Material Characterization Study of Magnetite Nanocrystals for RF Sensing

Sherburne, Michael D.; Dreier, Timothy A.; Klitsner, Benjamin H.; Huber, Dale L.; Ivanov, Sergei A.; Parks, Chris; Simons, Matt T.; Schamiloglu, Edl

doi:10.1021/acsomega.4c04589

Title: Material Characterization Study of Magnetite Nanocrystals for RF Sensing

Journal Article · 24 September 2024 · ACS Omega

DOI: https://doi.org/10.1021/acsomega.4c04589 · OSTI ID:2472597

^[1]; Dreier, Timothy A. ^[2]; Klitsner, Benjamin H. ^[2];

^[2];

^[3]; Parks, Chris ^[4]; Simons, Matt T. ^[4]; Schamiloglu, Edl ^[5]

Johns Hopkins Univ., Baltimore, MD (United States)
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
National Inst. of Standards and Technology (NIST), Boulder, CO (United States)
Univ. of New Mexico, Albuquerque, NM (United States)

Magnetite nanocrystals show promise for electrically small gigahertz frequency applications, which could lead to miniaturizing transformer cores and new sensing technologies. This work presents a rigorous radiofrequency characterization of these nanocrystals using vector network analyzer (VNA) ferromagnetic resonance (FMR) measurements. For the first time, two different average diameters of Fe₃O₄ nanocrystals are investigated (7.3 and 20.2 nm). When the VNA–FMR results were compared to micromagnetic simulations, the magnetic anisotropy (K₁) deviated from the ideal mean orientation value of K₁/2 to K₁/80 for the 7.3 nm nanocrystal. In contrast, the obtained magnetic anisotropy in 20.2 nm nanocrystals slightly deviated to K₁/11 due to less structural deformations. These findings resulted in a newly proposed methodology for an approximate simulation based on VNA–FMR measurements. In addition, this work estimates the approximate amount of nanocrystals needed to measure a useful VNA–FMR spectrum.

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Research Organization:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: 89233218CNA000001; NA0003525

OSTI ID:: 2472597

Report Number(s):: LA-UR--24-29830

Journal Information:: ACS Omega, Journal Name: ACS Omega Journal Issue: 40 Vol. 9; ISSN 2470-1343

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

References (36)

Development of a high‐sensitivity VNA‐FMR spectrometer with field modulation detection and its application to magnetic characterization Tamaru, Shingo; Yamamoto, Tatsuya; Onuma, Tomoyuki Electronics and Communications in Japan, Vol. 104, Issue 3 https://doi.org/10.1002/ecj.12320	journal	September 2021
Heating magnetic fluid with alternating magnetic field Rosensweig, R. E. Journal of Magnetism and Magnetic Materials, Vol. 252 https://doi.org/10.1016/S0304-8853(02)00706-0	journal	November 2002
From pure superparamagnetism to glass collective state in γ-Fe2O3 nanoparticle assemblies Dormann, J. L.; Fiorani, D.; Cherkaoui, R. Journal of Magnetism and Magnetic Materials, Vol. 203, Issue 1-3 https://doi.org/10.1016/S0304-8853(99)00180-8	journal	August 1999
Enhanced Nanoparticle Size Control by Extending LaMer’s Mechanism Vreeland, Erika C.; Watt, John; Schober, Gretchen B. Chemistry of Materials, Vol. 27, Issue 17 https://doi.org/10.1021/acs.chemmater.5b02510	journal	August 2015
Temperature and Excitation Wavelength Dependence of Surface-Plasmon-Mediated Emission from CdSe Nanocrystals Lu, Liu; Chen, Daifen; Zhao, Guangming The Journal of Physical Chemistry C, Vol. 114, Issue 43 https://doi.org/10.1021/jp107211n	journal	October 2010
Temperature Dependence of the Photoluminescence of InP/ZnS Quantum Dots Narayanaswamy, Arun; Feiner, L. F.; van der Zaag, P. J. The Journal of Physical Chemistry C, Vol. 112, Issue 17 https://doi.org/10.1021/jp800339m	journal	May 2008
Intrinsic origin of interfacial second-order magnetic anisotropy in ferromagnet/normal metal heterostructures Gweon, Hyung Keun; Park, Hyeon-Jong; Kim, Kyoung-Whan NPG Asia Materials, Vol. 12, Issue 1 https://doi.org/10.1038/s41427-020-0205-z	journal	March 2020
Efficient and Sensitive Electrically Small Rectenna for Ultra-Low Power RF Energy Harvesting Assimonis, Stylianos D.; Fusco, Vincent; Georgiadis, Apostolos Scientific Reports, Vol. 8, Issue 1 https://doi.org/10.1038/s41598-018-33388-w	journal	October 2018
An ultra wideband-high spatial resolution-compact electric field sensor based on Lab-on-Fiber technology Calero, V.; Suarez, M. -A.; Salut, R. Scientific Reports, Vol. 9, Issue 1 https://doi.org/10.1038/s41598-019-44644-y	journal	May 2019
The role of faceting and elongation on the magnetic anisotropy of magnetite Fe3O4 nanocrystals Moreno, Roberto; Poyser, Samuel; Meilak, Daniel Scientific Reports, Vol. 10, Issue 1 https://doi.org/10.1038/s41598-020-58976-7	journal	February 2020
Ultra-high rate of temperature increment from superparamagnetic nanoparticles for highly efficient hyperthermia Lee, Jae-Hyeok; Kim, Bosung; Kim, Yongsub Scientific Reports, Vol. 11, Issue 1 https://doi.org/10.1038/s41598-021-84424-1	journal	March 2021
Electro-optical measurement of intense electric field on a high energy pulsed power accelerator Owens, Israel; Grabowski, Chris; Biller, Andrew Scientific Reports, Vol. 11, Issue 1 https://doi.org/10.1038/s41598-021-89851-8	journal	May 2021
Designing magnetic field sensor based on tapered photonic crystal fibre assisted by a ferrofluid Taghizadeh, Mostafa; Bozorgzadeh, Forough; Ghorbani, Marjan Scientific Reports, Vol. 11, Issue 1 https://doi.org/10.1038/s41598-021-93568-z	journal	July 2021
Highly efficient heat-dissipation power driven by ferromagnetic resonance in MFe2O4 (M = Fe, Mn, Ni) ferrite nanoparticles Lee, Jae-Hyeok; Kim, Yongsub; Kim, Sang-Koog Scientific Reports, Vol. 12, Issue 1 https://doi.org/10.1038/s41598-022-09159-z	journal	March 2022
New Permanent Magnet Materials Nesbitt, E. A.; Willens, R. H.; Sherwood, R. C. Applied Physics Letters, Vol. 12, Issue 11 https://doi.org/10.1063/1.1651855	journal	June 1968
Ferromagnetic resonance linewidth in metallic thin films: Comparison of measurement methods Kalarickal, Sangita S.; Krivosik, Pavol; Wu, Mingzhong Journal of Applied Physics, Vol. 99, Issue 9 https://doi.org/10.1063/1.2197087	journal	May 2006
Temperature tunability of photonic crystal fiber filled with Fe3O4 nanoparticle fluid Miao, Yinping; Liu, Bo; Zhang, Kailiang Applied Physics Letters, Vol. 98, Issue 2 https://doi.org/10.1063/1.3540647	journal	January 2011
Photonic crystal fiber injected with Fe3O4 nanofluid for magnetic field detection Thakur, Harneet V.; Nalawade, Sandipan M.; Gupta, Swati Applied Physics Letters, Vol. 99, Issue 16 https://doi.org/10.1063/1.3651490	journal	October 2011
Magneto-optical fiber sensor based on bandgap effect of photonic crystal fiber infiltrated with magnetic fluid Zu, Peng; Chiu Chan, Chi; Gong, Tianxun Applied Physics Letters, Vol. 101, Issue 24 https://doi.org/10.1063/1.4772017	journal	December 2012
Determination of anisotropy constants via fitting of magnetic hysteresis to numerical calculation of Stoner–Wohlfarth model Peterson, S. F.; Idzerda, Y. U. AIP Advances, Vol. 11, Issue 8 https://doi.org/10.1063/5.0051454	journal	August 2021
Magneto-optical sensor based on the bandgap effect of a hollow-core photonic crystal fiber injected with Fe3O4 Aobaid, R. A.; Hussain, H. S. IOP Conference Series: Materials Science and Engineering, Vol. 871, Issue 1 https://doi.org/10.1088/1757-899X/871/1/012068	journal	June 2020
Blocking and Freezing of Magnetic Moments for Iron Nitride Fine Particle Systems Mamiya, H.; Nakatani, I.; Furubayashi, T. Physical Review Letters, Vol. 80, Issue 1 https://doi.org/10.1103/PhysRevLett.80.177	journal	January 1998
Temperature Dependence of the Luminescence Lifetime of Single C d S e / Z n S Quantum Dots Labeau, Olivier; Tamarat, Philippe; Lounis, Brahim Physical Review Letters, Vol. 90, Issue 25 https://doi.org/10.1103/PhysRevLett.90.257404	journal	June 2003
A re-examination of the fundamental limits on the radiation Q of electrically small antennas McLean, J. S. IEEE Transactions on Antennas and Propagation, Vol. 44, Issue 5 https://doi.org/10.1109/8.496253	journal	May 1996
Electric Field Sensor Approach to Determine Fidelity and Overmoding Region of GTEM Cell Sherburne, Michael D.; Sommerdyke, Heather L.; Erickson, Nicholas G. IEEE Sensors Journal, Vol. 23, Issue 4 https://doi.org/10.1109/JSEN.2022.3233571	journal	February 2023
Calibrating a Radio Frequency Electrooptic Sensor for Field-Relevant Temperature Conditions in a Laboratory Setting Sherburne, Michael D.; Harjes, Cameron D.; Pohle, Hugh H. IEEE Sensors Journal, Vol. 23, Issue 6 https://doi.org/10.1109/JSEN.2023.3242330	journal	March 2023
Exchange coupled composite media for perpendicular magnetic recording Victora, R. H.; Shen, X. IEEE Transactions on Magnetics, Vol. 41, Issue 10 https://doi.org/10.1109/TMAG.2005.855263	journal	October 2005
Ubermag: Toward More Effective Micromagnetic Workflows Beg, Marijan; Lang, Martin; Fangohr, Hans IEEE Transactions on Magnetics, Vol. 58, Issue 2 https://doi.org/10.1109/TMAG.2021.3078896	journal	February 2022
Minimally invasive optical sensors for microwave-electric-field exposure measurements Behague, Florent; Calero, Venancio; Coste, Antoine Journal of Optical Microsystems, Vol. 1, Issue 02 https://doi.org/10.1117/1.jom.1.2.020902	journal	April 2021
Magnetic nanoparticles: preparation, physical properties, and applications in biomedicine Akbarzadeh, Abolfazl; Samiei, Mohamad; Davaran, Soodabeh Nanoscale Research Letters, Vol. 7, Issue 1 https://doi.org/10.1186/1556-276x-7-144	journal	January 2012
Optimizing colormaps with consideration for color vision deficiency to enable accurate interpretation of scientific data Nuñez, Jamie R.; Anderton, Christopher R.; Renslow, Ryan S. PLOS ONE, Vol. 13, Issue 7 https://doi.org/10.1371/journal.pone.0199239	journal	August 2018
Review of Applications of the Laboratory for Electromagnetic Compatibility Infrastructure Staniec, Kamil; Jóskiewicz, Zbigniew; Janukiewicz, Jarosław International Journal of Electronics and Telecommunications https://doi.org/10.24425/ijet.2020.131852	journal	January 2020
A System for Monitoring of Broadband FMR Phenomenon in Low-Carbon Steel Films Subjected to Deformations Psuj, Grzegorz; Lopato, Przemyslaw; Maciusowicz, Michal Sensors, Vol. 21, Issue 13 https://doi.org/10.3390/s21134301	journal	June 2021
Rapid Prototyping for Nanoparticle-Based Photonic Crystal Fiber Sensors Sherburne, Michael; Harjes, Cameron; Klitsner, Benjamin Sensors, Vol. 24, Issue 12 https://doi.org/10.3390/s24123707	journal	June 2024
Magnetic interactions between nanoparticles Mørup, Steen; Hansen, Mikkel Fougt; Frandsen, Cathrine Beilstein Journal of Nanotechnology, Vol. 1 https://doi.org/10.3762/bjnano.1.22	journal	January 2010
A general waveguide circuit theory Marks, R. B.; Williams, D. F. Journal of Research of the National Institute of Standards and Technology, Vol. 97, Issue 5 https://doi.org/10.6028/jres.097.024	journal	September 1992

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Title: Material Characterization Study of Magnetite Nanocrystals for RF Sensing

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