Review of Solid State Consolidation Processing Techniques of ODS Steels (Hot Extrusion, Hot Isostatic Pressing, Spark Plasma Sintering, and Stir Friction Consolidation): Resulting Microstructures and Mechanical Properties

deJong, Matthew; Horn, Timothy; Kaoumi, Djamel

doi:10.1007/s11837-024-06853-3

Title: Review of Solid State Consolidation Processing Techniques of ODS Steels (Hot Extrusion, Hot Isostatic Pressing, Spark Plasma Sintering, and Stir Friction Consolidation): Resulting Microstructures and Mechanical Properties

Journal Article · 31 December 2023 · The Journal of The Minerals, Metals & Materials Society

DOI: https://doi.org/10.1007/s11837-024-06853-3 · OSTI ID:2453862

deJong, Matthew ^[1]; Horn, Timothy ^[2]; Kaoumi, Djamel ^[2]

North Carolina State University, Raleigh, NC (United States); North Carolina State University
North Carolina State University, Raleigh, NC (United States)

This paper reviews the solid-state consolidation processing techniques for Oxide Dispersion Strengthened steels and compares them in terms of the resulting microstructure and reported mechanical properties. Synthesis techniques include hot extrusion, hot isostatic pressing, spark plasma sintering and friction consolidation. The effects of process parameters on the resulting microstructures and performance are discussed for each technique. Average oxide size, average grain size, and porosity are compared across techniques, as well as mechanical strength and ductility. Across consolidation techniques where temperature can be controlled, a low sintering temperature with a high sintering pressure is favorable for keeping oxide sizes, grain sizes, and porosity low. The use of yttrium and titanium for oxide formation has been evidenced to reduce oxide sizes, and tungsten additions have been shown to improve strength. Current literature suggests that the more mature hot extrusion technique produces stronger steel with consistently fine oxides, while other alternative solid-state consolidation, while promising, offer margin for improvement.

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Research Organization:: North Carolina State University

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: NA0003996

OSTI ID:: 2453862

Journal Information:: The Journal of The Minerals, Metals & Materials Society, Journal Name: The Journal of The Minerals, Metals & Materials Society; ISSN 1047-4838

Country of Publication:: United States

Language:: English

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Tantalum and molybdenum barriers to prevent carbon diffusion in spark plasma sintered tungsten Kwak, Nojun; Min, Guensik; Oh, Yeonju Scripta Materialia, Vol. 196 https://doi.org/10.1016/j.scriptamat.2021.113759	journal	April 2021
Understanding ferrite deformation caused by austenite to martensite transformation in dual phase steels Atreya, Vibhor; Bos, Cornelis; Santofimia, Maria J. Scripta Materialia, Vol. 202 https://doi.org/10.1016/j.scriptamat.2021.114032	journal	September 2021
Studies on wear behavior of nano-Y2O3 dispersed ferritic steel developed by mechanical alloying and hot isostatic pressing Karak, S. K.; Vishnu, C. S.; Witczak, Z. Wear, Vol. 270, Issue 1-2 https://doi.org/10.1016/j.wear.2010.08.021	journal	December 2010
The Precipitated Particle Refinement in High-Cr ODS Steels by Microalloying Element Addition Li, Yingying; Zhang, Liye; Long, Dijun Materials, Vol. 14, Issue 24 https://doi.org/10.3390/ma14247767	journal	December 2021
Assessment of Ferritic ODS Steels Obtained by Laser Additive Manufacturing Autones, Lucas; Aubry, Pascal; Ribis, Joel Materials, Vol. 16, Issue 6 https://doi.org/10.3390/ma16062397	journal	March 2023
Effect of Small Variations in Zr Content on the Microstructure and Properties of Ferritic ODS Steels Consolidated by SPS García-Junceda, Andrea; Macía, Eric; Garbiec, Dariusz Metals, Vol. 10, Issue 3 https://doi.org/10.3390/met10030348	journal	March 2020
Development of New 14 Cr ODS Steels by Using New Oxides Formers and B as an Inhibitor of the Grain Growth Meza, Alberto; Macía, Eric; García-Junceda, Andrea Metals, Vol. 10, Issue 10 https://doi.org/10.3390/met10101344	journal	October 2020
Characterization of 14Cr ODS Steel Fabricated by Spark Plasma Sintering Zhao, Qian; Qiao, Zhixia; Liu, Yongchang Metals, Vol. 9, Issue 2 https://doi.org/10.3390/met9020200	journal	February 2019
Microstructure Evolution of Mechanically Alloyed ODS Ferritic Steels during Hot Extrusion Couvrat, Mathieu; Chaffron, Laurent; Nunes, Daniel Solid State Phenomena, Vol. 172-174 https://doi.org/10.4028/www.scientific.net/SSP.172-174.721	journal	June 2011
Effects of heat Treatments on Microstructures and Mechanical Properties of dual Phase ods Steels for high Temperature Strength Noh, Sanghoon; Choi, Byoung-Kwon; Han, Chang-Hee Nuclear Engineering and Technology, Vol. 45, Issue 6 https://doi.org/10.5516/net.02.2013.529	journal	November 2013

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36 MATERIALS SCIENCE

Title: Review of Solid State Consolidation Processing Techniques of ODS Steels (Hot Extrusion, Hot Isostatic Pressing, Spark Plasma Sintering, and Stir Friction Consolidation): Resulting Microstructures and Mechanical Properties

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