1798-5. https://www.osti.gov/servlets/purl/1240726.
@article{osti_1240726,
title = {Characterization of an aluminum alloy hemispherical shell fabricated via direct metal laser melting},
author = {Holesinger, T. G. and Carpenter, J. S. and Lienert, T. J. and Patterson, B. M. and Papin, P. A. and Swenson, H. and Cordes, N. L.},
abstractNote = {The ability of additive manufacturing to directly fabricate complex shapes provides characterization challenges for part qualification. The orientation of the microstructures produced by these processes will change relative to the surface normal of a complex part. In this work, the microscopy and x-ray tomography of an AlSi10Mg alloy hemispherical shell fabricated using powder bed metal additive manufacturing are used to illustrate some of these challenges. The shell was manufactured using an EOS M280 system in combination with EOS-specified powder and process parameters. The layer-by-layer process of building the shell with the powder bed additive manufacturing approach results in a position-dependent microstructure that continuously changes its orientation relative to the shell surface normal. X-ray tomography was utilized to examine the position-dependent size and distribution of porosity and surface roughness in the 98.6% dense part. Optical and electron microscopy were used to identify global and local position-dependent structures, grain morphologies, chemistry, and precipitate sizes and distributions. The rapid solidification processes within the fusion zone (FZ) after the laser transit results in a small dendrite size. Cell spacings taken from the structure in the middle of the FZ were used with published relationships to estimate a cooling rate of ~9 × 105 K/s. Uniformly-distributed, nanoscale Si precipitates were found within the primary α-Al grains. A thin, distinct boundary layer containing larger α-Al grains and extended regions of the nanocrystalline divorced eutectic material surrounds the FZ. Moreover, subtle differences in the composition between the latter layer and the interior of the FZ were noted with scanning transmission electron microscopy (STEM) spectral imaging.},
doi = {10.1007/s11837-015-1798-5},
journal = {JOM. Journal of the Minerals, Metals & Materials Society},
number = 3,
volume = 68,
place = {United States},
year = {Mon Jan 11 00:00:00 EST 2016},
month = {Mon Jan 11 00:00:00 EST 2016}
}
Web of Science
Works referenced in this record:
Metal Additive Manufacturing: A Review
journal, April 2014
- Frazier, William E.
- Journal of Materials Engineering and Performance, Vol. 23, Issue 6
Laser additive manufacturing of metallic components: materials, processes and mechanisms
journal, May 2012
- Gu, D. D.; Meiners, W.; Wissenbach, K.
- International Materials Reviews, Vol. 57, Issue 3, p. 133-164
A review on selective laser sintering/melting (SLS/SLM) of aluminium alloy powders: Processing, microstructure, and properties
journal, October 2015
- Olakanmi, E. O.; Cochrane, R. F.; Dalgarno, K. W.
- Progress in Materials Science, Vol. 74
Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder
journal, March 2013
- Thijs, Lore; Kempen, Karolien; Kruth, Jean-Pierre
- Acta Materialia, Vol. 61, Issue 5
Selective laser melting of AlSi10Mg alloy: Process optimisation and mechanical properties development
journal, January 2015
- Read, Noriko; Wang, Wei; Essa, Khamis
- Materials & Design (1980-2015), Vol. 65
Selective laser melting of aluminum die-cast alloy—Correlations between process parameters, solidification conditions, and resulting mechanical properties
journal, February 2015
- Buchbinder, D.; Meiners, W.; Wissenbach, K.
- Journal of Laser Applications, Vol. 27, Issue S2
Microstructure and mechanical properties of aluminium alloy cellular lattice structures manufactured by direct metal laser sintering
journal, March 2015
- Yan, Chunze; Hao, Liang; Hussein, Ahmed
- Materials Science and Engineering: A, Vol. 628
Selective laser melting of aluminium components
journal, February 2011
- Louvis, Eleftherios; Fox, Peter; Sutcliffe, Christopher J.
- Journal of Materials Processing Technology, Vol. 211, Issue 2
High Power Selective Laser Melting (HP SLM) of Aluminum Parts
journal, January 2011
- Buchbinder, D.; Schleifenbaum, H.; Heidrich, S.
- Physics Procedia, Vol. 12
Additive Manufacturing of Al-12Si Alloy Via Pulsed Selective Laser Melting
journal, January 2015
- Chou, R.; Milligan, J.; Paliwal, M.
- JOM, Vol. 67, Issue 3
Combining X-ray CT and 3D printing technology to produce microcosms with replicable, complex pore geometries
journal, August 2012
- Otten, W.; Pajor, R.; Schmidt, S.
- Soil Biology and Biochemistry, Vol. 51
Sub-Micrometer X-ray Tomography of Radiolarians: Computer Modeling and Skeletonization
journal, September 2015
- Wagner, Roger C.; Jungck, John R.; Van Loo, Denis
- Microscopy Today, Vol. 23, Issue 5
X-ray tomography system to investigate granular materials during mechanical loading
journal, August 2014
- Athanassiadis, Athanasios G.; La Rivière, Patrick J.; Sidky, Emil
- Review of Scientific Instruments, Vol. 85, Issue 8
Synchrotron-Based X-ray Computed Tomography During Compression Loading of Cellular Materials
journal, April 2015
- Cordes, Nikolaus L.; Henderson, Kevin; Stannard, Tyler
- Microscopy Today, Vol. 23, Issue 3
Rapid solidification processing with specific application to aluminium alloys
journal, January 1992
- Lavernia, E. J.; Ayers, J. D.; Srivatsan, T. S.
- International Materials Reviews, Vol. 37, Issue 1
Liquation cracking in partial penetration aluminium welds: assessing tendencies to liquate, crack and backfill
journal, April 2004
- Huang, C.; Cao, G.; Kou, S.
- Science and Technology of Welding and Joining, Vol. 9, Issue 2
Hot Cracking in Welds of Aluminum and Magnesium Alloys
book, January 2011
- Kou, S.; Firouzdor, V.; Haygood, I. W.
- Hot Cracking Phenomena in Welds III
Microstructural variations in rapidly solidified alloys
journal, February 1988
- Boettinger, William J.
- Materials Science and Engineering, Vol. 98
Works referencing / citing this record:
Comparative investigations into microstructural and mechanical properties of as‐cast and laser powder bed fusion (LPBF) fabricated duplex steel (1.4517)
journal, April 2020
- Raffeis, I.; Vroomen, U.; Adjei‐Kyeremeh, F.
- Materialwissenschaft und Werkstofftechnik, Vol. 51, Issue 4
Process-Structure Linkages Using a Data Science Approach: Application to Simulated Additive Manufacturing Data
journal, March 2017
- Popova, Evdokia; Rodgers, Theron M.; Gong, Xinyi
- Integrating Materials and Manufacturing Innovation, Vol. 6, Issue 1
Spall fracture in additive manufactured tantalum
journal, December 2018
- Jones, D. R.; Fensin, S. J.; Ndefru, B. G.
- Journal of Applied Physics, Vol. 124, Issue 22
Modeling mechanical behavior of an additively manufactured metal structure with local texture variations: a study on model form error
journal, January 2019
- Brown, Judith A.; Bishop, Joseph E.
- Modelling and Simulation in Materials Science and Engineering, Vol. 27, Issue 2
Microstructure evolution and thermal properties of an additively manufactured, solution treatable AlSi10Mg part
journal, November 2018
- Yang, Pin; Deibler, Lisa A.; Bradley, Donald R.
- Journal of Materials Research, Vol. 33, Issue 23
Effect of thermal annealing on microstructure evolution and mechanical behavior of an additive manufactured AlSi10Mg part
journal, May 2018
- Yang, Pin; Rodriguez, Mark A.; Deibler, Lisa A.
- Journal of Materials Research, Vol. 33, Issue 12
Corrosion Behavior of Heat-Treated AlSi10Mg Manufactured by Laser Powder Bed Fusion
journal, June 2018
- Cabrini, Marina; Calignano, Flaviana; Fino, Paolo
- Materials, Vol. 11, Issue 7
Vergleichende Untersuchungen zu mikrostrukturellen und mechanischen Eigenschaften von Gussstahl und durch Laser-Pulver-Bett-Schmelzen hergestelltem Duplexstahl (1.4517)
text, January 2020
- Raffeis, Iris; Vroomen, Uwe; Adjei-Kyeremeh, Frank
- RWTH Aachen University
Corrosion Behavior of Heat-Treated AlSi10Mg Manufactured by Laser Powder Bed Fusion
journal, June 2018
- Cabrini, Marina; Calignano, Flaviana; Fino, Paolo
- Materials, Vol. 11, Issue 7