Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression
Abstract
Complementary advances in high pressure research apparatus and techniques make it possible to carry out time-resolved high pressure research using what would customarily be considered static high pressure apparatus. This work specifically explores time-resolved high pressure x-ray diffraction with rapid compression and/or decompression of a sample in a diamond anvil cell. Key aspects of the synchrotron beamline and ancillary equipment are presented here, including source considerations, rapid (de)compression apparatus, high frequency imaging detectors, and software suitable for processing large volumes of data. A number of examples are presented, including fast equation of state measurements, compression rate dependent synthesis of metastable states in silicon and germanium, and ultrahigh compression rates using a piezoelectric driven diamond anvil cell.
- Authors:
-
- Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Sponsoring Org.:
- USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1203748
- Alternate Identifier(s):
- OSTI ID: 1228699
- Grant/Contract Number:
- EAR-1128799; FG02-94ER14466; NA0001974; FG02-99ER45775; AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 86; Journal Issue: 7; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- ENGLISH
- Subject:
- 47 OTHER INSTRUMENTATION; Mechanical instruments; Image sensors; Synchrotrons; High pressure instruments; Insertion device; Diamond anvil cells; Quantum efficiency; Equations of state; X-ray diffraction; Metallurgy
Citation Formats
Smith, Jesse S., Sinogeikin, Stanislav V., Lin, Chuanlong, Rod, Eric, Bai, Ligang, and Shen, Guoyin. Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression. United States: N. p., 2015.
Web. doi:10.1063/1.4926887.
Smith, Jesse S., Sinogeikin, Stanislav V., Lin, Chuanlong, Rod, Eric, Bai, Ligang, & Shen, Guoyin. Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression. United States. https://doi.org/10.1063/1.4926887
Smith, Jesse S., Sinogeikin, Stanislav V., Lin, Chuanlong, Rod, Eric, Bai, Ligang, and Shen, Guoyin. Fri .
"Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression". United States. https://doi.org/10.1063/1.4926887. https://www.osti.gov/servlets/purl/1203748.
@article{osti_1203748,
title = {Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression},
author = {Smith, Jesse S. and Sinogeikin, Stanislav V. and Lin, Chuanlong and Rod, Eric and Bai, Ligang and Shen, Guoyin},
abstractNote = {Complementary advances in high pressure research apparatus and techniques make it possible to carry out time-resolved high pressure research using what would customarily be considered static high pressure apparatus. This work specifically explores time-resolved high pressure x-ray diffraction with rapid compression and/or decompression of a sample in a diamond anvil cell. Key aspects of the synchrotron beamline and ancillary equipment are presented here, including source considerations, rapid (de)compression apparatus, high frequency imaging detectors, and software suitable for processing large volumes of data. A number of examples are presented, including fast equation of state measurements, compression rate dependent synthesis of metastable states in silicon and germanium, and ultrahigh compression rates using a piezoelectric driven diamond anvil cell.},
doi = {10.1063/1.4926887},
journal = {Review of Scientific Instruments},
number = 7,
volume = 86,
place = {United States},
year = {Fri Jul 24 00:00:00 EDT 2015},
month = {Fri Jul 24 00:00:00 EDT 2015}
}
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Works referencing / citing this record:
Online remote control systems for static and dynamic compression and decompression using diamond anvil cells
journal, July 2015
- Sinogeikin, Stanislav V.; Smith, Jesse S.; Rod, Eric
- Review of Scientific Instruments, Vol. 86, Issue 7
A CO 2 laser heating system for in situ high pressure-temperature experiments at HPCAT
journal, August 2018
- Smith, Dean; Smith, Jesse S.; Childs, Christian
- Review of Scientific Instruments, Vol. 89, Issue 8
Advanced Spectral Analysis Program
journal, February 2019
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Fly scan apparatus for high pressure research using diamond anvil cells
journal, January 2019
- Smith, Jesse S.; Rod, Eric A.; Shen, Guoyin
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Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments
journal, February 2019
- Hrubiak, Rostislav; Smith, Jesse S.; Shen, Guoyin
- Review of Scientific Instruments, Vol. 90, Issue 2
New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments
journal, June 2019
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In situ x-ray diffraction study of polyamorphism in H 2 O under isothermal compression and decompression
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Experimental evidence of low-density liquid water upon rapid decompression
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- Lin, Chuanlong; Smith, Jesse S.; Sinogeikin, Stanislav V.
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