Laboratory-Based Micro-X-ray Computed Tomography of Energy Materials at Idaho National Laboratory

Chuirazzi, William C.; Kancharla, Rahul Reddy; Morankar, Swapnil Kishor

doi:10.1007/s11837-024-06970-z

Title: Laboratory-Based Micro-X-ray Computed Tomography of Energy Materials at Idaho National Laboratory

Journal Article · 18 December 2024 · JOM. Journal of the Minerals, Metals & Materials Society

DOI: https://doi.org/10.1007/s11837-024-06970-z · OSTI ID:2482580

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Idaho National Laboratory (INL), Idaho Falls, ID (United States)

The Idaho National Laboratory (INL) has implemented laboratory-based micro-X-ray computed tomography in a laboratory equipped for the examination of highly radioactive samples. This capability provides nondestructive three-dimensional volumetric information on samples to inform subsequent traditional destructive examinations as well as real-world inputs for high-fidelity scientific modeling. Samples can be imaged with spatial resolutions ranging from several hundred nm/voxel up to ~ 100 µm/voxel. The best usable spatial resolution achieved to date is 384 nm/voxel with this instrument, while the highest radiological dose rate of a sample imaged is ~ 60 R/h β/γ on contact. Advanced data analysis, including custom tomographic reconstruction and segmentation methods, have also been developed to support this capability. In addition to traditional digital X-ray radiography and tomography, this instrument is also able to visualize in situ tensile and compression testing as well as perform diffraction contrast tomography. This work describes the X-ray computed tomography post-irradiation examination capabilities at INL, as well as detailing a variety of applications this instrument has examined.

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Research Organization:: Idaho National Laboratory (INL), Idaho Falls, ID (United States)

Sponsoring Organization:: USDOE Laboratory Directed Research and Development (LDRD) Program; USDOE Office of Nuclear Energy (NE)

Grant/Contract Number:: AC07-05ID14517

OSTI ID:: 2482580

Report Number(s):: INL/JOU--24-77365-Rev001

Journal Information:: JOM. Journal of the Minerals, Metals & Materials Society, Journal Name: JOM. Journal of the Minerals, Metals & Materials Society Journal Issue: 3 Vol. 77; ISSN 1047-4838; ISSN 1543-1851

Publisher:: SpringerCopyright Statement

Country of Publication:: United States

Language:: English

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