Exploring toroidal anvil profiles for larger sample volumes above 4 Mbar

Zurkowski, Claire C.; Yang, Jing; Miozzi, Francesca; Vitale, Suzy; O.’Bannon, III, Earl. F.; Jenei, Zsolt; Chariton, Stella; Prakapenka, Vitali; Fei, Yingwei

doi:10.1038/s41598-024-61861-2

Title: Exploring toroidal anvil profiles for larger sample volumes above 4 Mbar

Journal Article · 17 May 2024 · Scientific Reports

DOI: https://doi.org/10.1038/s41598-024-61861-2 · OSTI ID:2352322

Zurkowski, Claire C.; Yang, Jing; Miozzi, Francesca; Vitale, Suzy; O.’Bannon, III, Earl. F.; Jenei, Zsolt; Chariton, Stella; Prakapenka, Vitali; Fei, Yingwei

Abstract With the advent of toroidal and double-stage diamond anvil cells (DACs), pressures between 4 and 10 Mbar can be achieved under static compression, however, the ability to explore diverse sample assemblies is limited on these micron-scale anvils. Adapting the toroidal DAC to support larger sample volumes offers expanded capabilities in physics, chemistry, and planetary science: including, characterizing materials in soft pressure media to multi-megabar pressures, synthesizing novel phases, and probing planetary assemblages at the interior pressures and temperatures of super-Earths and sub-Neptunes. Here we have continued the exploration of larger toroidal DAC profiles by iteratively testing various torus and shoulder depths with central culet diameters in the 30–50 µm range. We present a 30 µm culet profile that reached a maximum pressure of 414(1) GPa based on a Pt scale. The 300 K equations of state fit to our P–V data collected on gold and rhenium are compatible with extrapolated hydrostatic equations of state within 1% up to 4 Mbar. This work validates the performance of these large-culet toroidal anvils to > 4 Mbar and provides a promising foundation to develop toroidal DACs for diverse sample loading and laser heating.

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Sponsoring Organization:: USDOE

Grant/Contract Number:: AC52-07NA27344; AC02-06CH11357

OSTI ID:: 2352322

Alternate ID(s):: OSTI ID: 2375944

Journal Information:: Scientific Reports, Journal Name: Scientific Reports Journal Issue: 1 Vol. 14; ISSN 2045-2322

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United Kingdom

Language:: English

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