Search Menu
DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information
Search Scholarly Publications

Title: Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures

Abstract

The problem of calculating the inverse pole figure (IPF) is analyzed from the perspective of the application of time-of flight neutron diffraction toin situmonitoring of the thermomechanical behavior of engineering materials. On the basis of a quasi-Monte Carlo (QMC) method, a consistent set of grain orientations is generated and used to compute the weighting factors for IPF normalization. The weighting factors are instrument dependent and were calculated for the engineering materials diffractometer VULCAN (Spallation Neutron Source, Oak Ridge National Laboratory). The QMC method is applied to face-centered cubic structures and can be easily extended to other crystallographic symmetries. Examples include 316LN stainless steelin situloaded in tension at room temperature and an Al–2%Mg alloy, substantially deformed by cold rolling and in situannealed up to 653 K.

Authors:
 [1];  [1];  [1];  [1];  [2];  [3];  [4]
+ Show Author Affiliations
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Los Alamos National Lab. (LANL), Los Alamos, NM (United States). Los Alamos Neutron Science Center (LANSCE)
  3. Los Alamos National Lab. (LANL), Los Alamos, NM (United States). Materials Science and Technology Div.
  4. City Univ. of Hong Kong (China)
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Spallation Neutron Source (SNS)
Sponsoring Org.:
USDOE Office of Science (SC)
OSTI Identifier:
1185368
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Applied Crystallography (Online)
Additional Journal Information:
Journal Name: Journal of Applied Crystallography (Online); Journal Volume: 47; Journal Issue: 6; Journal ID: ISSN 1600-5767
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
73 NUCLEAR PHYSICS AND RADIATION PHYSICS; TOF; VULCAN; grain orientation; inverse pole figure

Citation Formats

Stoica, Grigoreta M., Stoica, Alexandru Dan, An, Ke, Ma, Dong, Vogel, S. C., Carpenter, J. S., and Wang, Xun-Li. Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures. United States: N. p., 2014. Web. doi:10.1107/S1600576714023036.
Copy to clipboard
Stoica, Grigoreta M., Stoica, Alexandru Dan, An, Ke, Ma, Dong, Vogel, S. C., Carpenter, J. S., & Wang, Xun-Li. Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures. United States. https://doi.org/10.1107/S1600576714023036
Copy to clipboard
Stoica, Grigoreta M., Stoica, Alexandru Dan, An, Ke, Ma, Dong, Vogel, S. C., Carpenter, J. S., and Wang, Xun-Li. Fri . "Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures". United States. https://doi.org/10.1107/S1600576714023036. https://www.osti.gov/servlets/purl/1185368.
Copy to clipboard
@article{osti_1185368,
title = {Extracting grain-orientation-dependent data from in situ time-of-flight neutron diffraction. I. Inverse pole figures},
author = {Stoica, Grigoreta M. and Stoica, Alexandru Dan and An, Ke and Ma, Dong and Vogel, S. C. and Carpenter, J. S. and Wang, Xun-Li},
abstractNote = {The problem of calculating the inverse pole figure (IPF) is analyzed from the perspective of the application of time-of flight neutron diffraction toin situmonitoring of the thermomechanical behavior of engineering materials. On the basis of a quasi-Monte Carlo (QMC) method, a consistent set of grain orientations is generated and used to compute the weighting factors for IPF normalization. The weighting factors are instrument dependent and were calculated for the engineering materials diffractometer VULCAN (Spallation Neutron Source, Oak Ridge National Laboratory). The QMC method is applied to face-centered cubic structures and can be easily extended to other crystallographic symmetries. Examples include 316LN stainless steelin situloaded in tension at room temperature and an Al–2%Mg alloy, substantially deformed by cold rolling and in situannealed up to 653 K.},
doi = {10.1107/S1600576714023036},
journal = {Journal of Applied Crystallography (Online)},
number = 6,
volume = 47,
place = {United States},
year = {Fri Nov 28 00:00:00 EST 2014},
month = {Fri Nov 28 00:00:00 EST 2014}
}
Copy to clipboard
Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1107/S1600576714023036
Copyright Statement
Other availability
Search WorldCat Search WorldCat to find libraries that may hold this journal
Citation Metrics:
Cited by: 14 works
Citation information provided by
Web of Science
Save / Share:
Export Metadata
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.

Works referenced in this record:

First In Situ Lattice Strains Measurements Under Load at VULCAN
journal, October 2010

  • An, Ke; Skorpenske, Harley D.; Stoica, Alexandru D.
  • Metallurgical and Materials Transactions A, Vol. 42, Issue 1
  • DOI: 10.1007/s11661-010-0495-9

Texture Analysis with MTEX – Free and Open Source Software Toolbox
journal, February 2010

Calculation of the rotation rate field on the basis of experimental texture data
journal, January 1993

Prediction of deformation texture using a physical principle of conservatiol
journal, September 1982

Shifting scintillator prototype large pixel wavelength-shifting fiber detector for the POWGEN3 powder diffractometer
journal, August 2004

  • Crow, M. L.; Hodges, J. P.; Cooper, R. G.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 529, Issue 1-3
  • DOI: 10.1016/j.nima.2004.04.167

On the efficiency of certain quasi-random sequences of points in evaluating multi-dimensional integrals
journal, December 1960

X. Quantitative measurement of preferred orientation in rolled uranium bars
journal, January 1952

  • Harris, G. B.
  • The London, Edinburgh, and Dublin Philosophical Magazine and Journal of Science, Vol. 43, Issue 336
  • DOI: 10.1080/14786440108520972

Application of symmetrized harmonics expansion to correction of the preferred orientation effect
journal, August 1993

Modelling deformation texture formation by orientation flow fields
journal, December 1991

Rietveld texture analysis from diffraction images
journal, November 2007

Combined texture and structure analysis of deformed limestone from time-of-flight neutron diffraction spectra
journal, January 1997

  • Lutterotti, L.; Matthies, S.; Wenk, H. -R.
  • Journal of Applied Physics, Vol. 81, Issue 2
  • DOI: 10.1063/1.364220

Texture Evolution and Phase Transformation in Titanium Investigated by In-Situ Neutron Diffraction
journal, March 2011

Some basic concepts of texture analysis and comparison of three methods to calculate orientation distributions from pole figures
journal, August 1988

  • Matthies, S.; Wenk, H. -R.; Vinel, G. W.
  • Journal of Applied Crystallography, Vol. 21, Issue 4
  • DOI: 10.1107/S0021889888000275

Effect of fluorine doping on highly transparent conductive spray deposited nanocrystalline tin oxide thin films
journal, September 2009

Reducing the Effects of Nonuniform Pole Distribution in Inverse Pole Figure Studies
journal, April 1959

  • Morris, Peter R.
  • Journal of Applied Physics, Vol. 30, Issue 4
  • DOI: 10.1063/1.1702413

Texture in Rietveld refinement
journal, October 1992

On elastic moduli and elastic anisotropy in polycrystalline martensitic NiTi
journal, August 2011

A profile refinement method for nuclear and magnetic structures
journal, June 1969

Three-Dimensional Characterization of Microstructure by Electron Back-Scatter Diffraction
journal, August 2007

Large Strain Deformation in Uranium 6 Wt Pct Niobium
journal, November 2011

  • Tupper, Catherine N.; Brown, Don W.; Field, Robert D.
  • Metallurgical and Materials Transactions A, Vol. 43, Issue 2
  • DOI: 10.1007/s11661-011-0931-5

Texture measurements using the new neutron diffractometer HIPPO and their analysis using the Rietveld method
journal, March 2004

  • Vogel, Sven C.; Hartig, Christian; Lutterotti, Luca
  • Powder Diffraction, Vol. 19, Issue 1
  • DOI: 10.1154/1.1649961

Quantitative texture analysis by Rietveld refinement
journal, August 1997

Randomized Halton sequences
journal, October 2000

VULCAN—The engineering diffractometer at the SNS
journal, November 2006

First Results from the VULCAN Diffractometer at the SNS
journal, May 2010

Focusing neutron guides for VULCAN—Design aspects, estimated performance, and detector deployment
journal, February 2009

  • Wang, X. -L.; Stoica, A. D.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 600, Issue 1
  • DOI: 10.1016/j.nima.2008.11.050

Texture analysis with the new HIPPO TOF diffractometer
journal, December 2003

  • Wenk, H. -R.; Lutterotti, L.; Vogel, S.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 515, Issue 3
  • DOI: 10.1016/j.nima.2003.05.001

Rietveld texture analysis from TOF neutron diffraction data
journal, September 2010

  • Wenk, H. -R.; Lutterotti, L.; Vogel, S. C.
  • Powder Diffraction, Vol. 25, Issue 3
  • DOI: 10.1154/1.3479004

Rotation field and continuity equation for texture evolution
journal, January 1984

Lattice rotations of individual bulk grains Part II: correlation with initial orientation and model comparison
journal, June 2004

Texture memory and strain-texture mapping in a NiTi shape memory alloy
journal, August 2007

  • Ye, B.; Majumdar, B. S.; Dutta, I.
  • Applied Physics Letters, Vol. 91, Issue 6
  • DOI: 10.1063/1.2768899

Texture development and strain hysteresis in a NiTi shape-memory alloy during thermal cycling under load
journal, May 2009

    Sort by:
    [ × clear filter / sort ]

    Works referencing / citing this record:

    A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory
    journal, September 2018

    • Calder, S.; An, K.; Boehler, R.
    • Review of Scientific Instruments, Vol. 89, Issue 9
    • DOI: 10.1063/1.5033906

    Time-of-Flight Neutron Diffraction (TOF-ND) Analyses of the Composition and Minting of Ancient Judaean “Biblical” Coins
    journal, March 2019

    • Nagler, Stephen E.; Stoica, Alexandru D.; Stoica, Grigoreta M.
    • Journal of Analytical Methods in Chemistry, Vol. 2019
    • DOI: 10.1155/2019/6164058

    Distinct Recrystallization Pathways in a Cold-Rolled Al-2%Mg Alloy Evidenced by In-Situ Neutron Diffraction
    journal, September 2018

    • Stoica, Grigoreta; Dessieux, Luc; Stoica, Alexandru
    • Quantum Beam Science, Vol. 2, Issue 3
    • DOI: 10.3390/qubs2030017
      Sort by:
      [ × clear filter / sort ]

      Similar Records in DOE PAGES and OSTI.GOV collections: