Imaging extended single crystal lattice distortion fields with multi-peak Bragg ptychography

Kandel, Saugat; Maddali, Sidharth; Huang, Xiaojing; Nashed, Youssef S. G.; Jacobsen, Chris; Allain, Marc; Hruszkewycz, Stephan O.

doi:10.1364/OE.516729

Title: Imaging extended single crystal lattice distortion fields with multi-peak Bragg ptychography

Journal Article · 13 May 2024 · Optics Express

DOI: https://doi.org/10.1364/OE.516729 · OSTI ID:2350720

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; Huang, Xiaojing;

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; Allain, Marc;

Recent advances in phase-retrieval-based x-ray imaging methods have demonstrated the ability to reconstruct 3D distortion vector fields within a nanocrystal by using coherent diffraction information from multiple crystal Bragg reflections. However, these works do not provide a solution to the challenges encountered in imaging lattice distortions in crystals with significant defect content that result in phase wrapping. Moreover, these methods only apply to isolated crystals smaller than the x-ray illumination, and therefore cannot be used for imaging of distortions in extended crystals. We introduce multi-peak Bragg ptychography which addresses both challenges via an optimization framework that combines stochastic gradient descent and phase unwrapping methods for robust image reconstruction of lattice distortions and defects in extended crystals. Our work uses modern automatic differentiation toolsets so that the method is easy to extend to other settings and easy to implement in high-performance computers. This work is particularly timely given the broad interest in using the increased coherent flux in fourth-generation synchrotrons for innovative material research.

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Sponsoring Organization:: USDOE

OSTI ID:: 2350720

Alternate ID(s):: OSTI ID: 2428900

Journal Information:: Optics Express, Journal Name: Optics Express Journal Issue: 11 Vol. 32; ISSN 1094-4087; ISSN OPEXFF

Publisher:: Optical Society of AmericaCopyright Statement

Country of Publication:: United States

Language:: English

References (41)

Measuring Three-Dimensional Strain and Structural Defects in a Single InGaAs Nanowire Using Coherent X-ray Multiangle Bragg Projection Ptychography Hill, Megan O.; Calvo-Almazan, Irene; Allain, Marc Nano Letters, Vol. 18, Issue 2 https://doi.org/10.1021/acs.nanolett.7b04024	journal	January 2018
Using automatic differentiation as a general framework for ptychographic reconstruction Kandel, Saugat; Maddali, S.; Allain, Marc Optics Express, Vol. 27, Issue 13 https://doi.org/10.1364/OE.27.018653	journal	January 2019
Tunable and Transferable Diamond Membranes for Integrated Quantum Technologies Guo, Xinghan; Delegan, Nazar; Karsch, Jonathan C. Nano Letters, Vol. 21, Issue 24 https://doi.org/10.1021/acs.nanolett.1c03703	journal	December 2021
Three-Dimensional Coherent X-Ray Diffraction Microscopy Robinson, Ian K.; Miao, Jianwei MRS Bulletin, Vol. 29, Issue 3 https://doi.org/10.1557/mrs2004.56	journal	March 2004
Three-dimensional high-resolution quantitative microscopy of extended crystals Godard, P.; Carbone, G.; Allain, M. Nature Communications, Vol. 2, Issue 1 https://doi.org/10.1038/ncomms1569	journal	September 2011
Invited Article: A unified evaluation of iterative projection algorithms for phase retrieval Marchesini, S. Review of Scientific Instruments, Vol. 78, Issue 1 https://doi.org/10.1063/1.2403783	journal	January 2007
Concurrent multi-peak Bragg coherent x-ray diffraction imaging of 3D nanocrystal lattice displacement via global optimization Maddali, Siddharth; Frazer, Travis D.; Delegan, Nazar npj Computational Materials, Vol. 9, Issue 1 https://doi.org/10.1038/s41524-023-01022-7	journal	May 2023
Structural sensitivity of x-ray Bragg projection ptychography to domain patterns in epitaxial thin films Hruszkewycz, S. O.; Zhang, Q.; Holt, M. V. Physical Review A, Vol. 94, Issue 4 https://doi.org/10.1103/PhysRevA.94.043803	journal	October 2016
Strain annealing of SiC nanoparticles revealed through Bragg coherent diffraction imaging for quantum technologies Hruszkewycz, S. O.; Maddali, S.; Anderson, C. P. Physical Review Materials, Vol. 2, Issue 8 https://doi.org/10.1103/PhysRevMaterials.2.086001	journal	August 2018
Nucleation of dislocations and their dynamics in layered oxide cathode materials during battery charging Singer, A.; Zhang, M.; Hy, S. Nature Energy, Vol. 3, Issue 8 https://doi.org/10.1038/s41560-018-0184-2	journal	July 2018
Nanoscale imaging of the full strain tensor of specific dislocations extracted from a bulk sample Hofmann, Felix; Phillips, Nicholas W.; Das, Suchandrima Physical Review Materials, Vol. 4, Issue 1 https://doi.org/10.1103/PhysRevMaterials.4.013801	journal	January 2020
Use of coherent X-ray diffraction to map strain fields in nanocrystals Robinson, I. K.; Vartanyants, I. A. Applied Surface Science, Vol. 182, Issue 3-4 https://doi.org/10.1016/S0169-4332(01)00438-X	journal	October 2001
Framework for three-dimensional coherent diffraction imaging by focused beam x-ray Bragg ptychography Hruszkewycz, Stephan O.; Holt, Martin V.; Tripathi, Ash Optics Letters, Vol. 36, Issue 12 https://doi.org/10.1364/OL.36.002227	journal	January 2011
Identifying Defects with Guided Algorithms in Bragg Coherent Diffractive Imaging Ulvestad, A.; Nashed, Y.; Beutier, G. Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/s41598-017-09582-7	journal	August 2017
Study of the Internal Compositions of Binary Alloy Pd-Rh Nanoparticles by Using Bragg Coherent Diffraction Imaging Kawaguchi, Tomoya; Cha, Wonsuk; Latyshev, Vitalii Journal of the Korean Physical Society, Vol. 75, Issue 7 https://doi.org/10.3938/jkps.75.528	journal	October 2019
Simultaneous Multi-Bragg Peak Coherent X-ray Diffraction Imaging Lauraux, Florian; Labat, Stéphane; Yehya, Sarah Crystals, Vol. 11, Issue 3 https://doi.org/10.3390/cryst11030312	journal	March 2021
Quantitative Nanoscale Imaging of Lattice Distortions in Epitaxial Semiconductor Heterostructures Using Nanofocused X-ray Bragg Projection Ptychography Hruszkewycz, S. O.; Holt, M. V.; Murray, C. E. Nano Letters, Vol. 12, Issue 10 https://doi.org/10.1021/nl303201w	journal	September 2012
Topological defect dynamics in operando battery nanoparticles Ulvestad, A.; Singer, A.; Clark, J. N. Science, Vol. 348, Issue 6241 https://doi.org/10.1126/science.aaa1313	journal	June 2015
Three-dimensional imaging of strain in a single ZnO nanorod Newton, Marcus C.; Leake, Steven J.; Harder, Ross Nature Materials, Vol. 9, Issue 2 https://doi.org/10.1038/nmat2607	journal	December 2009
High-resolution three-dimensional structural microscopy by single-angle Bragg ptychography Hruszkewycz, S. O.; Allain, M.; Holt, M. V. Nature Materials, Vol. 16, Issue 2 https://doi.org/10.1038/nmat4798	journal	November 2016
Concurrent phase retrieval for imaging strain in nanocrystals Newton, Marcus C. Physical Review B, Vol. 102, Issue 1 https://doi.org/10.1103/PhysRevB.102.014104	journal	July 2020
Fast two-dimensional phase-unwrapping algorithm based on sorting by reliability following a noncontinuous path Herráez, Miguel Arevallilo; Burton, David R.; Lalor, Michael J. Applied Optics, Vol. 41, Issue 35 https://doi.org/10.1364/AO.41.007437	journal	January 2002
Adorym: a multi-platform generic X-ray image reconstruction framework based on automatic differentiation Du, Ming; Kandel, Saugat; Deng, Junjing Optics Express, Vol. 29, Issue 7 https://doi.org/10.1364/OE.418296	journal	January 2021
Gas-Induced Segregation in Pt-Rh Alloy Nanoparticles Observed by In Situ Bragg Coherent Diffraction Imaging Kawaguchi, Tomoya; Keller, Thomas F.; Runge, Henning Physical Review Letters, Vol. 123, Issue 24 https://doi.org/10.1103/PhysRevLett.123.246001	journal	December 2019
Propagation uniqueness in three-dimensional coherent diffractive imaging Huang, Xiaojing; Harder, Ross; Xiong, Gang Physical Review B, Vol. 83, Issue 22 https://doi.org/10.1103/PhysRevB.83.224109	journal	June 2011
Coherent X-ray diffraction imaging of strain at the nanoscale Robinson, Ian; Harder, Ross Nature Materials, Vol. 8, Issue 4 https://doi.org/10.1038/nmat2400	journal	April 2009
A Review of Actuation and Sensing Mechanisms in MEMS-Based Sensor Devices Algamili, Abdullah Saleh; Khir, Mohd Haris Md.; Dennis, John Ojur Nanoscale Research Letters, Vol. 16, Issue 1 https://doi.org/10.1186/s11671-021-03481-7	journal	January 2021
Efficient ptychographic phase retrieval via a matrix-free Levenberg-Marquardt algorithm Kandel, Saugat; Maddali, S.; Nashed, Youssef S. G. Optics Express, Vol. 29, Issue 15 https://doi.org/10.1364/OE.422768	journal	July 2021
Imaging Local Polarization in Ferroelectric Thin Films by Coherent X-Ray Bragg Projection Ptychography Hruszkewycz, S. O.; Highland, M. J.; Holt, M. V. Physical Review Letters, Vol. 110, Issue 17, Article No. 177601 https://doi.org/10.1103/PhysRevLett.110.177601	journal	April 2013
The structure of gold nanoparticles: molecular dynamics modeling and its verification by X-ray diffraction Kamiński, Michał; Jurkiewicz, Karolina; Burian, Andrzej Journal of Applied Crystallography, Vol. 53, Issue 1 https://doi.org/10.1107/S1600576719014511	journal	February 2020
Phase retrieval of diffraction from highly strained crystals Newton, Marcus C.; Harder, Ross; Huang, Xiaojing Physical Review B, Vol. 82, Issue 16 https://doi.org/10.1103/PhysRevB.82.165436	journal	October 2010
Single Particle Nanomechanics in Operando Batteries via Lensless Strain Mapping Ulvestad, Andrew; Singer, Andrej; Cho, Hyung-Man Nano Letters, Vol. 14, Issue 9 https://doi.org/10.1021/nl501858u	journal	August 2014
Strain in a silicon-on-insulator nanostructure revealed by 3D x-ray Bragg ptychography Chamard, V.; Allain, M.; Godard, P. Scientific Reports, Vol. 5, Issue 1 https://doi.org/10.1038/srep09827	journal	May 2015
Adam: A Method for Stochastic Optimization Kingma, Diederik P.; Ba, Jimmy arXiv https://doi.org/10.48550/arXiv.1412.6980	preprint	January 2014
scikit-image: image processing in Python van der Walt, Stéfan; Schönberger, Johannes L.; Nunez-Iglesias, Juan PeerJ, Vol. 2 https://doi.org/10.7717/peerj.453	journal	January 2014
Dealloying in Individual Nanoparticles and Thin Film Grains: A Bragg Coherent Diffractive Imaging Study Cha, Wonsuk; Liu, Yihua; You, Hoydoo Advanced Functional Materials, Vol. 27, Issue 25 https://doi.org/10.1002/adfm.201700331	journal	May 2017
TensorFlow: Large-Scale Machine Learning on Heterogeneous Distributed Systems Abadi, Martín; Agarwal, Ashish; Barham, Paul arXiv https://doi.org/10.48550/arXiv.1603.04467	preprint	January 2016
New Robust 3-D Phase Unwrapping Algorithms: Application to Magnetic Field Mapping and Undistorting Echoplanar Images Cusack, R.; Papadakis, N. NeuroImage, Vol. 16, Issue 3 https://doi.org/10.1006/nimg.2002.1092	journal	July 2002
Bragg x-ray ptychography of a silicon crystal: Visualization of the dislocation strain field and the production of a vortex beam Takahashi, Yukio; Suzuki, Akihiro; Furutaku, Shin Physical Review B, Vol. 87, Issue 12 https://doi.org/10.1103/PhysRevB.87.121201	journal	March 2013
Experimental demonstration of coupled multi-peak Bragg coherent diffraction imaging with genetic algorithms Wilkin, Matthew J.; Maddali, Siddharth; Hruszkewycz, Stephan O. Physical Review B, Vol. 103, Issue 21 https://doi.org/10.1103/PhysRevB.103.214103	journal	June 2021
Bragg coherent diffraction imaging by simultaneous reconstruction of multiple diffraction peaks Gao, Yuan; Huang, Xiaojing; Yan, Hanfei Physical Review B, Vol. 103, Issue 1 https://doi.org/10.1103/PhysRevB.103.014102	journal	January 2021

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