Effects of Halides on Organic Compound Degradation during Plasma Treatment of Brines

Chen, Moshan; Moher, Dillon; Rogers, Jacqueline; Yatom, Shurik; Thimsen, Elijah; Parker, Kimberly M.

doi:10.1021/acs.est.3c07162

Title: Effects of Halides on Organic Compound Degradation during Plasma Treatment of Brines

Journal Article · 05 March 2024 · Environmental Science and Technology

DOI: https://doi.org/10.1021/acs.est.3c07162 · OSTI ID:2352444

^[1];

^[2]; Thimsen, Elijah ^[1];

^[1]

Washington Univ., St. Louis, MO (United States)
Princeton Plasma Physics Laboratory (PPPL), Princeton, NJ (United States)

Plasma has been proposed as an alternative strategy to treat organic contaminants in brines. Chemical degradation in these systems is expected to be partially driven by halogen oxidants, which have been detected in halide-containing solutions exposed to plasma. In this study, we characterized specific mechanisms involving the formation and reactions of halogen oxidants during plasma treatment. Here, we first demonstrated that addition of halides accelerated the degradation of a probe compound known to react quickly with halogen oxidants (i.e., para-hydroxybenzoate) but did not affect the degradation of a less reactive probe compound (i.e., benzoate). This effect was attributed to the degradation of para-hydroxybenzoate by hypohalous acids, which were produced via a mechanism involving halogen radicals as intermediates. We applied this mechanistic insight to investigate the impact of constituents in brines on reactions driven by halogen oxidants during plasma treatment. Bromide, which is expected to occur alongside chloride in brines, was required to enable halogen oxidant formation, consistent with the generation of halogen radicals from the oxidation of halides by hydroxyl radical. Other constituents typically present in brines (i.e., carbonates, organic matter) slowed the degradation of organic compounds, consistent with their ability to scavenge species involved during plasma treatment.

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Research Organization:: Princeton Plasma Physics Laboratory (PPPL), Princeton, NJ (United States)

Sponsoring Organization:: USDOE; National Science Foundation (NSF)

Grant/Contract Number:: AC02-09CH11466

OSTI ID:: 2352444

Journal Information:: Environmental Science and Technology, Journal Name: Environmental Science and Technology Journal Issue: 11 Vol. 58; ISSN 0013-936X

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

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37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
brine treatment
halides
halogen radicals
hypohalous acids
plasma

Title: Effects of Halides on Organic Compound Degradation during Plasma Treatment of Brines

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