DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Microstructural control of additively manufactured Ti6Al4V via in-situ large-area laser annealing

Journal Article · · Scripta Materialia

Additively manufactured (AM) alloy Ti6Al4V often exhibits a distinctive α/α’ microstructure due to the high cooling rates associated with AM, which can lead to increased brittleness and necessitate costly post-processing and heat treatment. In this work, we explore the use of layer-by-layer large area surface annealing with a secondary diode laser to control the microstructure of Ti6Al4V during AM and site-specifically induce more ductile, dual-phase α/β Ti6Al4V. Annealing treatments were selected to target sub- and super-β-transus temperatures at annealed layers, leading to 13% and 20% reductions in hardness, respectively, in the 2 mm below the annealed surfaces. Components with rapid switching between annealed and unannealed microstructures were also produced. Temperature measurements at the built surface and base plate were combined with a thermal model to validate microstructural observations, setting the stage for development of full 3-D microstructure and property control using in-situ laser annealing.

Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
Grant/Contract Number:
AC52-07NA27344
OSTI ID:
2202706
Alternate ID(s):
OSTI ID: 2202550
Report Number(s):
LLNL-JRNL-853691; 1081565
Journal Information:
Scripta Materialia, Vol. 239; ISSN 1359-6462
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (25)

Diode-based additive manufacturing of metals using an optically-addressable light valve journal January 2017
Energy and emissions saving potential of additive manufacturing: the case of lightweight aircraft components journal November 2016
The Additive Manufacturing (AM) of titanium alloys journal March 2017
Additive manufacturing of strong and ductile Ti–6Al–4V by selective laser melting via in situ martensite decomposition journal February 2015
Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM) journal February 2017
Mechanical properties and microstructure of a Ti-6Al-4V alloy subjected to cold rolling, asymmetric rolling and asymmetric cryorolling journal January 2018
Controlling martensitic decomposition during selective laser melting to achieve best ductility in high strength Ti-6Al-4V journal January 2019
As-Fabricated and Heat-Treated Microstructures of the Ti-6Al-4V Alloy Processed by Selective Laser Melting journal May 2011
Effect of heat treatment on the phase transformation and mechanical properties of Ti6Al4V fabricated by selective laser melting journal October 2018
Heat treatment of Ti6Al4V produced by Selective Laser Melting: Microstructure and mechanical properties journal November 2012
Ductility improvement due to martensite α′ decomposition in porous Ti–6Al–4V parts produced by selective laser melting for orthopedic implants journal February 2016
In situ observations of lattice expansion and transformation rates of α and β phases in Ti–6Al–4V journal January 2005
In situ tailoring microstructure in additively manufactured Ti-6Al-4V for superior mechanical performance journal February 2017
Effect of subtransus heat treatment on the microstructure and mechanical properties of additively manufactured Ti-6Al-4V alloy journal February 2018
Parent grain reconstruction from partially or fully transformed microstructures in MTEX journal February 2022
Phase evolution of Ti–6Al–4V during continuous heating journal August 1999
Inducing Stable α + β Microstructures during Selective Laser Melting of Ti-6Al-4V Using Intensified Intrinsic Heat Treatments journal March 2017
The formation of α + β microstructure in as-fabricated selective laser melting of Ti–6Al–4V journal July 2014
Texture Analysis with MTEX – Free and Open Source Software Toolbox journal February 2010
The Kinetics of Phase Transformations During Continuous Cooling of the Ti6Al4V Alloy from the Single-Phase β Range journal September 2011
Variant selection during α precipitation in Ti–6Al–4V under the influence of local stress – A simulation study journal September 2013
Review of Mechanical Properties of Ti-6Al-4V Made by Laser-Based Additive Manufacturing Using Powder Feedstock journal December 2015
Recycling of Titanium Alloy Powders and Swarf through Continuous Extrusion (ConformTM) into Affordable Wire for Additive Manufacturing journal June 2020
The effect of heat treatment on microstructure evolution and tensile properties of selective laser melted Ti6Al4V alloy journal April 2019
A Review on Additive Manufacturing of Titanium Alloys for Aerospace Applications: Directed Energy Deposition and Beyond Ti-6Al-4V journal April 2021

Similar Records

Evaluation of microstructure and mechanical properties of additively manufactured Ti–5V–5Mo-5 Al-3 Cr alloy
Journal Article · 2024 · Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing · OSTI ID:2396385

Tailoring Microstructure and Mechanical Properties of Additively-Manufactured Ti6Al4V Using Post Processing
Journal Article · 2021 · Materials · OSTI ID:1815802

Hydrogen-Aided Microstructural Engineering of Additively Manufactured Ti–6Al–4V
Journal Article · 2023 · Metallurgical and Materials Transactions. B, Process Metallurgy and Materials Processing Science · OSTI ID:2007704