Title: Carbon-detected deuterium solid-state NMR rotating frame relaxation measurements for protein methyl groups under magic angle spinning

Journal Article · · Solid State Nuclear Magnetic Resonance
; ;

Not Available

Sponsoring Organization:
USDOE
OSTI ID:
2326248
Journal Information:
Solid State Nuclear Magnetic Resonance, Journal Name: Solid State Nuclear Magnetic Resonance Journal Issue: C Vol. 130; ISSN 0926-2040
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (38)

Quadruple-Resonance Magic-Angle Spinning NMR Spectroscopy of Deuterated Solid Proteins journal January 2014
Deuterium Rotating Frame NMR Relaxation Measurements in the Solid State under Static Conditions for Quantification of Dynamics journal August 2018
Ramped-Amplitude Cross Polarization in Magic-Angle-Spinning NMR journal October 1994
Deuterium Cross-Polarization Magic-Angle Spinning journal September 1996
Improved Proton Decoupling in NMR Spectroscopy of Crystalline Solids Using the S PINAL -64 Sequence journal December 2002
Monitoring conformational dynamics with solid-state R 1ρ experiments journal July 2009
Conformational dependence of 13C shielding and coupling constants for methionine methyl groups journal August 2010
Microsecond motions probed by near-rotary-resonance R1ρ 15N MAS NMR experiments: the model case of protein overall-rocking in crystals journal May 2018
Off-resonance 13C–2H REDOR NMR for site-resolved studies of molecular motion journal August 2021
Deuterium Relaxation In Molecular Solids book January 1991
Comment to -NMR studies of α and γ polymorphs of glycine journal June 1998
Heteronuclear decoupling under fast MAS by a rotor-synchronized Hahn-echo pulse train journal October 2005
Characterization of dynamic processes using deuterium in uniformly 2H,13C,15N enriched peptides by MAS solid-state NMR journal March 2006
2H–13C HETCOR MAS NMR for indirect detection of 2H quadrupole patterns and spin–lattice relaxation rates journal January 2013
Chemical exchange in biomacromolecules: Past, present, and future journal April 2014
Relaxing with liquids and solids – A perspective on biomolecular dynamics journal September 2019
Dynamics of uniformly labelled solid proteins between 100 and 300 K: A 2D 2H-13C MAS NMR approach journal June 2021
Deuteron rotating frame relaxation for the detection of slow motions in rotating solids journal April 2022
Deuteron off-resonance rotating frame relaxation for the characterization of slow motions in rotating and static solid-state proteins journal July 2023
On the use of cross polarization in solid-state NMR: 1H spin-lock versus adiabatic demagnetization in the rotating frame journal August 2022
Studying dynamics by magic-angle spinning solid-state NMR spectroscopy: Principles and applications to biomolecules journal August 2016
Static solid-state 2H NMR methods in studies of protein side-chain dynamics journal August 2017
Recent developments in deuterium solid-state NMR for the detection of slow motions in proteins journal February 2021
Site-specific protein backbone deuterium 2Hα quadrupolar patterns by proton-detected quadruple-resonance 3D 2HαcαNH MAS NMR spectroscopy journal June 2023
Characterization of Dynamics of Perdeuterated Proteins by MAS Solid-State NMR journal August 2005
Protein Side-Chain Dynamics Observed by Solution- and Solid-State NMR:  Comparative Analysis of Methyl 2H Relaxation Data journal September 2006
Proton-Detected Solid-State NMR Spectroscopy of Fully Protonated Proteins at 40 kHz Magic-Angle Spinning journal September 2007
A Study of Phenylalanine Side-Chain Dynamics in Surface-Adsorbed Peptides Using Solid-State Deuterium NMR and Rotamer Library Statistics journal August 2014
Site-Specific Internal Motions in GB1 Protein Microcrystals Revealed by 3D 2 H– 13 C– 13 C Solid-State NMR Spectroscopy journal March 2016
Optimal 2 H rf Pulses and 2 H– 13 C Cross-Polarization Methods for Solid-State 2 H MAS NMR of Perdeuterated Proteins journal May 2011
The role of dynamic conformational ensembles in biomolecular recognition journal October 2009
Elucidating proline dynamics in spider dragline silk fibre using 2 H– 13 C HETCOR MAS NMR journal January 2014
Low-power polarization transfer between deuterons and spin-1/2 nuclei using adiabatic RESPIRATIONCP in solid-state NMR journal January 2014
The relaxation dynamics of spin I =1 nuclei with a static quadrupolar coupling and a radio‐frequency field journal October 1993
Deuterium to carbon cross-polarization in liquid crystals journal August 1998
Characterization of leucine side-chain reorientation in collagen-fibrils by solid-state 2H NMR. journal January 1982
Solid state deuterium NMR study of LKα14 peptide aggregation in biosilica journal June 2017
Performance of the cross-polarization experiment in conditions of radiofrequency field inhomogeneity and slow to ultrafast magic angle spinning (MAS) journal August 2023

Similar Records

Related Subjects