Shape-controlled synthesis of CO-free Pd nanocrystals with the use of formic acid as a reducing agent

Bao, Shixiong; Yang, Xuan; Luo, Ming; Zhou, Shan; Wang, Xue; Xie, Zhaoxiong; Xia, Younan

doi:10.1039/c6cc07055h

Title: Shape-controlled synthesis of CO-free Pd nanocrystals with the use of formic acid as a reducing agent

Journal Article · 29 September 2016 · ChemComm

DOI: https://doi.org/10.1039/c6cc07055h · OSTI ID:2008035

Bao, Shixiong ^[1]; Yang, Xuan ^[2]; Luo, Ming ^[2]; Zhou, Shan ^[3]; Wang, Xue ^[4]; Xie, Zhaoxiong ^[5]; Xia, Younan ^[2]

Georgia Institute of Technology, Atlanta, GA (United States); Emory Univ., Atlanta, GA (United States); Xiamen University (China); Georgia Institute of Technology School of Chemistry & Biochemistry
Georgia Institute of Technology, Atlanta, GA (United States); Emory Univ., Atlanta, GA (United States)
Georgia Institute of Technology, Atlanta, GA (United States)
Georgia Institute of Technology, Atlanta, GA (United States); Emory Univ., Atlanta, GA (United States); Xiamen University (China)
Xiamen University (China)

The work in this paper reports the use of formic acid as a reducing agent for the shape-controlled synthesis of Pd nanocrystals with no chemisorption of CO on the surface, as confirmed by attenuated total reflection Fourier transform infrared (ATR-FT-IR) spectroscopy.

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Research Organization:: Univ. of Wisconsin, Madison, WI (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: FG02-05ER15731

OSTI ID:: 2008035

Journal Information:: ChemComm, Journal Name: ChemComm Journal Issue: 85 Vol. 52; ISSN 1359-7345

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

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