DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Predicting Sintering Window of Binder Jet Additively Manufactured Parts Using a Coupled Data Analytics and CALPHAD Approach

Journal Article · · Integrating Materials and Manufacturing Innovation

Batch-to-batch variation in powder compositions for binder jet additive manufacturing (BJAM) can significantly deter defining an “ideal” sintering window for a given alloy. One way to overcome the problem is by running sintering experiments at various temperatures for each batch of the powder. However, such an approach increases the time required to achieve large-scale production of parts. The predictive capabilities of computational thermodynamic tools like CALPHAD can be leveraged to overcome the challenge, especially for binder jet additive manufacturing, since the process occurs under near-equilibrium conditions. However, calculating the sintering window using CALPHAD can be computationally expensive, considering many possible feedstock compositions within “specification”. Here, we generate high throughput CALPHAD data for nickel-based superalloys to develop machine learning models to predict the sintering window rapidly. The predictive capability of the models has been validated using published results on BJAM of Inconel 718 and 625. Further, validated models are lightweight and can be deployed in an industrial setting to get sintering window in an accelerated manner.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Manufacturing Demonstration Facility (MDF)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE), Energy Efficiency Office. Advanced Materials & Manufacturing Technologies Office (AMMTO); USDOE Office of Fossil Energy and Carbon Management (FECM)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
2204597
Journal Information:
Integrating Materials and Manufacturing Innovation, Journal Name: Integrating Materials and Manufacturing Innovation Vol. 12; ISSN 2193-9764
Publisher:
SpringerCopyright Statement
Country of Publication:
United States
Language:
English

References (18)

Process development toward full-density stainless steel parts with binder jetting printing journal October 2017
Analysis of DTA curves and calculation of kinetic data using computer technique journal April 1978
Effect of production parameters on the properties of IN 718 superalloy by three-dimensional printing journal December 2008
Predicting sintering window during supersolidus liquid phase sintering of steels using feedstock analysis and CALPHAD journal December 2021
Powder bed binder jet printed alloy 625: Densification, microstructure and mechanical properties journal October 2016
Supersolidus liquid-phase sintering of prealloyed powders journal July 1997
Influence of powder type and binder saturation on binder jet 3D–printed and sintered Inconel 625 samples journal July 2021
Supersolidus Liquid Phase Sintering Modeling of Inconel 718 Superalloy journal November 2015
Heat Transfer and Phase Transition in DTA Experiments book January 2012
Thermo-Calc & DICTRA, computational tools for materials science journal June 2002
Effect of powder size distribution on densification and microstructural evolution of binder-jet 3D-printed alloy 625 journal January 2019
Supersolidus liquid phase sintering of high speed steels: Part 3: computer aided design of sinterable alloys journal February 1999
Densification and shape retention in supersolidus liquid phase sintering journal December 1999
Microstructural evolution and mechanical properties of differently heat-treated binder jet printed samples from gas- and water-atomized alloy 625 powders journal February 2017
Powder bed binder jet 3D printing of Inconel 718: Densification, microstructural evolution and challenges☆ journal August 2017
Binder jet 3D printing—Process parameters, materials, properties, modeling, and challenges journal June 2020
Metal Binder Jetting Additive Manufacturing: A Literature Review journal June 2020
Transient liquid phase bonding of Inconel 617 superalloy: effect of filler metal type and bonding time journal October 2018